Flame ionization detector
View Patent ↗The flame ionization detector, which comprises a supply and an ignition device ( 7 ) for the combustible gas, a supply for the sample gas, a combustion chamber ( 4 ) in which the sample gas is ionized by the flame, and electrodes ( 8, 1 ) to which a voltage is applied in order to generate and measure the ion current, is distinguished in that it is constructed as an integrated planar system of at least three parallel platelet-like substrates ( 1, 2, 3 ) which are connected to one another and are processed by microsystem technology methods, with a central substrate ( 1 ) comprising nozzles ( 5, 6 ) for the gases and the ignition device ( 7 ) and a recess which forms a part of the combustion chamber ( 4 ), is completed by recesses in the neighboring substrates ( 2, 3 ) and is essentially closed together with the nozzle region by these substrates ( 2, 3 ), and the neighboring substrates ( 2, 3 ) comprise supply channels ( 10, 11 ) for the gases.
1. A flame ionization detector comprising:
a supply and an ignition device ( 7 ) for a combustible gas,
a supply for a sample gas,
a combustion chamber ( 4 ) wherein the sample gas is ionized by a flame, electrodes ( 8 , 1 ) situated inside the combustion chamber, to which a voltage is applied for generating and measuring an ion current,
wherein the detector is constructed as an integrated planar system of at least three parallel planar substrates ( 1 , 2 , 3 ) that are bonded to one another in a sandwich configuration, wherein a central substrate ( 1 ) comprises nozzles ( 5 , 6 ) for the gases and the ignition device ( 7 ) and a recess which forms a part of the combustion chamber ( 4 ), and wherein the combustion chamber is formed by recesses in a top and bottom substrate ( 2 , 3 ) and is essentially closed together with the nozzle region by the top substrate and the bottom substrate ( 2 , 3 ), the top and bottom substrates ( 2 , 3 ) comprise supply channels ( 10 , 11 ) for the gases.
2. The flame ionization detector as claimed in claim 1 , wherein the central substrate ( 1 ) is electrically conductive and the neighboring substrates ( 2 , 3 ) are essentially nonconductive.
3. The flame ionization detector as claimed in claim 1 , wherein central substrate ( 1 ) consists of silicon and the neighboring substrates ( 2 , 3 ) consist of glass, in particular borosilicate glass.
4. The flame ionization detector as claimed in claim 1 , wherein an electrode ( 8 ) is arranged in each of the neighboring substrates ( 2 , 3 ) in the region of the combustion chamber ( 4 ).
5. The flame ionization detector as claimed in claim 2 , wherein one electrode is formed by the central substrate ( 1 ).
6. The flame ionization detector as claimed in claim 5 , wherein the central substrate comprises a shielding electrode ( 12 ).
7. The flame Ionization detector as claimed in claim 1 , wherein all the substrates ( 1 , 2 , 3 ) comprise parts with rounded contours.
8. The flame ionization detector as claimed in claim 1 , wherein the substrates ( 1 , 2 , 3 ) are connected by anodic bonding.
9. The flame ionization detector as claimed in claim 4 , wherein the electrodes ( 8 ) on the neighboring substrates ( 1 , 2 ) are reflective.
10. The flame Ionization detector as claimed in claim 1 , wherein the nozzles ( 5 , 6 ) for the gases are formed as a buried structure and are covered by at least one further substrate.
11. The flame Ionization detector as claimed in claim 1 , wherein the central substrate ( 1 ) comprises at least one electrode tip ( 7 ) immediately behind the nozzles ( 5 , 6 ), to which a high-voltage pulse is being applied for ignition.
12. The flame ionization detector as claimed in claim 1 , wherein the detector is provided with two high-induction magnets for forming a magneto-hydrodynamic generator.