IP Library Granted Patent US 9,522,218
Granted Patent B2
US 9,522,218 · App. 12/681,682 · Granted Dec 20, 2016

Method for preparing porous scaffold for tissue engineering, cell culture and cell delivery

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Quick Facts
Patent No.
US 9,522,218
App. No.
12/681,682
Granted
Dec 20, 2016
Kind
B2
Abstract

The present invention relates to a method for preparing a porous scaffold for tissue engineering. It is another object of the present invention to provide a porous scaffold obtainable by the method as above described, and its use for tissue engineering, cell culture and cell delivery. The method of the invention comprises the steps consisting of: a) preparing an alkaline aqueous solution comprising an amount of at least one polysaccharide, an amount of a cross-linking agent and an amount of a porogen agent b) transforming the solution into a hydrogel by placing said solution at a temperature from about 4° C. to about 80° C. for a sufficient time to allow the cross-linking of said amount of polysaccharide and c) submerging said hydrogel into an aqueous solution d) washing the porous scaffold obtained at step c).

Claims (14)

1. A method for preparing a porous scaffold which consists of the following steps:

a) preparing an alkaline aqueous solution comprising an amount of at least one polysaccharide selected from the group consisting of dextran, agar, pullulan, inulin, heparin, fucoidan, and mixtures thereof; an amount of a covalent cross-linking agent selected from the group consisting of trisodium trimetaphosphate (STMP), phosphorus oxychloride (POCl 3 ), epichlorohydrin, formaldehydes, and glutaraldehydes; and an amount of a porogen agent selected from the group consisting of ammonium carbonate, ammonium bicarbonate, calcium carbonate, sodium carbonate, and sodium bicarbonate and mixtures thereof;

b) transforming the solution into a hydrogel by placing said solution at a temperature from about 4° C. to about 80° C. for a sufficient time to allow the cross-linking of said amount of polysaccharide;

c) submerging said hydrogel into an aqueous acidic solution to form pores; and

d) washing the porous scaffold obtained at step c),

wherein

the porous scaffold is a hydrogel;

the porogen agent is dissolved in step a);

the weight ratio of the polysaccharide to the porogen agent is in the range from 6:1 to 1:1; and

wherein the alkaline aqueous solution in a) does not include a surfactant.

2. The method according to claim 1 wherein the weight ratio of the polysaccharide to the cross-linking agent is in the range from 15:1 to 1:1.

3. The method according to claim 1 wherein the solution of step a) is poured in a mould before step b).

4. The method according to claim 1 wherein said scaffold is shaped.

5. The method according to claim 1 wherein the porogen agent is selected from the group consisting of ammonium carbonate, calcium carbonate, sodium carbonate, sodium bicarbonate, and mixtures thereof.

Assignments (4)
CHANGE OF NAME Recorded Mar 25, 2022
From: UNIVERSITÉ DE PARIS
To: UNIVERSITÉ PARIS CITÉ
Reel/Frame 059504/0225 →
MERGER Recorded Jul 12, 2021
From: UNIVERSITE PARIS DIDEROT - PARIS 7
To: UNIVERSITE DE PARIS
Reel/Frame 056817/0647 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 25, 2017
From: INSERM (INSTITUT NATIONAL DE LA SANTE ET DE LA RECHERCHE MEDICALE)
To: UNIVERSITE PARIS 7 - DENIS DIDEROT
Reel/Frame 042135/0395 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 9, 2016
From: LE VISAGE, CATHERINE; LETOURNEUR, DIDIER
To: INSERM (INSTITUT NATIONAL DE LA SANTE ET DE LA RECHERCHE MEDICALE)
Reel/Frame 040262/0540 →