IP Library Granted Patent US 7,915,299
Granted Patent B2
US 7,915,299 · App. 12/515,049 · Granted Mar 29, 2011

2-(2-hydroxyphenyl)benzimidazoles useful for treating obesity and diabetes

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Quick Facts
Patent No.
US 7,915,299
App. No.
12/515,049
Granted
Mar 29, 2011
Kind
B2
Abstract

The present invention relates to novel compounds that act as chemical uncouplers. Compounds of the invention are useful, inter alia, in the treatment, including prevention, of obesity, diabetes and a number of diseases or conditions associated therewith.

Claims (59)

1. A compound according to formula I or a pharmaceutically acceptable salt thereof:

wherein

m is 0;

R 1 is tert-butyl;

R 2 is hydrogen, halogen, C 1-6 alkyl, C 1-6 alkenyl, C 1-6 alkynyl, C 3-8 -cycloalkyl, C 4-8 cycloalkenyl or C 1-6 alkoxy;

R 4 is methyl;

R 5 , R 6 and R 7 independently are hydrogen, nitro, cyano, halogen, C 1-6 alkyl, C 1-6 alkenyl, C 1-6 alkynyl, C 3-8 cycloalkyl, C 4-8 cycloalkenyl, C 1-6- haloalkyl, —OR 10 , —NR 10 R 11 , —C(O)OR 10 , —COR 10 , —C(O)NR 10 R 11 , —SH, —S(O) 2 NR 10 R 11 , —S(O)R 11 , aryl or heteroaryl, wherein the latter aryl or heteroaryl groups are optionally substituted with one or more substituents selected independently from the group consisting of C 1-6 alkyl, halogen, hydroxy and phenyl;

R 10 and R 11 independently are hydrogen, C 1-6 alkyl, C 1-6 alkenyl, C 1-6 alkynyl, C 3-8 -cycloalkyl, C 4-8 cycloalkenyl or C 1-6 haloalkyl; or R 10 and R 11 , together with the nitrogen atom to which they are attached form a saturated or unsaturated carbocyclic or heterocyclic 3-8-membered ring, optionally substituted with one or more C 1-6 alkyl substituents; and

R 3 is —SCH 3 , —S(O)CH 3 , —S(O) 2 CH 3 , fluoro, or chloro;

or a hydrate of any of the foregoing.

2. The compound according to claim 1 , wherein one substituent from among R 5 , R 6 and R 7 is —SR 11 , —S(O)R 11 or —S(O) 2 R 11 , wherein R 11 is C 1-6 -fluoroalkyl.

3. The compound according to claim 2 , wherein one substituent from among R 5 , R 6 and R 7 is —S(O) 2 CF 3 .

4. A compound, which is a compound selected from the group consisting of:

6-tert-Butyl-3-methyl-2-(5-trifluoromethyl-1H-benzimidazol-2-yl)-phenol;

2-(3-tert-Butyl-2-hydroxy-6-methyl-phenyl)-1H-benzimidazole-5-carbonitrile;

4-Bromo-6-tert-butyl-3-methyl-2-(5-trifluoromethyl-1H-benzimidazol-2-yl)-phenol;

2-(3-tert-Butyl-5-chloro-2-hydroxy-6-methyl-phenyl)-1H-benzimidazole-5-carbonitrile;

2-(3-tert-Butyl-5-chloro-2-hydroxy-6-methyl-phenyl)-1H-benzimidazole-5-sulfonic acid diethylamide;

6-tert-Butyl-4-chloro-3-methyl-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)-phenol;

6-tert-Butyl-3-methoxy-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)-phenol;

6-tert-Butyl-4-chloro-2-(5,6-difluoro-1H-benzimidazol-2-yl)-3-methyl-phenol;

6-tert-Butyl-4-chloro-3-methyl-2-(5-trifluoromethoxy-1H-benzimidazol-2-yl)-phenol;

4-Bromo-6-tert-butyl-3-methyl-2-(5-trifluoromethoxy-1H-benzimidazol-2-yl)-phenol;

6-tert-Butyl-3-methyl-4-methylsulfanyl-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)-phenol;

6-tert-Butyl-4-methanesulfinyl-3-methyl-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)-phenol;

6-tert-Butyl-4-fluoro-3-methyl-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)-phenol;

6-tert-Butyl-4-bromo-3-methyl-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)-phenol;

N-[5-tert-Butyl-4-hydroxy-2-methyl-3-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)-phenyl]-methanesulfonamide;

5-tert-Butyl-4-hydroxy-2-methyl-3-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)-benzonitrile;

6-tert-Butyl-4-methanesulfonyl-3-methyl-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)-phenol;

6-tert-Butyl-3-methyl-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)-4-trifluoromethylsulfanyl-phenol;

6-tert-Butyl-4-chloro-3-ethyl-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)-phenol;

6-tert-Butyl-3-ethyl-4-methanesulfinyl-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)-phenol;

(R)-6-tert-Butyl-4-methanesulfinyl-3-methyl-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)-phenol;

(S)-6-tert-Butyl-4-methanesulfinyl-3-methyl-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)-phenol;

4-Bromo-6-tert-butyl-3-isopropyl-2-(5-methanesulfonyl-1H-benzimidazol-2-yl)-phenol;

N-[5-tert-Butyl-4-hydroxy-3-(5-methanesulfonyl-1H-benzimidazol-2-yl)-2-methyl-phenyl]-methanesulfonamide;

6-tert-Butyl-4-fluoro-2-(5-methanesulfonyl-1H-benzimidazol-2-yl)-3-methyl-phenol;

6-tert-Butyl-3-isopropyl-2-(5-methanesulfonyl-1H-benzimidazol-2-yl)-phenol;

6-tert-Butyl-2-(5-methanesulfonyl-1H-benzimidazol-2-yl)-3-methyl-phenol; and

6-tert-Butyl-3-methyl-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)-phenol;

or a pharmaceutically acceptable salt thereof, or a hydrate of any of the foregoing.

5. A compound, which is a compound selected from the group consisting of:

6-tert-Butyl-3-methyl-2-(5-trifluoromethyl-1H-benzimidazol-2-yl)-phenol;

2-(3-tert-Butyl-2-hydroxy-6-methyl-phenyl)-1H-benzimidazole-5-carbonitrile;

2-(3-tert-Butyl-5-chloro-2-hydroxy-6-methyl-phenyl)-1H-benzimidazole-5-carbonitrile;

2-(3-tert-Butyl-5-chloro-2-hydroxy-6-methyl-phenyl)-1H-benzimidazole-5-sulfonic acid diethylamide;

6-tert-Butyl-4-chloro-3-methyl-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)-phenol;

6-tert-Butyl-3-methoxy-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)-phenol;

6-tert-Butyl-4-chloro-3-methyl-2-(5-trifluoromethoxy-1H-benzimidazol-2-yl)-phenol;

4-Bromo-6-tert-butyl-3-methyl-2-(5-trifluoromethoxy-1H-benzimidazol-2-yl)-phenol;

6-tert-Butyl-3-methyl-4-methylsulfanyl-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)-phenol;

6-tert-Butyl-4-methanesulfinyl-3-methyl-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)-phenol;

6-tert-Butyl-4-fluoro-3-methyl-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)-phenol; and

6-tert-Butyl-3-methyl-2-(5-trifluoromethanesulfonyl-1H-benzimidazol-2-yl)-phenol;

or a pharmaceutically acceptable salt thereof, or a hydrate of any of the foregoing.

6. A pharmaceutical composition comprising a compound according to claim 1 and a pharmaceutically acceptable carrier or diluent.

7. A pharmaceutical composition comprising a compound according to claim 4 and a pharmaceutically acceptable carrier or diluent.

8. A pharmaceutical composition comprising a compound according to claim 5 and a pharmaceutically acceptable carrier or diluent.

Assignments (3)
NOTICE OF RELEASE OF SECURITY INTEREST IN PATENTS FOR REEL/FRAME 030982/0793 Recorded Apr 7, 2014
From: M&F TTP HOLDINGS LLC
To: HIGH POINT PHARMACEUTICALS, LLC
Reel/Frame 032621/0867 →
SECURITY AGREEMENT Recorded Aug 9, 2013
From: HIGH POINT PHARMACEUTICALS, LLC
To: M&F TTP HOLDINGS LLC C/O MACANDREWS & FORBES HOLDINGS INC.
Reel/Frame 030982/0793 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 17, 2009
From: PETERSEN, ANDERS KLARSKOV; OLESEN, PREBEN HOULBERG; CHRISTIANSEN, LISE BROWN; HANSEN, HOLGER CLAUS; NIELSEN, FLEMMING ELMELUND
To: HIGH POINT PHARMACEUTICALS, LLC
Reel/Frame 023244/0713 →