IP Library Granted Patent US 9,303,502
Granted Patent B2
US 9,303,502 · App. 12/606,464 · Granted Apr 5, 2016

Method of controlling water production through treating particles with RPMS

View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 9,303,502
App. No.
12/606,464
Granted
Apr 5, 2016
Kind
B2
Abstract

Water production from a subterranean formation is inhibited or controlled by pumping a fluid containing coated particles through a wellbore into the formation. The particles have been previously coated with a relative permeability modifier (RPM). Upon contact with water, the RPM coating expands or swells and inhibits and controls the production of water. The RPM may be a water hydrolyzable polymer having a weight average molecular weight greater than 100,000. The particles may be conventional proppants or gravel.

Claims (23)

1. A method of controlling water production from a subterranean formation comprising:

introducing particles coated with a relative permeability modifier (RPM) into a subterranean formation through a wellbore, where the RPM is a crosslinked water hydrolyzable polymer having a weight average molecular weight greater than 100,000, and where the particles are selected from the group consisting of glass beads, ceramic beads, metal beads, bauxite grains, walnut shell fragments, aluminum pellets, nylon pellets and combinations thereof; wherein the crosslinked water hydrolyzable polymer is selected from the group consisting of:

crosslinked polysiloxanes, copolymers of vinylamide monomers and monomers containing ammonium or quaternary ammonium moieties; and

copolymers of vinylamide monomers and monomers comprising vinylcarboxylic acid monomers and/or vinylsulfonic acid monomers, and salts thereof, and wherein these vinyl amide copolymers comprise a crosslinking monomer selected from the group consisting of diallylamine, N,N-diallylacrylamide, divinyloxyethane, and divinyldimethylsilane; and

contacting the coated particles with water, causing swelling of the RPM thereby inhibiting water flow.

2. The method of claim 1 further comprising coating the particles with the RPM to form coated particles and mixing the coated particles with a carrier fluid prior to introducing the particles into the subterranean formation.

3. The method of claim 1 where the RPM loading ranges from one pound of RPM per about 100 to about 5000 pounds of particles (1 kilogram of RPM per about 100 to about 5000 kilograms of particles).

4. The method of claim 1 where the particles range in size from about 10 mesh to about 200 mesh (from about 2000 microns to about 75 microns).

5. The method of claim 1 wherein the method further comprises coating the particles with the RPM, wherein coating the particles with the RPM comprises:

at least partially hydrolyzing the RPM in a liquid selected from the group consisting of water, brine, glycol, ethanol and mixtures thereof;

contacting the particles with the liquid; and

at least partially vaporizing the liquid.

6. A method of controlling water production from a subterranean formation comprising:

introducing particles coated with a relative permeability modifier (RPM) into a subterranean formation through a wellbore where the particles range in size from about 10 mesh to about 200 mesh (from about 2000 microns to about 75 microns), where the RPM loading ranges from one pound of RPM per about 100 to about 5000 pounds of particles (1 kilogram of RPM per about 100 to about 5000 kilograms of particles), where the RPM is a crosslinked water hydrolyzable polymer and where the particles are selected from the group consisting of glass beads, ceramic beads, metal beads, bauxite grains, walnut shell fragments, aluminum pellets, nylon pellets and combinations thereof; wherein the crosslinked water hydrolyzable polymer is selected from the group consisting of:

crosslinked polysiloxanes; and

copolymers of vinylamide monomers and monomers containing ammonium or quaternary ammonium moieties, copolymers of vinylamide monomers and monomers comprising vinylcarboxylic acid monomers and/or vinylsulfonic acid monomers, and salts thereof, and wherein these vinyl amide copolymers comprise a crosslinking monomer selected from the group consisting of-diallylamine, N,N-diallylacrylamide, divinyloxyethane, and divinyldimethylsilane; and

contacting the coated particles with water, causing swelling of the RPM thereby inhibiting water flow;

wherein the method further comprises coating the particles with the RPM, wherein coating the particles with the RPM comprises:

at least partially hydrolyzing the RPM in a liquid selected from the group consisting of water, brine, glycol, ethanol and mixtures thereof;

contacting the particles with the liquid; and

at least partially vaporizing the liquid.

7. The method of claim 6 further comprising mixing the coated particles with a carrier fluid prior to introducing the particles into the subterranean formation.

8. The method of claim 6 where the crosslinked water hydrolyzable polymer has a weight average molecular weight greater than 100,000.

Assignments (3)
CHANGE OF NAME Recorded Mar 8, 2022
From: BAKER HUGHES, A GE COMPANY, LLC
To: BAKER HUGHES HOLDINGS LLC
Reel/Frame 059338/0944 →
CHANGE OF NAME Recorded Feb 16, 2022
From: BAKER HUGHES INCORPORATED
To: BAKER HUGHES, A GE COMPANY, LLC
Reel/Frame 059126/0123 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 18, 2009
From: HUANG, TIANPING; CREWS, JAMES B.; WILLINGHAM, JOHN R.
To: BAKER HUGHES INCORPORATED
Reel/Frame 023536/0719 →