IP Library Granted Patent US 8,094,783
Granted Patent B2
US 8,094,783 · App. 12/572,934 · Granted Jan 10, 2012

Method and system for performing materials analysis with reflected inelastic scatter

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Quick Facts
Patent No.
US 8,094,783
App. No.
12/572,934
Granted
Jan 10, 2012
Kind
B2
Abstract

A method for performing materials analysis of an object using an X-ray system includes generating an X-ray beam using an X-ray source having an anode and acquiring a scatter spectrum from Compton scatter produced when the X-ray beam interacts with the object. The scatter spectrum is acquired using an energy resolving detector. A Compton profile is extracted from the scatter spectrum by processing the scatter spectrum using a control system of the X-ray system. The Compton profile includes peaks at characteristic lines of the anode. The method further includes identifying a characteristic of a material of the object using the Compton profile, and outputting an indication of the characteristic of the material.

Claims (56)

1. A method for performing materials analysis of an object using an X-ray system, said method comprising:

generating an X-ray beam using an X-ray source having an anode;

acquiring a scatter spectrum from Compton scatter produced when the X-ray beam interacts with the object, the scatter spectrum acquired using an energy resolving detector;

extracting a Compton profile from the scatter spectrum by processing the scatter spectrum using a control system of the X-ray system, the Compton profile including peaks at characteristic lines of the anode;

identifying a characteristic of a material of the object using the Compton profile; and

outputting an indication of the characteristic of the material.

2. A method in accordance with claim 1 , wherein acquiring a scatter spectrum from Compton scatter comprises:

irradiating the object with a pencil beam;

collimating the Compton scatter to be a predetermined angle with respect to a direction of the pencil beam; and

recording the scatter spectrum of the Compton scatter at the predetermined angle using the energy resolving detector.

3. A method in accordance with claim 1 , wherein extracting a Compton profile comprises:

normalizing the scatter spectrum;

correcting the normalized scatter spectrum by removing a background signal from the normalized scatter spectrum; and

extracting the Compton profile from the normalized and corrected scatter spectrum.

4. A method in accordance with claim 3 , wherein normalizing the scatter spectrum comprises dividing a number of detected photons in each energy bin within a first predetermined range by a total number of detected photons summed over a plurality of energy bins within a second predetermined range that is different than the first predetermined range.

5. A method in accordance with claim 1 , wherein extracting a Compton profile comprises:

deconvolving the scatter spectrum;

removing a finite energy resolution of the energy resolving detector and a doublet structure of the characteristic lines of the anode from the scatter spectrum; and

yielding features of the scatter spectrum for material identification.

6. A method in accordance with claim 1 , wherein extracting a Compton profile comprises:

assuming a Compton profile for the acquired scatter spectrum;

synthesizing a simulated scatter spectrum from the assumed Compton profile;

comparing the simulated scatter spectrum with the acquired scattered spectrum to produce a difference signal;

iteratively correcting the assumed Compton profile using the difference signal to produce a corrected Compton profile; and

yielding features of the scatter spectrum for material identification based on the corrected Compton profile.

7. A method in accordance with claim 6 , wherein synthesizing a simulated scatter spectrum from the assumed Compton profile comprises superposing a predetermined number of Gaussian functions.

8. A method in accordance with claim 1 , wherein extracting a Compton profile comprises:

processing the scatter spectrum using a plurality of Gaussians, each Gaussian of the plurality of Gaussians including a peak amplitude and a width; and

yielding features of the scatter spectrum for material identification based on the peak amplitudes and the widths of the plurality of Gaussians.

9. An X-ray system for analyzing an object, said X-ray system comprising:

an X-ray source comprising an anode and at least one source focus, said X-ray source configured to generate an X-ray beam at said at least one source focus, said anode configured to generate characteristic lines;

an energy resolving detector positioned with respect to said at least one source focus, said energy resolving detector configured to record Compton scatter produced from the X-ray beam interacting with the object, the Compton scatter at an angle to a direction of the X-ray beam; and

a control system operationally coupled to said X-ray source and said energy resolving detector, said control system configured to:

acquire a scatter spectrum from the Compton scatter using said energy resolving detector;

extract a Compton profile from the scatter spectrum by processing the scatter spectrum, the Compton profile including peaks at the characteristic lines of said anode; and

identify a characteristic of a material of the object using the Compton profile.

10. An X-ray system in accordance with claim 9 , further comprising a primary collimator configured to produce sequentially a plurality of pencil beams from a source focus to scan the object.

11. An X-ray system in accordance with claim 9 , further comprising a secondary collimator configured to collimate the Compton scatter to be at the angle for detection by said energy resolving detector.

12. An X-ray system in accordance with claim 9 , wherein said anode comprises a tungsten (W) anode that generates a W Kα1 line and a W Kα2 line as the characteristic lines.

13. An X-ray system in accordance with claim 9 , wherein said energy resolving detector comprises a Schottky contacted cadmium telluride (CdTe) detector configured to provide energy resolutions of about 1% full width at half maximum (FWHM) at 60 kilo-electronvolts (keV).

14. An X-ray system in accordance with claim 9 , wherein said energy resolving detector comprises a semiconductor detector configured to provide an energy resolution greater than 2% FWHM at 60 keV.

15. An X-ray system in accordance with claim 9 , wherein a Z-axis of said X-ray system defines an axis of symmetry, said at least one source focus and said energy resolving detector positioned on said axis of symmetry.

16. An X-ray system in accordance with claim 9 , further comprising:

an axis of symmetry; and

a primary collimator configured to produce a pencil beam at said at least source focus, said primary collimator rotationally symmetric about said axis of symmetry.

17. An X-ray system in accordance with claim 9 , further comprising:

an axis of symmetry; and

a secondary collimator configured to collimate the Compton scatter to be at the angle, said secondary collimator rotationally symmetric about said axis of symmetry.

18. An X-ray system in accordance with claim 9 , wherein the angle is at least 150°.

19. An X-ray system in accordance with claim 9 , wherein said control system is further configured to:

normalize the scatter spectrum;

correct the normalized scatter spectrum by removing a background signal from the normalized scatter spectrum; and

extract the Compton profile from the normalized and corrected scatter spectrum.

20. An X-ray system in accordance with claim 9 , wherein said control system is further configured to:

process the scatter spectrum using a plurality of Gaussians, each Gaussian of the plurality of Gaussians including a peak amplitude and a width; and

yield features of the scatter spectrum for material identification based on the peak amplitudes and the widths of the plurality of Gaussians.

Assignments (7)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 6, 2025
From: SMITHS DETECTION INC.
To: SMITHS DETECTION GERMANY GMBH
Reel/Frame 073508/0846 →
CHANGE OF NAME Recorded Oct 30, 2025
From: MORPHO DETECTION, LLC
To: SMITHS DETECTION, LLC
Reel/Frame 073411/0553 →
MERGER Recorded Oct 30, 2025
From: SMITHS DETECTION, LLC
To: SMITHS DETECTION INC.
Reel/Frame 073406/0059 →
CORRECTIVE ASSIGNMENT TO CORRECT THE THE PURPOSE OF THE CORRECTION IS TO ADD THE CERTIFICATE OF CONVERSION PAGE TO THE ORIGINALLY FILED CHANGE OF NAME DOCUMENT PREVIOUSLY RECORDED ON REEL 032122 FRAME 67. ASSIGNOR(S) HEREBY CONFIRMS THE THE CHANGE OF NAME. Recorded Mar 19, 2014
From: MORPHO DETECTION, INC.
To: MORPHO DETECTION, LLC
Reel/Frame 032470/0682 →
CHANGE OF NAME Recorded Jan 24, 2014
From: MORPHO DETECTION, INC.
To: MORPHO DETECTION, LLC
Reel/Frame 032122/0067 →
CHANGE OF NAME Recorded Mar 15, 2010
From: GE HOMELAND PROTECTION, INC.
To: MORPHO DETECTION, INC.
Reel/Frame 024081/0129 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 2, 2009
From: HARDING, GEOFFREY
To: GE HOMELAND PROTECTION, INC.
Reel/Frame 023322/0372 →