IP Library Granted Patent US 8,703,527
Granted Patent B2
US 8,703,527 · App. 12/623,364 · Granted Apr 22, 2014

Photovoltaic devices including copper indium gallium selenide

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Quick Facts
Patent No.
US 8,703,527
App. No.
12/623,364
Granted
Apr 22, 2014
Kind
B2
Abstract

A copper indium gallium selenide photovoltaic cell can include a substrate having a transparent conductive oxide layer. The copper indium gallium selenide can be deposited using sputtering and vapor transport deposition.

Claims (41)

1. A method of manufacturing a photovoltaic device comprising:

sequentially forming a plurality of material layers over a substrate by:

depositing by sputtering a first layer including copper, indium and gallium over the substrate;

depositing by vapor transport deposition a selenium layer over and in direct contact with the first layer including copper, indium and gallium to form a selenium layer directly over the first layer including copper, indium, and gallium;

depositing by sputtering a second layer including copper, indium and gallium over and in direct contact with the selenium layer directly over the first layer including copper, indium and gallium; and

depositing by vapor transport deposition a selenium layer over and in direct contact with the second layer including copper, indium and gallium to form a second selenium layer directly over the second layer including copper, indium and gallium.

2. The method of claim 1 , wherein the substrate comprises glass.

3. The method of claim 1 , further comprising:

depositing a transparent conductive layer over the substrate prior to the sequentially forming of a plurality of material layers.

4. The method of claim 3 , wherein the transparent conductive layer is a transparent conductive oxide layer.

5. The method of claim 4 , wherein the transparent conductive oxide layer is indium tin oxide.

6. The method of claim 1 , wherein the sequentially forming of a plurality of material layers includes forming at least 4 pairs of a selenium layer directly over a layer including copper, indium, and gallium, wherein each pair of layers is formed over and in direct contact with a respective pair of a selenium layer formed directly over a layer including copper, indium, and gallium.

7. The method of claim 1 , wherein the sequentially forming of a plurality of material layers includes forming at least 9 pairs of a selenium layer directly over a layer including copper, indium, and gallium, wherein each pair of layers is formed over and in direct contact with a respective pair of a selenium layer formed directly over a layer including copper, indium, and gallium.

8. The method of claim 1 , further comprising:

depositing a plurality of additional layers including copper, indium, and gallium over the substrate; and

depositing selenium over and in direct contact with each of the plurality of additional layers.

9. A method of manufacturing a photovoltaic device comprising:

depositing by sputtering a first layer including copper, indium and gallium over a substrate;

combining a carrier gas and selenium;

heating the carrier gas and selenium combination to form a heating vapor;

passing the heated vapor through a permeable membrane;

depositing a selenium layer from the vapor over and in direct contact with the first layer including copper, indium and gallium;

depositing by sputtering a second layer including copper, indium and gallium over and in direct contact with the selenium layer directly over the first layer including copper, indium and gallium; and

depositing a selenium layer over and in direct contact with the second layer including copper, indium and gallium.

10. The method of claim 9 , further comprising depositing a transparent conductive layer over the substrate prior to the depositing the first layer including copper, indium and gallium.

11. The method of claim 10 , wherein the transparent conductive layer is a transparent conductive oxide layer.

12. The method of claim 11 , wherein the transparent conductive oxide layer is indium tin oxide.

13. A method of manufacturing a photovoltaic device comprising:

depositing by sputtering a first layer including copper, indium and gallium over a substrate; and

depositing by vapor transport deposition a selenium layer over and in direct contact with the first layer including copper, indium and gallium to form a first selenium layer directly over the first layer including copper, indium and gallium,

wherein the first layer including copper, indium and gallium is no more than about 0.1 micron thick;

depositing by sputtering a second layer including copper, indium and gallium over and in direct contact with the first selenium layer directly over the first layer including copper, indium and gallium, the second layer being no more than about 0.1 micron thick; and

depositing by vapor transport deposition a second selenium layer over and in direct contact with the second layer including copper, indium and gallium.

14. The method of claim 13 , wherein deposition of selenium comprising:

combining a carrier gas and selenium;

heating the carrier gas and selenium combination to form a heated vapor;

passing the heated vapor through a permeable membrane, and

depositing the selenium from the vapor over and in direct contact with the first and second layers including copper, indium and gallium.

15. The method of claim 13 , further comprising:

depositing a plurality of additional layers including copper, indium, and gallium over the substrate; and

depositing selenium over and in direct contact with each of the plurality of additional layers.

Assignments (3)
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENT RIGHTS Recorded Nov 15, 2021
From: JPMORGAN CHASE BANK, N.A.
To: FIRST SOLAR, INC.
Reel/Frame 058132/0261 →
CORRECTIVE ASSIGNMENT TO CORRECT THE PATENT APPLICATION 13/895113 ERRONEOUSLY ASSIGNED BY FIRST SOLAR, INC. TO JPMORGAN CHASE BANK, N.A. ON JULY 19, 2013 PREVIOUSLY RECORDED ON REEL 030832 FRAME 0088. ASSIGNOR(S) HEREBY CONFIRMS THE CORRECT PATENT APPLICATION TO BE ASSIGNED IS 13/633664. Recorded Sep 19, 2014
From: FIRST SOLAR, INC.
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 033779/0081 →
SECURITY AGREEMENT Recorded Jul 19, 2013
From: FIRST SOLAR, INC.
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 030832/0088 →