Method of forming a protective film
View Patent ↗A method of forming a protective film for a magnetic recording medium is disclosed. The protective film suppresses cobalt elution out of the magnetic recording layer and has a thickness not larger than 3 nm. The method of the invention of forming a protective film for a magnetic recording medium comprises (1) a step of forming a protective film, on a lamination including a substrate and metallic film layers formed on the substrate, by means of a plasma CVD method using a raw gas of a hydrocarbon gas, wherein a flow rate of the hydrocarbon gas is in a range of 50 sccm to 200 sccm and a emission current is in a range of 0.1 A to 0.3 A, and (2) a step of surface treatment on the protective film that has been formed in the step (1), including sub-steps of (2a) a plasma treatment in an argon gas and (2b) a plasma treatment in a gas containing a nitrogen gas.
1. A method of forming a protective film for a magnetic recording medium, the method comprising:
(1) forming a protective film, on a lamination including a substrate and metallic film layers formed on the substrate, by means of a plasma CVD method using a hydrocarbon gas, wherein a flow rate of the hydrocarbon gas is in a range of 50 sccm to 200 sccm and an emission current is in a range of 0.1 A to 0.3 A: and
(2) surface treating the protective film that has been formed in (1), said surface treating including
(2a) a plasma treatment in an argon gas, and
(2b) a plasma treatment in a gas containing a nitrogen gas
wherein 2a precedes 2b.
2. The method of forming a protective film for a magnetic recording medium according to claim 1 , wherein the hydrocarbon gas is ethylene.