IP Library Granted Patent US 8,173,849
Granted Patent B2
US 8,173,849 · App. 12/596,711 · Granted May 8, 2012

Therapeutic compounds

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Quick Facts
Patent No.
US 8,173,849
App. No.
12/596,711
Granted
May 8, 2012
Kind
B2
Abstract

A (−)-stereoisomer of formula (I): (formula I), wherein X is H or F; or a pharmaceutically acceptable salt or prodrug thereof, is useful as an anesthetic.

Claims (47)

1. A (−)-stereoisomer of formula (I):

wherein X is H or F; or a salt or prodrug thereof.

2. A compound as claimed in claim 1 , which is a (−)-stereoisomer of formula (I) or a pharmaceutically acceptable salt or prodrug thereof.

3. A compound as claimed in claim 2 , which is a (−)-stereoisomer of formula (I) or a pharmaceutically acceptable salt thereof.

4. A compound as claimed in claim 1 , in which X is H.

5. A pharmaceutical composition comprising a compound as claimed in claim 2 , and a pharmaceutically acceptable carrier.

6. The pharmaceutical composition of claim 5 which is formulated for intravenous administration.

7. The pharmaceutical composition of claim 6 which is formulated as a lipid emulsion.

8. A method for inducing or maintaining general anesthesia in an animal comprising administering to the animal an effective amount of a (−)-stereoisomer of formula (I):

wherein X is H or F; or a pharmaceutically acceptable salt or prodrug thereof.

9. A method as claimed in claim 8 , in which X is H.

10. A method as claimed in claim 8 , comprising administering to the animal an effective amount of a (−)-stereoisomer of formula (I) in which X is H, or a pharmaceutically acceptable salt thereof.

11. A method for promoting sedation in an animal comprising administering to the animal an effective amount of a (−)-stereoisomer of formula (I):

wherein X is H or F; or a pharmaceutically acceptable salt or prodrug thereof.

12. A method as claimed in claim 11 , in which X is H.

13. A method as claimed in claim 11 , comprising administering to the animal an effective amount of a (−)-stereoisomer of formula (I) in which X is H, or a pharmaceutically acceptable salt thereof.

14. A process for preparing a (−)-stereoisomer of formula (I)

wherein X is H of F; or a salt or prodrug thereof, which comprises

(a) hydrolysing a carbamic acid (−)-2-sec-butyl-6-isopropylphenyl ester diastereomer of formula:

in which R 1 represents a chiral amino group;

(b) diazotizing a corresponding (−)-2-sec-butyl-6-isopropyl aniline of formula

or

(c) reducing a corresponding 2-(1-methylallyl)-6-isopropylphenol of formula

followed if required by forming the free phenol or salt or pro-drug thereof.

15. A carbamic acid (−)-2-sec-butyl-6-isopropylphenyl ester diastereoisomer of formula

in which R 1 represents a chiral amino group, and in which X is H or F.

16. A diastereoisomer as claimed in claim 15 , which R 1 represents an (R)-1-arylethylamino group.

17. A compound as claimed in claim 2 , in which X is H.

18. A compound as claimed in claim 3 , in which X is H.

19. A method for inducing or maintaining general anesthesia in an animal comprising administering to the animal an effective amount of a compound of claim 3 .

20. The method of claim 19 , wherein X is H.

21. A method for promoting sedation in an animal comprising administering to the animal an effective amount of a compound of claim 3 .

22. The method of claim 21 , wherein X is H.

23. The process of claim 14 , wherein X is H.

24. The process of claim 14 , wherein the method comprises forming the free phenol or salt or pro-drug thereof.

25. The process of claim 24 , wherein X is H.

26. The process of claim 24 , wherein the method comprises forming the free phenol or pharmaceutically acceptable salt or pro-drug thereof.

27. The process of claim 26 , wherein X is H.

28. The process of claim 26 , wherein the method comprises forming the free phenol or pharmaceutically acceptable salt.

29. The process of claim 28 , wherein X is H.

30. The pharmaceutical composition of claim 5 , wherein X is H.

31. A pharmaceutical composition comprising a compound of formula (I):

wherein the compound is a (−)-stereoisomer of formula (I) and wherein X is H or F; or a pharmaceutically acceptable salt thereof and a pharmaceutically acceptable carrier.

32. The pharmaceutical composition of claim 31 , wherein X is H.

33. The pharmaceutical composition of claim 31 , which is formulated for intravenous administration.

34. The pharmaceutical composition of claim 33 , which is formulated as a lipid emulsion.

35. The process of claim 14 , wherein the salt is a pharmaceutically acceptable salt.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 2, 2014
From: SIGNATURE THERAPEUTICS, INC.
To: SOWOOD HEALTHCARE LLC
Reel/Frame 033011/0017 →
CHANGE OF NAME Recorded Apr 2, 2012
From: PHARMACOFORE, INC.
To: SIGNATURE THERAPEUTICS, INC.
Reel/Frame 027976/0060 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 28, 2010
From: JENKINS, THOMAS E.
To: PHARMACOFORE, INC.
Reel/Frame 024605/0084 →