IP Library Granted Patent US 8,419,948
Granted Patent B2
US 8,419,948 · App. 12/623,435 · Granted Apr 16, 2013

Wastewater treatment

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Quick Facts
Patent No.
US 8,419,948
App. No.
12/623,435
Granted
Apr 16, 2013
Kind
B2
Abstract

A method for treating wastewater treats wastewater. In an embodiment, the method for treating wastewater includes treating wastewater comprising a chemical oxygen demand. The method includes dissolving an iron compound in the wastewater. The method also includes adjusting the pH of the wastewater to reduce the chemical oxygen demand of the wastewater.

Claims (21)

1. A method for treating wastewater, wherein the wastewater comprises a chemical oxygen demand, comprising:

(A) dissolving an iron compound in the wastewater, the wastewater comprising dimethylalkylamine-N-oxide;

(B) adjusting the pH of the wastewater to precipitate an insoluble iron composition comprising hydrated iron oxides; and

(C) reacting the iron composition with the dimethylalkylamine-N-oxide in the wastewater to reduce the chemical oxygen demand of the wastewater and provide a reduced chemical oxygen demand wastewater.

2. The method of claim 1 , further comprising reducing the chemical oxygen demand of the reduced chemical oxygen wastewater to less than about 300 milligrams/liter.

3. The method of claim 1 , further comprising reducing the chemical oxygen demand of the reduced chemical oxygen wastewater to less than about 100 milligrams/liter.

4. The method of claim 1 , further comprising reducing the chemical oxygen demand of the reduced chemical oxygen demand wastewater to less than about 50 milligrams/liter.

5. The method of claim 1 , wherein the dimethylalkylamine-N-oxide comprises an alkyl component, and wherein the alkyl component comprises C 6 to C 18 .

6. The method of claim 1 , wherein the iron compound comprises a soluble iron salt.

7. The method of claim 1 , wherein the iron compound comprises ferrous sulfate, ferric ammonium sulfate, ferrous ammonium sulfate, ferric chloride, ferric sulfate, a soluble ferrous salt, a soluble ferric salt, or any combinations thereof.

8. The method of claim 1 , wherein the iron compound comprises ferric ammonium sulfate.

9. The method of claim 1 , further comprising adding from about 1 gram/liter to about 5 grams/liter of the iron compound to the wastewater.

10. The method of claim 1 , wherein the iron compound comprises a soluble ferrous salt, a soluble ferric salt, or any combinations thereof.

11. The method of claim 1 , wherein adjusting the pH comprises increasing the pH of the wastewater to a pH from about 5 to about 9.

12. The method of claim 1 , wherein adjusting the pH comprises increasing the pH of the wastewater to a pH from about 7 to about 9.

13. The method of claim 1 , wherein adjusting the pH comprises adding trisodium phosphate, ammonia, sodium bicarbonate, borax, sodium carbonate, or any combination thereof to the wastewater.

14. The method of claim 1 , wherein adjusting the pH comprises adding sodium bicarbonate to the wastewater.

15. The method of claim 1 , further comprising heating the wastewater.

16. The method of claim 15 , wherein heating the wastewater comprises heating the wastewater to temperatures from about 50° C. to about 100° C.

17. The method of claim 15 , wherein heating the wastewater comprises heating the wastewater to temperatures from about 50° C. to about 60° C.

18. The method of claim 15 , wherein heating the wastewater comprises adding heat for about 3 hours to about 6 hours.

Assignments (8)
MERGER Recorded Mar 15, 2025
From: CR3 ZYMEFLOW, INC.
To: ZYMEFLOW, INC.
Reel/Frame 070523/0169 →
MERGER Recorded Mar 13, 2025
From: TRISTAR GLOBAL ENERGY SOLUTIONS, INC.
To: CR3 ZYMEFLOW, INC.
Reel/Frame 070508/0396 →
MERGER Recorded Mar 12, 2025
From: UNITED LABORATORIES INTERNATIONAL, LLC
To: TRISTAR GLOBAL ENERGY SOLUTIONS, INC.
Reel/Frame 070491/0243 →
RELEASE OF SECURITY INTEREST Recorded Sep 8, 2023
From: ABACUS FINANCE GROUP LLC
To: UNITED LABORATORIES INTERNATIONAL LLC
Reel/Frame 064839/0568 →
SECURITY INTEREST Recorded Jan 5, 2015
From: UNITED LABORATORIES INTERNATIONAL, LLC; GLOBAL VAPOR CONTROL, INC.
To: ABACUS FINANCE GROUP, LLC, AS AGENT
Reel/Frame 034631/0429 →
RELEASE OF SECURITY INTEREST Recorded Jan 5, 2015
From: TEXAS CAPITAL BANK, NATIONAL ASSOCIATION
To: UNITED LABORATORIES INTERNATIONAL, LLC
Reel/Frame 034634/0719 →
SECURITY AGREEMENT Recorded Oct 2, 2013
From: UNITED LABORATORIES INTERNATIONAL, LLC
To: TEXAS CAPITAL BANK, NATIONAL ASSOCIATION
Reel/Frame 031327/0650 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 24, 2010
From: FROST, JACK G.
To: UNITED LABORATORIES INTERNATIONAL, LLC
Reel/Frame 023836/0752 →