IP Library Granted Patent US 8,158,823
Granted Patent B2
US 8,158,823 · App. 12/464,518 · Granted Apr 17, 2012

Method for the modernization of a urea production plant

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Quick Facts
Patent No.
US 8,158,823
App. No.
12/464,518
Granted
Apr 17, 2012
Kind
B2
Abstract

A method for revamping a conventional self-stripping urea plant is disclosed, where a minor portion ( 18 a ) of the carbon dioxide feed is fed to the stripper ( 7 ) and used as a stripping agent. In further embodiments, another carbamate condenser is installed, or the conventional horizontal shell-and-tube carbamate condenser ( 6 ) is replaced with a vertical submerged unit.

Claims (13)

1. A method for revamping a self-stripping urea plant, said plant comprising a high-pressure loop comprising at least a synthesis reactor receiving an ammonia feed and a carbon dioxide feed, a stripping section comprising at least one thermal stripper and a condensation section comprising at least one carbamate condenser, and further comprising medium-pressure and low-pressure equipments for carbamate and ammonia recover, the method comprising providing of a flow line adapted to feed, in operation, a minor portion of the total carbon dioxide feed to said stripping section, for use as a stripping agent.

2. The method according to claim 1 , wherein said minor portion of the total carbon dioxide feed, to be used as a stripping agent, is between 20 and 50%.

3. The method according to claim 1 , wherein a further condenser is added in parallel or in series with an existing condenser of said self-stripping urea plant.

4. The method according to claim 1 , wherein said self-stripping urea plant comprises a horizontal shell-and-tube carbamate condenser, and said condenser is replaced with a submerged vertical condenser.

5. The method according to claim 4 , wherein said submerged vertical condenser is arranged in a raised position with respect to the existing reactor and stripper of said urea plant, so as to allow, during operation of the revamped plant, a natural circulation by gravity in said high-pressure loop.

6. The method according to claim 5 , wherein a suitable support structure is provided for said condenser arranged in a raised position with respect to the existing reactor and stripper.

7. The method according to claim 4 , wherein said submerged vertical condenser is arranged substantially at the same height as the reactor.

8. The method according to claim 7 , wherein a pump is installed to deliver the condensed recycled carbamate solution from said condenser to the reactor.

9. The method according to claim 1 , characterized by the provision of a flow line adapted to feed a minor portion of a gaseous phase containing ammonia and carbon dioxide, coming out from the stripping section of said plant, directly to the reactor.

10. A process for the synthesis of urea in a self-stripping urea plant, where a high-pressure loop receives an ammonia feed and a carbon dioxide feed, said loop comprising a synthesis reactor, a stripping section comprising at least one thermal stripper, and a condensation section comprising at least one carbamate condenser, the process being characterized in that a minor portion of the total carbon dioxide feed to said stripping section, for use as a stripping agent.

11. The process according to claim 10 , where said minor portion is between 20% and 50%.

12. The method according to claim 2 , wherein said minor portion of the total carbon dioxide feed, to be used as a stripping agent, is around 30%.

13. The process according to claim 12 , where said minor portion is around 30%.

Assignments (2)
MERGER Recorded Dec 4, 2014
From: AMMONIA CASALE SA; UREA CASALE SA; METHANOL CASALE SA; CASALE CHEMICALS SA
To: CASALE SA
Reel/Frame 034533/0456 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 7, 2009
From: ZARDI, FEDERICO; SCOTTO, ANDREA
To: UREA CASALE S.A.
Reel/Frame 022923/0656 →