IP Library Granted Patent US 9,101,536
Granted Patent B2
US 9,101,536 · App. 12/643,890 · Granted Aug 11, 2015

Biocompatible phase invertable proteinaceous compositions and methods for making and using the same

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Quick Facts
Patent No.
US 9,101,536
App. No.
12/643,890
Granted
Aug 11, 2015
Kind
B2
Abstract

Biocompatible phase invertible proteinaceous compositions and methods for making and using the same are provided. The subject phase invertible compositions are prepared by combining a proteinaceous substrate and a crosslinking agent, such as a stabilized aldehyde crosslinking agent. Also provided are kits for use in preparing the subject compositions. The subject compositions, kits and systems find use in a variety of different applications.

Claims (27)

1. A method of sealing a body site of a subject in need thereof, comprising the step of applying a composition comprising a stabilized dialdehyde crosslinker and a proteinaceous substrate to said site, wherein the dialdehyde has been stabilized by heating it to a temperature ranging from 40 to 60° C. for a period of time ranging from 1 to 20 days.

2. The method according to claim 1 , wherein the dialdehyde is heat treated glutaraldehyde.

3. The method according to claim 1 , wherein the composition comprises molecules described by the following formula:

wherein R1 and R2 are H or hydrocarbon moieties which are polymerization products produced by sequential aldol reaction and dehydration of one or more glutaraldehyde molecules.

4. The method according to claim 1 , wherein the site is an arterial vessel.

5. The method according to claim 1 , wherein the site is an organ.

6. The method according to claim 1 , wherein the site comprises connective tissue.

7. The method according to claim 6 , wherein the connective tissue comprises tissue selected from the group consisting of ligaments, tendons and bone.

8. The method according to claim 1 , wherein the subject is a mammal.

9. The method according to claim 8 , wherein the mammal is a human.

10. The method according to claim 1 , wherein the mammal is from an ungulate.

11. The method according to claim 10 , wherein the ungulate is selected from the group consisting of cows, pigs, sheep and horses.

12. The method according to claim 1 , wherein said composition is at an amount of from 1 to 100 ml.

13. A method of sealing an arterial vessel of a subject in need thereof, comprising the step of applying a composition comprising a stabilized dialdehyde crosslinker and a proteinaceous substrate to said arterial vessel, wherein the dialdehyde has been stabilized by heating it to a temperature ranging from 40 to 60° C. for a period of time ranging from 1 to 20 days.

14. The method according to claim 13 , wherein the dialdehyde is heat treated glutaraldehyde.

15. The method according to claim 13 , wherein the composition comprises molecules described by the following formula:

wherein R1 and R2 are H or hydrocarbon moieties which are polymerization products produced by sequential aldol reaction and dehydration of one or more glutaraldehyde molecules.

16. The method according to claim 13 , wherein said composition is at an amount of from 1 to 100 ml.

17. A method of sealing mammalian tissue of a subject in need thereof, comprising the step of applying a composition comprising a stabilized dialdehyde crosslinker and a proteinaceous substrate onto said mammalian tissue, wherein the dialdehyde has been stabilized by heating it to a temperature ranging from 40 to 60° C. for a period of time ranging from 1 to 20 days.

18. The method according to claim 17 , wherein the dialdehyde is heat treated glutaraldehyde.

19. The method according to claim 17 , wherein the composition comprises molecules described by the following formula:

wherein R1 and R2 are H or hydrocarbon moieties which are polymerization products produced by sequential aldol reaction and dehydration of one or more glutaraldehyde molecules.

20. The method according to claim 17 , wherein said composition is at an amount of from 1 to 100 ml.

21. The method according to claim 17 , wherein the tissue is an organ.

22. The method according to claim 17 , wherein the mammal is a human.

23. The method according to claim 17 , wherein the mammal is an ungulate.

24. The method according to claim 23 , wherein the ungulate is selected from the group consisting of cows, pigs, sheep and horses.

Assignments (6)
RELEASE OF PATENT SECURITY INTERESTS RECORDED AT REEL 043596, FRAME 0259 Recorded Nov 16, 2023
From: DEUTSCHE BANK AG NEW YORK BRANCH, AS COLLATERAL AGENT
To: MALLINCKRODT INTERNATIONAL FINANCE S.A.; MALLINCKRODT CB LLC; MALLINCKRODT FINANCE GMBH; MALLINCKRODT US HOLDINGS LLC (F/K/A MALLINCKRODT US HOLDINGS INC.); MALLINCKRODT CARRIBEAN, INC.; MALLINCKRODT US POOL LLC; MNK 2011 LLC (F/K/A MALLINCKRODT INC.); LUDLOW LLC (F/K/A LUDLOW CORPORATION); CNS THERAPEUTICS, INC.; MALLINCKRODT ENTERPRISES HOLDINGS LLC (F/K/A MALLINCKRODT ENTERPRISES HOLDINGS, INC.); MALLINCKRODT ENTERPRISES LLC; MALLINCKRODT LLC; LAFAYETTE PHARMACEUTICALS LLC; LIEBEL-FLARSHEIM COMPANY LLC; MALLINCKRODT BRAND PHARMACEUTICALS LLC (F/K/A MALLINCKRODT BRAND PHARMACEUTICALS, INC.); MALLINCKRODT VETERINARY, INC.; MALLINCKRODT US HOLDINGS LLC; IMC EXPLORATION COMPANY; MEH, INC.; MALLINCKRODT HOSPITAL PRODUCTS IP UNLIMITED COMPANY (F/K/A MALLINCKRODT HOSPITAL PRODUCTS IP LIMITED); MALLINCKRODT ARD IP UNLIMITED COMPANY (F/K/A MALLINCKRODT ARD IP LIMITED); OCERA THERAPEUTICS LLC (F/K/A OCERA THERAPEUTICS, INC.); SPECGX LLC; STRATATECH CORPORATION; SUCAMPO PHARMA AMERICAS LLC; VTESSE LLC (F/K/A VTESSE INC.); MALLINCKRODT PHARMACEUTICALS IRELAND LIMITED; MALLINCKRODT PHARMA IP TRADING UNLIMITED COMPANY (F/K/A MALLINCKRODT PHARMA IP TRADING D.A.C.); INFACARE PHARMACEUTICAL CORPORATION; ST SHARED SERVICES LLC; THERAKOS, INC.; IKARIA THERAPEUTICS LLC; INO THERAPEUTICS LLC
Reel/Frame 065610/0324 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 14, 2018
From: MATRIX MEDICAL, LLC
To: TENAXIS MEDICAL, INC.
Reel/Frame 046089/0659 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 9, 2018
From: MALLINCKRODT PHARMA IP TRADING DAC
To: BAXTER INTERNATIONAL, INC.
Reel/Frame 045754/0904 →
NUNC PRO TUNC ASSIGNMENT Recorded Oct 3, 2017
From: TENAXIS MEDICAL, INC.
To: MALLINCKRODT PHARMA IP TRADING D.A.C.
Reel/Frame 043767/0923 →
NOTICE OF GRANT OF SECURITY INTEREST IN PATENTS Recorded Aug 18, 2017
From: MALLINCKRODT PHARMA IP TRADING DESIGNATED ACTIVITY COMPANY
To: DEUTSCHE BANK AG NEW YORK BRANCH, AS COLLATERAL AGENT
Reel/Frame 043596/0259 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 9, 2010
From: SCHANKERELI, KEMAL; DIECK, RONALD
To: MATRIX MEDICAL LLC
Reel/Frame 024214/0281 →