Glass-cell vial for examining slight amount of specimen
View Patent ↗A glass-cell vial is provided which can examine specimen without causing any hindrance even when as minimum as possible specimen is used, and prevents mixture of foreign substances from causing examination errors. A vial is provided which comprises function of cell capable of optical examination, and the inner surface of bottom of the vial is formed to be a round-state convex part upwardly and the outer surface of the bottom is formed to be in convex state. When a small amount of liquid specimen is introduced into this cell vial, a part which can be a light irradiation part for optical examination can be positioned between the meniscus part of the liquid specimen and the upper end of the inner bottom. Consequently, it becomes possible to examine light quantity variation even though the specimen is in small amount.
1. A manufacturing method of a glass tube for examining a specimen, comprising the steps of:
holding a slender glass tube formed with an opening at a lower end of the glass tube for examining a specimen in the upright state;
heating an upper end of the glass tube for examining a specimen with a burner while simultaneously rotating the glass tube for examining a specimen, and collecting melted glass at a central part of the upper end of the glass tube for examining a specimen to form a bottom of the glass tube for examining a specimen to be in a convex state upwardly or downwardly, and while simultaneously blowing in compressed air from the opening at the lower end of the glass tube for examining a specimen;
varying the compressed air pressure so that an inner surface of the bottom of the glass tube for examining a specimen is formed to be a round-state convex part in a direction toward the opening at the lower end of the glass tube for examining a specimen, and an outer surface of the bottom of the glass tube for examining a specimen is formed to be in convex state in an opposite direction from the inner surface of the bottom of the glass tube for examining a specimen; and
filling the glass tube for examining a specimen with a small quantity of reagent.
2. The manufacturing method according to claim 1 , comprising the steps of:
manufacturing the glass tube for examining a specimen having a thin bottom, a thin bottom being a bottom having a thickness equivalent to the thickness of an outer peripheral of the glass tube for examining a specimen, by heating with a burner and collecting melted glass at the central part of the upper end of the glass tube for examining a specimen; and
subsequently, heating with a burner again to melt glass at the central part of the upper end of the glass tube for examining a specimen to form a thick bottom glass tube for examining a specimen, a thick bottom being a bottom having a thickness of 1.3 to 2 times that of the thin bottom, so that the inner surface of the bottom of the glass tube for examining a specimen is formed to be a round-state convex part in the direction toward the opening at the lower end of the glass tube for examining a specimen, and the outer surface of the bottom of the glass tube for examining a specimen is formed to be in a convex state in the opposite direction from the inner surface of the bottom of the glass tube for examining a specimen.
3. The manufacturing method according to claim 1 , comprising the step of
forming the outer surface of the bottom of the glass tube for examining a specimen to be a round-state convex part in the opposite direction from the inner surface of the bottom of the glass tube for examining a specimen.