Specimen collecting method and blade temperature estimating method
View Patent ↗In a specimen collecting method according to the present invention, a specimen is collected from a surface ( 114 a ) of a blade. An ultrasonic cutter having a cylindrical cutting blade is fed from the surface ( 114 a ) of the blade to a surface ( 110 a ) of a base material ( 100 ), and thus, a cylindrical incision is formed. After performing cutting to expand the incision outwardly, a rotating cutter ( 220 ) having a disc-shaped cutting blade ( 222 ) performs cutting inwardly from the cylindrical incision. Thus, a part ( 20 a ) situated inside the incision is cut away. The part ( 20 a ) becomes the specimen.
1. A specimen collecting method of collecting a specimen from a member whose surface is provided with a layer, the specimen collecting method comprising:
an incision forming step of forming a cylindrical incision by feeding a cylindrical cutter having a cylindrical cutting blade from the surface in the direction of thickness of the member to perform cutting; and
a specimen cutting away step of cutting away a specimen formed inside the incision by inwardly cutting the member from the cylindrical incision, the specimen collecting method further comprising an incision expanding step of cutting the member so that the incision is outwardly expanded after forming the cylindrical incision by cutting away an area located radially outward of an outer edge of the incision, wherein a rotating cutter having a disc-shaped cutting blade is inserted to the cylindrical incision to cut the member at the specimen cutting away step.
2. The specimen collecting method according to claim 1 , wherein
the member is a blade of a gas turbine,
a surface of the blade is formed by providing a layer of a thermal barrier coat on a base material,
the cylindrical cutter is fed until the cylindrical cutter comes in contact with the base material at the incision forming step, and
the rotating cutter cuts the base material at the specimen cutting away step.
3. The specimen collecting method according to claim 1 , wherein a plurality of incisions is formed so that the incisions partially overlap at the incision forming step.
4. A temperature estimating method of a blade in which a bond coat and a top coat are sequentially formed on a base material by using a specimen, which is obtained by the specimen collecting method comprising steps of an incision forming step of forming a cylindrical incision by feeding a cylindrical cutter having a cylindrical cutting blade from the surface in the direction of thickness of the member to perform cutting, wherein a plurality of incisions is formed so that the incisions partially overlap at the incision forming step; an incision expanding step of cutting the member so that the incision is outwardly expanded after forming the cylindrical incision, and a specimen cutting away step of cutting away a specimen formed inside the incision by inwardly cutting the member from the cylindrical incision, wherein a rotating cutter having a disc-shaped cutting blade is inserted to the cylindrical incision to cut the member at the specimen cutting away step, wherein
a relationship between a thickness and a temperature of an oxide scale layer of the blade, and time is obtained based on a test piece having a same composition as the blade, and then, by utilizing the relationship, a metal temperature of the blade is estimated based on the thickness of the oxide scale layer of the specimen obtained from the gas turbine.
5. A temperature estimating method of a blade formed with a top coat that is a ceramic layer on a base material by using a specimen, which is obtained by the specimen collecting method comprising steps of an incision forming step of forming a cylindrical incision by feeding a cylindrical cutter having a cylindrical cutting blade from the surface in the direction of thickness of the member to perform cutting, wherein a plurality of incisions is formed so that the incisions partially overlap at the incision forming step; an incision expanding step of cutting the member so that the incision is outwardly expanded after forming the cylindrical incision, and a specimen cutting away step of cutting away a specimen formed inside the incision by inwardly cutting the member from the cylindrical incision, wherein a rotating cutter having a disc-shaped cutting blade is inserted to the cylindrical incision to cut the member at the specimen cutting away step, wherein
an amount of a monoclinic crystal formed on the top coat of the obtained specimen is measured by X-ray diffraction method, and a surface temperature of the top coat is estimated based on the amount of the monoclinic crystal.