IP Library Granted Patent US 8,106,138
Granted Patent B2
US 8,106,138 · App. 12/650,633 · Granted Jan 31, 2012

Random propylene copolymer compositions, articles and process

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Quick Facts
Patent No.
US 8,106,138
App. No.
12/650,633
Granted
Jan 31, 2012
Kind
B2
Abstract

The present disclosure is directed to random propylene/α-olefin compositions, articles, and processes for producing the same. The present compositions contain a random copolymer of propylene and α-olefin. Polymerization with an improved catalyst composition increases the molecular weight distribution of the copolymer and increases the randomness of comonomer distribution to yield random propylene/α-olefin copolymers with improved stiffness and/or improved optical properties.

Claims (5)

1. A polymerization process comprising:

contacting, under polymerization conditions, propylene and ethylene with a catalyst composition comprising a substituted phenylene aromatic diester; and

forming a random propylene/ethylene copolymer with a Koening B-value from greater than or equal to 0.83 to about 1.0.

2. The polymerization process of claim 1 comprising maintaining a H 2 /C 3 molar ratio from 0.002 to 0.02 and forming a propylene/ethylene copolymer having a melt flow rate from 0.1g/10 min to 5 g/10 min as measured in accordance with ASTM D 1238, 2.16 kg, 230° C.

3. The polymerization process of claim 1 comprising maintaining a H 2 /C 3 molar ratio from 0.010 to 0.25 and forming a propylene/ethylene copolymer having a melt flow rate from greater than 5 g/10 min to about 800 g/10 min as measured in accordance with ASTM D 1238, 2.16, 230° C.

Assignments (13)
NOTES SECURITY INTEREST Recorded Jan 29, 2026
From: W. R. GRACE & CO.-CONN.; ADVANCED REFINING TECHNOLOGIES LLC
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS NOTES COLLATERAL AGENT
Reel/Frame 074532/0229 →
SECURITY AGREEMENT (NOTES) Recorded Aug 19, 2025
From: W. R. GRACE & CO.-CONN.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS NOTES COLLATERAL AGENT
Reel/Frame 072520/0653 →
SECURITY INTEREST Recorded Feb 17, 2023
From: W.R. GRACE & CO.-CONN.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION
Reel/Frame 062792/0510 →
NOTES SECURITY AGREEMENT Recorded Sep 23, 2021
From: W. R. GRACE & CO.-CONN.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION
Reel/Frame 057594/0156 →
RELEASE OF SECURITY INTEREST Recorded Sep 23, 2021
From: GOLDMAN SACHS BANK USA
To: W. R. GRACE & CO.-CONN.
Reel/Frame 057594/0026 →
TERM LOAN SECURITY AGREEMENT Recorded Sep 23, 2021
From: W. R. GRACE & CO.-CONN.
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 057594/0104 →
SECURITY INTEREST Recorded Apr 3, 2018
From: W. R. GRACE & CO.-CONN.
To: GOLDMAN SACHS BANK USA, AS COLLATERAL AGENT
Reel/Frame 045828/0683 →
RELEASE OF SECURITY AGREEMENT RECORDED AT REEL/FRAME NO.: 032159/0384 Recorded Apr 3, 2018
From: GOLDMAN SACHS BANK USA, AS THE COLLATERAL AGENT
To: W.R. GRACE & CO.-CONN.
Reel/Frame 045832/0887 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNEE NAME TO "W. R. GRACE & CO. - CONN." PREVIOUSLY RECORDED ON REEL 032554 FRAME 0730. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNEE NAME WAS PREVIOUSLY INCORRECTLY LISTED IN THE RECORDATION COVER SHEET DATED 3/28/2014 AS "W. R. GRACE & CO. CONN.". Recorded Apr 2, 2014
From: DOW GLOBAL TECHNOLOGIES LLC; UNION CARBIDE CHEMICALS & PLASTICS TECHNOLOGY LLC
To: W. R. GRACE & CO. - CONN.
Reel/Frame 032589/0554 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 28, 2014
From: DOW GLOBAL TECHNOLOGIES LLC; UNION CARBIDE CHEMICALS & PLASTICS TECHNOLOGY LLC
To: W. R. GRACE & CO. CONN.
Reel/Frame 032554/0730 →
SECURITY AGREEMENT Recorded Feb 4, 2014
From: W.R. GRACE & CO.-CONN.
To: GOLDMAN SACHS BANK USA, AS THE COLLATERAL AGENT
Reel/Frame 032159/0384 →
CHANGE OF NAME Recorded Mar 21, 2011
From: DOW GLOBAL TECHNOLOGIES INC.
To: DOW GLOBAL TECHNOLOGIES LLC
Reel/Frame 025990/0927 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 29, 2010
From: SHEARD, WILLIAM G.; CHEN, LINFENG; BAUGH, DANIEL W., III; MARTIN, PETER S.
To: DOW GLOBAL TECHNOLOGIES INC.
Reel/Frame 024307/0861 →