IP Library Granted Patent US 8,216,675
Granted Patent B2
US 8,216,675 · App. 12/563,352 · Granted Jul 10, 2012

Methods for producing sintered particles from a slurry of an alumina-containing raw material

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Quick Facts
Patent No.
US 8,216,675
App. No.
12/563,352
Granted
Jul 10, 2012
Kind
B2
Abstract

Sintered, substantially round and spherical particles prepared from a slurry of a calcined, uncalcined or partially calcined raw material having an alumina content of more than 55% by weight, and a mullite growth promoter in an amount of from about 2 to about 10% dry weight of the total solids in the slurry. The sintered particles are suitable for use as a propping agent or as a foundry media.

Claims (22)

1. A substantially round and spherical sintered particle comprising:

an alumina-containing seed; and

a coating, wherein the coating comprises at least about 80% of the total volume of the substantially round and spherical sintered particle;

wherein the coating is formed from a slurry that is sprayed onto the seed, the slurry is prepared form an alumina-containing raw material and iron oxide, wherein the raw material has an alumina content of greater than about 55% by weight, and wherein the slurry has an iron oxide content of from about 2 to about 10% by weight of total solids in the slurry; and

wherein the alumina content of the raw material is at least 10% greater than the alumina content of the seed.

2. The substantially round and spherical sintered particle of claim 1 , wherein the sintered comprising the alumina-containing seed and the coating has an alumina content of greater than about 55% by weight and an iron oxide content of from about 2 to about 10% by weight.

3. The substantially round and spherical sintered particle of claim 1 wherein the sintered particle has:

a specific gravity of from about 2.70 g/cm 3 to about 3.50 g/cm 3 ;

a bulk density of from about 1.55 g/cm 3 to about 1.95 g/cm 3 ;

a crush strength at 10,000 psi of from about 4 percent to about 7 percent; and

a short term conductivity at 10,000 psi of from about 3000 mD-ft to about 3800 mD-ft.

4. The substantially round and spherical sintered particle comprising:

an alumina-containing seed; and

a coating, wherein the coating comprises at least about 80% of the total volume of the substantially round and spherical sintered particle;

wherein the coating is formed from a slurry that is sprayed onto the seed, the slurry is prepared form an alumina-containing raw material and iron oxide, wherein the raw material has an alumina content of greater than about 55% by weight, and wherein the slurry has an iron oxide content of from about 2 to about 10% by weight of total solids in the slurry; and

wherein the alumina content of the raw material is at least 10% less than the alumina content of the seed.

5. The substantially round and spherical sintered particle of claim 4 , wherein the sintered comprising the alumina-containg seed and the coating has an alumina content of greater than about 55% by weight and an iron oxide content of from about 2 to about 10% by weight.

6. The substantially round and spherical sintered particle of claim 4 wherein the sintered particle has:

a specific gravity of from about 2.70 g/cm 3 to about 3.50 g/cm 3 ;

a bulk density of from about 1.55 g/cm 3 to about 1.95 g/cm 3 ;

a crush strength at 10,000 psi of from about 4 percent to about 7 percent; and

a short term conductivity at 10,000 psi of from about 3000 mD-ft to about 3800 mD-ft.

Assignments (3)
RELEASE OF SECURITY INTEREST Recorded Mar 3, 2017
From: WELLS FARGO BANK, NATIONAL ASSOCIATION
To: CARBO CERAMICS INC.; ASSET GUARD PRODUCTS INC. (F/K/A FALCON TECHNOLOGIES AND SERVICES, INC.); STRATAGEN, INC.
Reel/Frame 041879/0930 →
PATENT SECURITY AGREEMENT Recorded Apr 28, 2016
From: CARBO CERAMICS INC.; FALCON TECHNOLOGIES AND SERVICES, INC.; STRATAGEN, INC.
To: WELLS FARGO BANK, NATIONAL ASSOCIATION
Reel/Frame 038555/0688 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 20, 2009
From: PALAMARA, THOMAS C.; WILSON, BRETT ALLEN
To: CARBO CERAMICS INC.
Reel/Frame 023551/0671 →