IP Library Granted Patent US 8,524,278
Granted Patent B2
US 8,524,278 · App. 12/656,704 · Granted Sep 3, 2013

Controlled release pharmaceutical formulations of nitazoxanide

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Quick Facts
Patent No.
US 8,524,278
App. No.
12/656,704
Granted
Sep 3, 2013
Kind
B2
Abstract

Solid dosage formulations of nitazoxanide or a nitazoxanide analogue are provided that comprise a controlled release portion and an immediate release portion. The pharmaceutical composition is typically in the form of a bilayer solid oral dosage form comprising (a) a first layer comprising a first quantity of nitazoxanide or analogue thereof in a controlled release formulation; and (b) a second layer comprising a second quantity of nitazoxanide or analogue thereof in an immediate release formulation. Method of using the formulations in the treatment of hepatitis C are also provided.

Claims (22)

1. A pharmaceutical composition in the form of a solid oral dosage form comprising:

(a) a first portion comprising a first quantity of nitazoxanide or an analogue thereof in a controlled release formulation; and

(b) a second portion comprising a second quantity of nitazoxanide or an analogue thereof in an immediate release formulation,

wherein the ratio of the first quantity of nitazoxanide or an analogue thereof to the second quantity of nitazoxanide or an analogue thereof is about 2.5:1 to about 4:1.

2. The composition of claim 1 , wherein the solid oral dosage form is a tablet.

3. The composition of claim 2 , wherein the first portion (a) forms a first layer of the tablet, and the second portion (b) forms a second layer deposited on top of the first layer (a).

4. The composition of claim 2 , wherein the first portion (a) forms a first layer of the tablet; the second portion (b) forms a second layer that is deposited on top of the first layer (a) to form a core tablet comprising the first layer and the second layer; and (c) an outer coating layer that is deposited on top of the core tablet.

5. The composition of claim 1 , wherein the solid oral dosage form is a capsule.

6. The composition of claim 5 , wherein the first portion (a) is in the form of controlled-release granules containing the first quantity of nitazoxanide or analogue thereof, and the second portion (b) is in the form of immediate-release granules containing the second quantity of nitazoxanide or analogue thereof.

7. The composition of claim 1 , wherein the first portion further comprises one or more diluents, disintegrants, binders, suspending agents, glidants, lubricants, fillers, or additional excipients.

8. The composition of claim 7 , wherein the first portion further comprises hydroxypropylcellulose and hydroxypropylmethylcellulose as the binders, dicalciumphosphate dehydrate as the filler, colloidal anhydrous silica as the glidant, and magnesium stearate as the lubricant.

9. The composition of claim 1 , wherein the second portion further comprises one or more diluents, disintegrants, binders, suspending agents, glidants, lubricants, fillers, or additional excipients.

10. The composition of claim 9 , wherein the second portion further comprises hydroxypropylcellulose and microcrystalline cellulose as the binders, maize starch as the diluent, sodium croscarmellose as the disintegrant, colloidal anhydrous silica as the glidant, and magnesium stearate as the lubricant.

11. The composition of claim 1 , wherein the first portion further comprises a low viscosity polymer.

12. The composition of claim 11 , wherein the low viscosity polymer is a low viscosity hydroxypropyl-methylcellulose.

13. A bilayer tablet for oral administration, the tablet comprising:

(a) a first layer comprising about 500 mg of nitazoxanide in a controlled release formulation; and

(b) a second layer comprising about 175 mg of nitazoxanide in an immediate release formulation, the second layer deposited on top of and compressed with the first layer to form a core tablet; and

(c) an outer coating applied to the core tablet;

wherein the first layer further comprises a low-viscosity hydroxypropylmethylcellulose.

14. The bilayer tablet of claim 13 , wherein the first layer comprises about 15% to about 20% by weight of the low-viscosity hydroxypropylmethylcellulose and the first layer has a total weight of about 750 mg.

15. The composition of claim 1 , wherein the first and second quantity of nitazoxanide or an analogue thereof are each independently selected from a group consisting of nitazoxanide, tizoxanide and a combination thereof.

Assignments (8)
SECURITY INTEREST Recorded Nov 16, 2019
From: ROMARK BIOSCIENCES S.À R.L. LLC; ROMARK LABORATORIES, L.C.
To: U.S. BANK NATIONAL ASSOCIATION
Reel/Frame 051030/0613 →
SECURITY INTEREST Recorded Jul 2, 2018
From: ROMARK BIOSCIENCES S.À R.L. LLC; ROMARK LABORATORIES, L.C.
To: U.S. BANK NATIONAL ASSOCIATION
Reel/Frame 046254/0524 →
SECURITY INTEREST Recorded Dec 22, 2017
From: ROMARK BIOSCIENCES S.À R.L. LLC; ROMARK LABORATORIES, L.C.
To: U.S. BANK NATIONAL ASSOCIATION
Reel/Frame 044472/0001 →
RELEASE OF SECURITY INTEREST Recorded Mar 6, 2015
From: U.S. BANK NATIONAL ASSOCIATION
To: ROMARK LABORATORIES, L.C.; ROMARK MANUFACTURING, LLC; LAPICOR, N.V.
Reel/Frame 035108/0474 →
SECURITY AGREEMENT Recorded Sep 4, 2013
From: ROMARK LABORATORIES, L.C.; ROMARK MANUFACTURING, LLC; LAPICOR, N.V.
To: U.S. BANK NATIONAL ASSOCIATION
Reel/Frame 031156/0923 →
RELEASE OF SECURITY INTEREST Recorded Sep 3, 2013
From: PAUL CAPITAL FUND MANAGEMENT, L.L.C.
To: ROMARK LABORATORIES, L.C.
Reel/Frame 031159/0636 →
SECURITY AGREEMENT Recorded Jul 29, 2011
From: ROMARK LABORATORIES, L.C.
To: PAUL CAPITAL FUND MANAGEMENT, L.L.C.
Reel/Frame 026676/0635 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 12, 2010
From: ROSSIGNOL, JEAN-FRANCOIS; AYERS, MARC
To: ROMARK LABORATORIES L.C.
Reel/Frame 023976/0831 →