IP Library Granted Patent US 8,617,310
Granted Patent B1
US 8,617,310 · App. 12/776,214 · Granted Dec 31, 2013

Method and system for perceiving a boundary between a first region and a second region of a superabrasive volume

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Quick Facts
Patent No.
US 8,617,310
App. No.
12/776,214
Granted
Dec 31, 2013
Kind
B1
Abstract

Methods of evaluating a superabrasive volume or a superabrasive compact are disclosed. One method may comprise exposing a superabrasive volume to beta particles and detecting a quantity of scattered beta particles. Further, a boundary may be perceived between a first region and a second region of the superabrasive volume in response to detecting the quantity of scattered beta particles. In another embodiment, a boundary between a catalyst-containing region and a catalyst-diminished region of a polycrystalline diamond volume may be perceived. In a further embodiment, a boundary may be perceived between a catalyst-containing region and a catalyst-diminished region of a polycrystalline diamond compact. Additionally, a depth to which a catalyst-diminished region extends within a polycrystalline diamond volume of a polycrystalline diamond compact may be measured in response to detecting a quantity of scattered beta particles. A system configured to evaluate a superabrasive volume is disclosed.

Claims (22)

1. A method of manufacturing a polycrystalline diamond component, the method comprising:

sintering diamond crystals in the presence of a catalyst material to form a diamond table;

removing a portion of the catalyst material from the diamond table such that the diamond table includes a catalyst-rich region and a catalyst-diminished region;

exposing the diamond table to radiation;

monitoring a reaction of the radiation to which the diamond table is exposed; and

detecting a boundary between the catalyst-rich region and the catalyst-diminished region in response to the monitored reaction of the radiation.

2. The method according to claim 1 , wherein removing a portion of the catalyst material further comprises leaching a portion of catalyst material from the diamond table.

3. The method according to claim 1 , wherein removing a portion of the catalyst material further comprises subjecting the diamond table to an electrolytic or electroless plating process.

4. The method according to claim 1 , wherein detecting a boundary between the catalyst-rich region and the catalyst-diminished region comprises measuring a depth of the catalyst-diminished region from an exterior surface of the diamond table.

5. The method according to claim 4 , wherein exposing the diamond table to radiation further comprises tailoring an energy level of the radiation based on an anticipated depth of the catalyst-diminished region.

6. The method according to claim 1 , wherein exposing the diamond table to radiation comprises exposing the diamond table to beta particles.

7. The method according to claim 6 , wherein monitoring a reaction of the radiation to which the diamond table is exposed comprises detecting a quantity of beta particles that are scattered when exposed to the diamond table.

8. The method according to claim 7 , wherein detecting a boundary between the catalyst-rich region and the catalyst-diminished region in response to the monitored reaction of the radiation comprises detecting the boundary in response to detecting the quantity of scattered beta particles.

9. The method according to claim 8 , wherein detecting a boundary between the catalyst-rich region and the catalyst-diminished region in response to the monitored reaction of the radiation further comprises comparing the quantity of scatter beta particles with calibration data.

10. The method according to claim 6 , further comprising collimating the beta particles to a selected spot size.

11. The method according to claim 1 , wherein sintering diamond crystals in the presence of a catalyst material further comprises sintering diamond crystals in the presence of cobalt.

12. The method according to claim 1 , wherein detecting a boundary between the catalyst-rich region and the catalyst-diminished region further comprises detecting a boundary between a cobalt-rich region and a cobalt-diminished region of the superabrasive volume.

13. The method according to claim 1 , wherein detecting a boundary between the catalyst-rich region and the catalyst-diminished region further comprises perceiving an arcuate boundary between the catalyst-rich region and the catalyst-diminished region.

14. The method according to claim 1 , further comprising bonding the diamond table to a substrate.

15. The method according to claim 14 , wherein bonding the diamond table to a substrate includes bonding the diamond table to a cemented carbide substrate while sintering the diamond crystals.

16. The method according to claim 15 , wherein bonding the diamond table to the cemented tungsten carbide substrate includes bonding the diamond table to a cobalt-cemented tungsten carbide substrate.

17. The method according to claim 1 , wherein sintering diamond crystals in the presence of a catalyst material further includes sintering diamond crystals in the presence of a material comprising a group VIII element.

Assignments (5)
SECURITY INTEREST Recorded Jul 18, 2025
From: US SYNTHETIC CORPORATION
To: KEYBANK NATIONAL ASSOCIATION
Reel/Frame 074973/0089 →
RELEASE OF SECURITY INTEREST IN PATENTS Recorded Jul 17, 2025
From: JPMORGAN CHASE BANK, N.A.
To: CHAMPIONX LLC; APERGY ESP SYSTEMS, LLC; APERGY BMCS ACQUISITION CORP; HARBISON-FISCHER, INC.; NORRIS RODS, INC.,; NORRIS RODS, INC.,; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; US SYNTHETIC CORPORATION
Reel/Frame 072004/0019 →
RELEASE OF SECURITY INTEREST Recorded Jun 7, 2022
From: BANK OF AMERICA, N.A.
To: ACE DOWNHOLE, LLC; HARBISON-FISCHER, INC.; NORRIS RODS, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; THETA OILFIELD SERVICES, INC.; APERGY BMCS ACQUISITION CORP.; NORRISEAL-WELLMARK, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
Reel/Frame 060305/0001 →
SECURITY INTEREST Recorded Jun 5, 2020
From: ACE DOWNHOLE, LLC; APERGY BMCS ACQUISITION CORP.; HARBISON-FISCHER, INC.; NORRIS RODS, INC.; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; THETA OILFIELD SERVICES, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
To: BANK OF AMERICA, N.A.
Reel/Frame 053790/0001 →
SECURITY AGREEMENT Recorded May 9, 2018
From: APERGY (DELAWARE) FORMATION, INC.; APERGY BMCS ACQUISITION CORP.; APERGY ENERGY AUTOMATION, LLC; HARBISON-FISCHER, INC.; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 046117/0015 →