IP Library Granted Patent US 8,986,836
Granted Patent B2
US 8,986,836 · App. 12/720,102 · Granted Mar 24, 2015

Microspheres and their methods of preparation

Inventors: Anima B. Bose (Athens, OH); Junbing Yang (Bolingbrook, IL)
Assignee: Ohio University
H01B1/04B82Y30/00C01B3/0021C01B3/0084C01B31/02C01B31/10A61M1/3679Y02E60/325Y10S977/773Y10S977/775Y10S977/932Y10S977/948Y10S977/962
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Quick Facts
Patent No.
US 8,986,836
App. No.
12/720,102
Granted
Mar 24, 2015
Kind
B2
Abstract

Carbon microspheres are doped with boron to enhance the electrical and physical properties of the microspheres. The boron-doped carbon microspheres are formed by a CVD process in which a catalyst, carbon source and boron source are evaporated, heated and deposited onto an inert substrate.

Claims (9)

1. Carbon microspheres having an average diameter of 50 to 700 nm wherein microspheres are doped with boron;

said sphere having pores wherein said pores are 0.6 to 2 nanometers;

wherein a gas is stored in said microsphere.

2. The carbon microspheres claimed in claim 1 wherein the boron to carbon ratio of said microspheres is at least 1:20.

3. The carbon microspheres claimed in claim 2 wherein the boron to carbon ratio of said carbon microspheres is less than 1.5 to 10.

4. The carbon microspheres claimed in claim 3 wherein the boron to carbon ratio of said microspheres is from about 1:4-1:12.

5. The carbon microspheres claimed in claim 1 further comprising nitrogen.

6. The microspheres claimed in claim 1 wherein said gas is H 2 .

7. A separator for an electrolytic cell comprising a support containing the carbon microspheres claimed in claim 1 .

Assignments (3)
CONFIRMATORY LICENSE Recorded Apr 21, 2022
From: UCHICAGO ARGONNE, LLC
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 059668/0472 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 9, 2010
From: BOSE, ANIMA B.
To: OHIO UNIVERSITY
Reel/Frame 024051/0222 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 9, 2010
From: YANG, JUNBING
To: UCHICAGO ARGONNE, LLC
Reel/Frame 024051/0369 →
Continuity (2)
Provisional Application 61161580 · Mar 19, 2009
Related Publication 20100237295A1 · Sep 23, 2010