IP Library Granted Patent US 8,048,340
Granted Patent B2
US 8,048,340 · App. 12/420,000 · Granted Nov 1, 2011

Polyaniline/c-MWNT nanocomposite and method for fabricating the same

Assignee: Chung-Shan Institute of Science and Technology Armaments Bureau, Ministry of National Defense
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Quick Facts
Patent No.
US 8,048,340
App. No.
12/420,000
Granted
Nov 1, 2011
Kind
B2
Abstract

The invention discloses a polyaniline/c-MWNT nanocomposite and a method for fabricating the same. The method comprises the following steps: carboxylating at least one carbon nanotube to form at least one carboxylic carbon nanotube; mixing the at least one carboxylic carbon nanotube with a solvent to form a first carbon nanotube solution; mixing at least one aniline monomer with the first carbon nanotube solution to form a second carbon nanotube solution; mixing an ammonium persulfate solution with the second carbon nanotube solution to form a third carbon nanotube solution; air-extracting and filtering the third carbon nanotube solution to obtain the polyaniline/c-MWNT nanocomposite; cleaning and baking the polyaniline/c-MWNT nanocomposite. The polyaniline/c-MWNT nanocomposite fabricated by the method could be used for electromagnetic shielding or anti-static shielding.

Claims (19)

1. A method for fabricating a polyaniline/c-MWNT nanocomposite, comprising the following steps:

carboxylating at least one carbon nanotube to form at least one carboxylic carbon nanotube;

mixing the at least one carboxylic carbon nanotube with a solvent to form a first carbon nanotube solution;

mixing at least one aniline monomer with the first carbon nanotube solution to form a second carbon nanotube solution;

mixing an ammonium persulfate solution with the second carbon nanotube solution to form a third carbon nanotube solution;

air-extracting and filtering the third carbon nanotube solution to obtain the polyaniline/c-MWNT nanocomposite; and

cleaning and baking the polyaniline/c-MWNT nanocomposite.

2. The method of claim 1 , wherein the carboxylic carbon nanotubes of the polyaniline/c-MWNT nanocomposite disperse in the polyaniline.

3. The method of claim 1 , further comprising the following steps:

mixing at least one carbon nanotube with a sulfuric acid/nitric acid solution to form a mixed solution;

ultrasonic vibrating the mixed solution;

air-extracting and filtering the mixed solution to obtain at lease one carboxylic carbon nanotube; and

cleaning and baking the carboxylic carbon nanotubes.

4. The method of claim 3 , wherein the ratio of the sulfuric acid to the nitric acid of the sulfuric acid/nitric acid solution is 3:1.

5. The method of claim 3 , wherein the mixed solution is ultrasonic vibrated under the temperature range of 20±5° C.

6. The method of claim 1 , wherein the composition of the solvent is hydrochloric acid, namely, hydrogen chloride.

7. The method of claim 1 , wherein the ammonium persulfate solution is a mixture of ammonium persulfate and a first solvent.

8. The method of claim 7 , wherein the composition of the first solvent is substantially the same as that of the solvent.

9. The method of claim 1 , wherein the polyaniline/c-MWNT nanocomposite comprises an emeraldine base form of polyaniline.

Assignments (2)
CHANGE OF NAME Recorded Apr 17, 2015
From: CHUNG-SHAN INSTITUTE OF SCIENCE AND TECHNOLOGY, ARMAMENTS, BUREAU, MINISTRY OF NATIONAL DEFENSE
To: NATIONAL CHUNG SHAN INSTITUTE OF SCIENCE AND TECHNOLOGY
Reel/Frame 035453/0379 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 7, 2009
From: YANG, CHENG-CHIEN; YEH, JUI-MING; GU, WANG-TSAI; HUANG, KUAN-YEH; PENG, YUEN-HSIN
To: CHUNG-SHAN INSTITUTE OF SCIENCE AND TECHNOLOGY, ARMAMENTS BUREAU, MINISTRY OF NATIONAL DEFENSE
Reel/Frame 022517/0662 →
Continuity (1)
Related Publication 20100256327A1 · Oct 7, 2010