IP Library Granted Patent US 9,222,035
Granted Patent B2
US 9,222,035 · App. 12/743,358 · Granted Dec 29, 2015

Process for stabilizing an oil-in-water or water-in-oil emulsion

Inventors: Jens Emil Vindstad (Stavanger, NO); Heidi Mediaas (Stavanger, NO); Knut Vebjørn Grande (Stavanger, NO)
Assignee: STATOIL PETROLEUM AS
C10G31/08C10G19/02C10G29/06C10M129/56C10M129/58B01F3/0807B01F17/0021
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Quick Facts
Patent No.
US 9,222,035
App. No.
12/743,358
Granted
Dec 29, 2015
Kind
B2
Abstract

A process for the preparation of at least one ARN acid or salt thereof comprising: (I) allowing at least one ARN acid salt to form during the production of crude oil in the presence of water; (II) removing at least 5 wt % of the formed at least one ARN acid salt, e.g. from the oil water interface; and optionally (III) converting said salt into an acid.

Claims (18)

1. A process for stabilizing an oil-in-water or water-in-oil emulsion comprising:

(I) adding at least one metal ion to a crude oil at a pH of at least 5 so as to form an ARN acid salt;

(II) separating at least a part of the formed ARN acid salt from the crude oil;

(III) converting said salt into an acid; and

(IV) adding said acid to a mixture of oil-in-water or water-in-oil.

2. A process as claimed in claim 1 wherein said salt is a calcium salt.

3. A process as claimed in claim 1 wherein said ARN acid is a tetracarboxylic acid with molecular weight in the range 1227-1235 or mixture of such acids.

4. A process as claimed in claim 1 wherein a pressure during ARN acid salt formation is ambient.

5. A process as claimed in claim 1 wherein the ARN acid content of the crude oil is at least 10 ppm.

6. A process for stabilizing an oil-in-water or water-in-oil emulsion comprising:

(I) allowing at least one ARN acid salt to form during the production of crude oil in the presence of water;

(II) separating at least a part of the formed ARN acid salt from the crude oil;

(III) converting said salt into an acid; and

(IV) adding said acid to a mixture of oil-in-water or water-in-oil.

7. A process as claimed in claim 6 wherein said salt is a calcium salt.

8. A process as claimed in claim 6 wherein said ARN acid is a tetracarboxylic acid with molecular weight in the range 1227-1235 or mixture of such acids.

9. A process as claimed in claim 6 wherein ARN acid salt formation is conducted at ambient pressure.

10. A process as claimed in claim 6 wherein the ARN acid content of the crude oil is at least 10 ppm.

Assignments (5)
CHANGE OF NAME Recorded Jan 30, 2019
From: STATOIL PETROLEUM AS
To: EQUINOR ENERGY AS
Reel/Frame 048196/0501 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 13, 2013
From: STATOIL ASA
To: STATOIL PETROLEUM AS
Reel/Frame 031627/0265 →
CHANGE OF NAME Recorded Oct 31, 2013
From: STATOILHYDRO ASA
To: STATOIL ASA
Reel/Frame 031528/0807 →
CHANGE OF NAME Recorded Oct 25, 2013
From: STATOIL ASA
To: STATOILHYDRO ASA
Reel/Frame 031495/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 9, 2010
From: VINDSTAD, JENS EMIL; MEDIAAS, HEIDI; GRANDE, KNUT VEBJORN
To: STATOIL ASA
Reel/Frame 024661/0250 →
Priority Claims (2)
GB 0722570.9 · Nov 16, 2007 · national
GB 0722591.5 · Nov 16, 2007 · national
Continuity (1)
Related Publication 20100292349A1 · Nov 18, 2010