IP Library Granted Patent US 8,263,692
Granted Patent B2
US 8,263,692 · App. 12/650,617 · Granted Sep 11, 2012

Propylene-based polymer, articles, and process for producing same

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Quick Facts
Patent No.
US 8,263,692
App. No.
12/650,617
Granted
Sep 11, 2012
Kind
B2
Abstract

Disclosed are propylene-based polymer compositions and processes for producing same. Polymerization with an improved catalyst composition provides a propylene-based polymer with improved stiffness.

Claims (21)

1. A composition comprising:

a propylene homopolymer; and

a substituted phenylene aromatic diester that is 3-methyl-5-tert butyl-1,2 phenylene dibenzoate.

2. The composition of claim 1 wherein the propylene homopolymer has a flexural modulus of greater than 260 kpsi as determined by ASTM D 790.

3. The composition of claim 1 wherein the propylene homopolymer is nucleated.

4. The composition of claim 3 wherein the nucleated propylene homopolymer has a flexural modulus of greater than 322 kpsi as determined by ASTM D 790.

5. The composition of claim 1 wherein the propylene homopolymer has a polydispersity index of 8.0 or less.

6. The composition of claim 1 wherein the propylene homopolymer has a xylene soluble content less than or equal to 1.5% by weight.

7. The composition of claim 1 wherein the propylene homopolymer has isotactic (mmmm) pentads higher than 97%, as determined by 13 C-NMR analysis.

8. The composition of claim 1 wherein the propylene homopolymer has a melt flow rate from 50 g/10 min to 100 g/10 min as measured in accordance with ASTM D 1238 (230° C., 2.16 kg).

9. The composition of claim 1 wherein the propylene homopolymer has a melt flow rate of 50 g/10 min and an oligomer content less than 1800 ppmw.

10. A composition comprising:

a non-nucleated propylene homopolymer comprising a substituted phenylene aromatic diester comprising 3-methyl-5-tert butyl-1,2 phenylene dibenzoate and having a polydispersity index less than 6.0, a flexural modulus greater than 283 kpsi and a melt flow rate greater than or equal to 50 g/10 min as measured in accordance with ASTM D 1238 (230° C., 2.16 kg); and

an oligomer content of less than 1800 ppmw.

11. The composition of claim 10 wherein the propylene-based polymer has a xylene soluble content less than or equal to 1.5% by weight.

12. A propylene impact copolymer comprising:

a propylene homopolymer;

a propylene/ethylene copolymer dispersed within the propylene homopolymer; and

a substituted phenylene aromatic diester that is 3-methyl-5-tert butyl-1,2 phenylene dibenzoate.

13. The propylene impact copolymer of claim 12 wherein the substituted phenylene aromatic diester is present in the propylene homopolymer.

14. The propylene impact copolymer of claim 12 wherein the substituted phenylene aromatic diester is present in the propylene/ethylene copolymer.

Assignments (6)
RELEASE OF SECURITY AGREEMENT RECORDED AT REEL/FRAME NO.: 032159/0384 Recorded Apr 3, 2018
From: GOLDMAN SACHS BANK USA, AS THE COLLATERAL AGENT
To: W.R. GRACE & CO.-CONN.
Reel/Frame 045832/0887 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNEE NAME TO "W. R. GRACE & CO. - CONN." PREVIOUSLY RECORDED ON REEL 032554 FRAME 0730. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNEE NAME WAS PREVIOUSLY INCORRECTLY LISTED IN THE RECORDATION COVER SHEET DATED 3/28/2014 AS "W. R. GRACE & CO. CONN.". Recorded Apr 2, 2014
From: DOW GLOBAL TECHNOLOGIES LLC; UNION CARBIDE CHEMICALS & PLASTICS TECHNOLOGY LLC
To: W. R. GRACE & CO. - CONN.
Reel/Frame 032589/0554 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 28, 2014
From: DOW GLOBAL TECHNOLOGIES LLC; UNION CARBIDE CHEMICALS & PLASTICS TECHNOLOGY LLC
To: W. R. GRACE & CO. CONN.
Reel/Frame 032554/0730 →
SECURITY AGREEMENT Recorded Feb 4, 2014
From: W.R. GRACE & CO.-CONN.
To: GOLDMAN SACHS BANK USA, AS THE COLLATERAL AGENT
Reel/Frame 032159/0384 →
CHANGE OF NAME Recorded Mar 21, 2011
From: DOW GLOBAL TECHNOLOGIES INC.
To: DOW GLOBAL TECHNOLOGIES LLC
Reel/Frame 025990/0927 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 18, 2010
From: SHEARD, WILLIAM G.; CHEN, LINFENG
To: DOW GLOBAL TECHNOLOGIES INC.
Reel/Frame 024100/0933 →