IP Library Granted Patent US 8,354,067
Granted Patent B2
US 8,354,067 · App. 12/404,165 · Granted Jan 15, 2013

Processing asphaltene-containing tailings

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Quick Facts
Patent No.
US 8,354,067
App. No.
12/404,165
Granted
Jan 15, 2013
Kind
B2
Abstract

Embodiments of a method and a system for recovering energy, materials or both from asphaltene-containing tailings are disclosed. The asphaltene-containing tailings can be generated, for example, from a process for recovering hydrocarbons from oil sand. Embodiments of the method can include a flotation separation and a hydrophobic agglomeration separation. Flotation can be used to separate the asphaltene-containing tailings into an asphaltene-rich froth and an asphaltene-depleted aqueous phase. The asphaltene-rich froth, or an asphaltene-rich slurry formed from the asphaltene-rich froth, then can be separated into a heavy mineral concentrate and a light tailings. Hydrophobic agglomeration can be used to recover an asphaltene concentrate from the light tailings. Another flotation separation can be included to remove sulfur-containing minerals from the heavy mineral concentrate. Oxygen-containing minerals also can be recovered from the heavy mineral concentrate. Water removed by the various separation steps can be recycled and its heat energy recovered.

Claims (17)

1. A system for recovering energy, materials or both from asphaltene-containing tailings, comprising:

a flotation apparatus for separating asphaltene-containing tailings into an asphaltene-rich froth and an asphaltene-depleted aqueous phase, the flotation apparatus including an asphaltene-containing tailings inlet, an asphaltene-rich froth outlet, and an asphaltene-depleted aqueous phase outlet;

a gravity separation apparatus for separating the asphaltene-rich froth into a heavy mineral concentrate and a light tailings, the gravity separation apparatus including a heavy mineral concentrate outlet, a light tailings outlet, and an asphaltene-rich froth inlet, the asphaltene-rich froth inlet being routed to the asphaltene-rich froth outlet;

a hydrophobic agglomeration mixing apparatus for dispersing a hydrophobic agglomeration agent within the light tailings, the hydrophobic agglomeration mixing apparatus including a mixed light tailings outlet and a light tailings inlet, the light tailings inlet being routed to the light tailings outlet; and

a hydrophobic agglomeration settling apparatus for separating an asphaltene concentrate from the light tailings, the hydrophobic agglomeration settling apparatus including a mixed light tailings inlet routed from the mixed light tailings outlet, an asphaltene concentrate outlet and a water and mineral solids outlet.

2. The system according to claim 1 , wherein the hydrophobic agglomeration settling apparatus is effective to concentrate asphaltenes.

3. The system according to claim 1 , further comprising a cyclone separation apparatus for separating coarse minerals from the asphaltene-containing tailings before the asphaltene-containing tailings enter the flotation apparatus, the cyclone separation apparatus including an asphaltene-containing tailings outlet routed to the asphaltene-containing tailings inlet.

4. The system according to claim 1 , wherein the flotation apparatus further comprises a conduit for recycling water that exits the flotation apparatus.

5. The system according to claim 1 , wherein the flotation apparatus is a first flotation apparatus and further comprising a second flotation apparatus for separating the heavy mineral concentrate into a sulfur-rich froth and a sulfur-depleted aqueous phase, the second flotation apparatus including a heavy mineral concentrate inlet routed to the heavy mineral concentrate outlet.

6. A system for recovering enerty, materials or both from asphaltene-containing tailings, comprising:

a flotation apparatus for separating asphaltene-containing tailings into an asphaltene-rich froth and an asphaltene-depleted aqueous phase, the flotation apparatus including an asphaltene-containing tailings inlet, an asphaltene-rich froth outlet, and an asphaltene-depleted aqueous phase outlet;

a thickening apparatus for thickening the asphaltene-rich froth to form an asphaltene-rich slurry, the thickening apparatus including an asphaltene-rich froth inlet and an asphaltene-rich slurry outlet, the asphaltene-rich froth inlet being routed to the asphaltene-rich froth outlet;

a gravity separation apparatus for separating the asphaltene-rich slurry into a heavy mineral concentrate and a light tailings, the gravity separation apparatus including a heavy mineral concentrate outlet, a light tailings outlet, and an asphaltene-rich slurry inlet, the asphaltene-rich slurry inlet being routed to the asphaltene-rich slurry outlet; and

a hydrophobic agglomeration mixing apparatus for dispersing a hydrophobic agglomeration agent within the light tailings, the hydrophobic agglomeration mixing apparatus including a mixed light tailings outlet and a light tailings inlet, the light tailings inlet being routed to the light tailings outlet.

7. The system according to claim 1 , further comprising:

a hydrophobic agglomeration agent source including a hydrophobic agglomeration agent outlet; and

wherein the hydrophobic agglomeration mixing apparatus further includes a hydrophobic agglomeration agent inlet, the hydrophobic agglomeration agent outlet being routed to the hydrophobic agglomeration agent inlet.

Assignments (2)
NUNC PRO TUNC ASSIGNMENT Recorded Feb 27, 2018
From: SHELL CANADA ENERGY
To: CANADIAN NATURAL UPGRADING LIMITED
Reel/Frame 045054/0463 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 30, 2012
From: MARATHON OIL CANADA CORPORATION
To: SHELL CANADA ENERGY
Reel/Frame 028128/0322 →