Process for manufacturing a thermostructural composite part
View Patent ↗The invention relates to a method of fabricating a composite material part comprising fiber reinforcement densified by a matrix, the method comprising the steps of: making a fiber preform consolidated by impregnating (S 4 ) a fiber texture made up of yarns with a liquid consolidation composition containing a precursor for a consolidating material, and by transforming (S 7 ) the precursor into consolidating material by pyrolysis so as to obtain a consolidated preform that is held in shape; and densifying (S 8 ) the consolidated fiber preform by chemical vapor infiltration; the method being characterized in that it includes, prior to impregnation (S 4 ) of the fiber texture with the consolidation liquid composition, a step of filling (S 2 ) the pores of the yarns of said fiber texture by means of a filler composition.
1. A method of fabricating a composite material part comprising fiber reinforcement densified by a matrix, said method comprising the steps of:
making a fiber preform consolidated by impregnating a fiber texture made up of yarns with a liquid consolidation composition containing a precursor for a consolidating material, and by transforming the precursor into consolidating material by pyrolysis so as to obtain a consolidated preform that is held in shape; and
densifying the consolidated fiber preform by chemical vapor infiltration;
the method being characterized in that it includes, prior to impregnation of the fiber texture with the consolidation liquid composition and prior to chemical vapor infiltration of the fiber preform, a step of filling the pores of the yarns of said fiber texture by means of a filler composition;
the method being further characterized in that in the filling step, the quantity of filler liquid composition is selected in such a manner as to fill the internal spaces within the yarns without any overflowing so as to prevent the filler liquid from occupying any of the spaces between the yarns of the fiber texture.
2. A method according to claim 1 , characterized in that in the filling step, the pores of the yarns of said texture are filled by means of a filler liquid composition.
3. A method according to claim 2 , characterized in that the filler liquid composition contains a sacrificial resin.
4. A method according to claim 3 , characterized in that the sacrificial resin is not miscible with the filler liquid composition.
5. A method according to claim 3 , characterized in that the sacrificial resin is selected from silicone oils, polyvinyl acetate, and thermoplastic resins.
6. A method according to claim 2 , characterized in that the preform is made from a carbon or ceramic fiber texture and in that the consolidating material precursor of the consolidation liquid composition is a resin selected from carbon-precursor resins and ceramic-precursor resins.
7. A method according to claim 1 , characterized in that, in the filling step, the pores in the yarns of said texture are filled by means of thermoplastic yarns mixed with the yarns of said texture.
8. A method according to claim 1 , characterized in that the fiber preform is made from a ceramic fiber texture and in that the filler liquid composition contains a carbon-precursor resin, said preform being oxidized after pyrolysis to eliminate the coke of the carbon-precursor resin.
9. A method according to claim 8 , characterized in that the consolidating material precursor of the consolidation liquid composition is a ceramic-precursor resin.
10. A method according to claim 9 , characterized in that the ceramic-precursor resin of the consolidation liquid composition is a resin selected from polycarbosilazane resin, polycarbosilane resin, and polysiloxane resin.
11. A method according to claim 10 , characterized in that it includes, prior to impregnating the fiber texture with the consolidation liquid composition, a step of polymerizing the carbon-precursor resin.
12. A method according to claim 9 , characterized in that it includes, prior to impregnating the fiber texture with the consolidation liquid composition, a step of polymerizing the carbon-precursor resin.
13. A method according to claim 8 , characterized in that it includes, prior to impregnating the fiber texture with the consolidation liquid composition, a step of polymerizing the carbon-precursor resin.
14. A method according to claim 1 , characterized in that the filler liquid composition contains a ceramic-precursor resin, the consolidation liquid composition containing a carbon-precursor resin.
15. A method according to claim 14 , characterized in that the ceramic-precursor resin of the filler liquid composition is a resin selected from polycarbosilazane resin, polycarbosilane resin, and polysiloxane resin.
16. A method according to claim 15 , characterized in that it includes, prior to impregnating the yarns of the fiber texture with the consolidation liquid composition, a step of polymerizing the ceramic-precursor resin.
17. A method according to claim 14 , characterized in that it includes, prior to impregnating the yarns of the fiber texture with the consolidation liquid composition, a step of polymerizing the ceramic-precursor resin.
18. A method according to claim 1 , characterized in that the filler liquid composition contains a sacrificial resin.
19. A method according to claim 18 , characterized in that the sacrificial resin is not miscible with the filler liquid composition.
20. A method according to claim 1 , characterized in that the preform is made from a carbon or ceramic fiber texture and in that the consolidating material precursor of the consolidation liquid composition is a resin selected from carbon-precursor resins and ceramic-precursor resins.