IP Library Granted Patent US 8,124,633
Granted Patent B2
US 8,124,633 · App. 12/593,168 · Granted Feb 28, 2012

Hydroxymethyl ether hydroisoindoline tachykinin receptor antagonists

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Quick Facts
Patent No.
US 8,124,633
App. No.
12/593,168
Granted
Feb 28, 2012
Kind
B2
Abstract

The present invention is directed to certain hydroxymethyl ether hydroisoindoline compounds which are useful as neurokinin-1 (NK-1) receptor antagonists, and inhibitors of tachykinin and in particular substance P. The invention is also concerned with pharmaceutical formulations comprising these compounds as active ingredients and the use of the compounds and their formulations in the treatment of certain disorders, including emesis, urinary incontinence, LUTS, depression, and anxiety.

Claims (62)

1. A compound of the formula I:

or a pharmaceutically acceptable salt thereof and individual enantiomers and diastereomers thereof wherein: R 1 is

X is independently selected from the group consisting of:

(1) hydrogen, and

(2) fluorine;

Y is independently selected from the group consisting of:

(1) hydrogen, and

(2) methyl; and

Z is independently selected from the group consisting of:

(1) hydrogen,

(2) C 1-6 alkyl, which is unsubstituted or substituted with halogen, hydroxyl or phenyl,

(3) —(CO)—C 1-6 alkyl,

(4) —(CO)-Aryl

(5) —(CO)O—C 1-6 alkyl,

(6) —(CO)—NH 2 ,

(7) —(CO)—NHC 1-6 alkyl, and

(8) —(CO)—N(C 1-6 alkyl)(C 1-6 alkyl).

2. The compound of claim 1 of the formula Ia or Ib:

or a pharmaceutically acceptable salt thereof and individual enantiomers and diastereomers thereof.

3. The compound of claim 2 of the formula Ia:

or a pharmaceutically acceptable salt thereof and individual enantiomers and diastereomers thereof.

4. The compound of claim 2 of the formula Ib:

or a pharmaceutically acceptable salt thereof and individual enantiomers and diastereomers thereof.

5. The compound of claim 1 wherein Z is selected from the group consisting of

(1) hydrogen,

(2) C 1-3 alkyl, which is unsubstituted or substituted with halogen, hydroxyl or phenyl,

(3) —(CO)-phenyl, and

(4) —(CO)O-methyl.

6. The compound of claim 1 wherein X is hydrogen.

7. The compound of claim 1 wherein X is fluorine.

8. The compound of claim 1 wherein Y is hydrogen.

9. The compound of claim 1 wherein Y is methyl.

10. The compound of claim 1 wherein Z is hydrogen.

11. The compound of claim 1 wherein Z is methyl.

12. The compound of claim 1 of the formula Ia or Ib:

or a pharmaceutically acceptable salt thereof and individual enantiomers and diastereomers thereof wherein

R 1 is

X is independently selected from the group consisting of:

(1) hydrogen, and

(2) fluorine;

Y is independently selected from the group consisting of:

(1) hydrogen, and

(2) methyl; and

Z is independently selected from the group consisting of:

(1) hydrogen,

(2) C 1-6 alkyl, which is unsubstituted or substituted with halogen, hydroxyl or phenyl,

(3) —(CO)—C 1-6 alkyl,

(4) —(CO)-Aryl

(5) —(CO)O—C 1-6 alkyl, and

(6) —(CO)—NH 2 .

13. A compound of claim 12 wherein Z is selected from the group consisting of

(1) hydrogen,

(2) C 1-3 alkyl, which is unsubstituted or substituted with halogen, hydroxyl or phenyl,

(3) —(CO)-phenyl, and

(4) —(CO)O-methyl.

14. A compound of claim 12 wherein Z is selected from hydrogen and methyl.

15. A compound which is selected from the group consisting of:

and pharmaceutically acceptable salts thereof.

16. A pharmaceutical composition which comprises an inert carrier and a compound of claim 1 .

17. A method for the treatment of pain or inflammation, migraine, emesis, post-therapeutic neuralgia, depression, anxiety or urinary incontinence, and LUTS which method comprises administration to a patient in need thereof a therapeutically effective amount of the compound of claim 1 .

18. A method according to claim 17 for the treatment of urinary incontinence or LUTS.

19. A method of antagonizing the effect of substance P at its receptor site or for the blockade of neurokinin-1 receptors in a patient in need thereof comprising administration to said patient a therapeutically effective amount of the compound of claim 1 .

Assignments (6)
RELEASE OF SECURITY INTEREST Recorded Sep 20, 2021
From: PERCEPTIVE CREDIT HOLDINGS II, LP
To: VYNE THERAPEUTICS INC. (F/K/A MENLO THERAPEUTICS INC. AND SUCCESSOR-IN-INTEREST TO VYNE PHARMACEUTICALS LTD., F/K/A FOAMIX PHARMACEUTICALS LTD.)
Reel/Frame 057531/0986 →
PATENT SECURITY AGREEMENT Recorded Mar 9, 2020
From: MENLO THERAPEUTICS INC.
To: PERCEPTIVE CREDIT HOLDINGS II, LP
Reel/Frame 052130/0980 →
CHANGE OF NAME Recorded Aug 29, 2012
From: SCHERING CORPORATION
To: MERCK SHARP & DOHME CORP.
Reel/Frame 028866/0511 →
MERGER Recorded Aug 27, 2012
From: MERCK SHARP & DOHME CORP.
To: SCHERING CORPORATION
Reel/Frame 028850/0515 →
CHANGE OF NAME Recorded Jan 27, 2010
From: MERCK & CO., INC.
To: MERCK SHARP & DOHME CORP.
Reel/Frame 023852/0595 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 5, 2009
From: DEVITA, ROBERT J.; MILLS, SANDER G.; JIANG, JINLONG; KASSICK, ANDREW J.; BAO, JIANMING
To: MERCK & CO., INC.
Reel/Frame 023473/0061 →