IP Library Granted Patent US 8,461,832
Granted Patent B2
US 8,461,832 · App. 12/785,014 · Granted Jun 11, 2013

Method of characterizing a polycrystalline diamond element by at least one magnetic measurement

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Quick Facts
Patent No.
US 8,461,832
App. No.
12/785,014
Granted
Jun 11, 2013
Kind
B2
Abstract

In an embodiment, a method of characterizing a polycrystalline diamond element is disclosed. The method includes providing the polycrystalline diamond element, and measuring at least one magnetic characteristic of the polycrystalline diamond element.

Claims (34)

1. A method of characterizing a polycrystalline diamond element, the method comprising:

providing the polycrystalline diamond element including a plurality of diamond grains defining a plurality of interstitial regions, wherein at least a portion of the plurality of interstitial regions are occupied by a metallic material;

measuring at least one magnetic characteristic of the polycrystalline diamond element; and

determining at least one physical characteristic of the polycrystalline diamond element at least partially based on the at least one magnetic characteristic.

2. The method of claim 1 wherein measuring at least one magnetic characteristic of the polycrystalline diamond element comprises measuring a coercivity of the polycrystalline diamond element.

3. The method of claim 1 wherein measuring at least one magnetic characteristic of the polycrystalline diamond element comprises measuring a magnetic saturation of the polycrystalline diamond element.

4. The method of claim 1 wherein measuring at least one magnetic characteristic of the polycrystalline diamond element comprises measuring a coercivity of the polycrystalline diamond element, and wherein the at least one physical characteristic of the polycrystalline diamond element is an extent of diamond-to-diamond bonding between the diamond grains in the polycrystalline diamond element.

5. The method of claim 1 wherein measuring at least one magnetic characteristic of the polycrystalline diamond element comprises measuring a coercivity of the polycrystalline diamond element, and wherein the at least one physical characteristic of the polycrystalline diamond element is mean free path between neighboring ones of the diamond grains.

6. The method of claim 1 wherein measuring at least one magnetic characteristic of the polycrystalline diamond element comprises measuring a magnetic saturation of the polycrystalline diamond element, and wherein the at least one physical characteristic of the polycrystalline diamond element is concentration of the metallic material.

7. The method of claim 1 , further comprising:

wherein measuring at least one magnetic characteristic of the polycrystalline diamond element comprises measuring a magnetic saturation and a coercivity of the polycrystalline diamond element; and

determining a specific permeability of the polycrystalline diamond element based on the magnetic saturation and the coercivity.

8. The method of claim 1 , further comprising:

wherein measuring at least one magnetic characteristic of the polycrystalline diamond element comprises measuring a magnetic saturation of the polycrystalline diamond element; and

determining a specific magnetic saturation of the polycrystalline diamond element at least partially based on the magnetic saturation and a mass of the polycrystalline diamond element.

9. The method of claim 1 , further comprising:

wherein measuring at least one magnetic characteristic of the polycrystalline diamond element comprises measuring a magnetic saturation of the polycrystalline diamond element; and

determining a concentration of the metallic material at least partially based on the at least one magnetic characteristic.

10. The method of claim 1 , further comprising determining a concentration of the metallic material at least partially based on the at least one magnetic characteristic.

11. The method of claim 1 wherein the metallic material comprises a metal-solvent catalyst.

12. The method of claim 11 wherein the metal-solvent catalyst comprises a member selected from the group consisting of iron, nickel, cobalt, and alloys thereof.

13. The method of claim 1 , further comprising calculating a concentration of the metallic material at least partially based on the at least one magnetic characteristic.

14. The method of claim 1 wherein the polycrystalline diamond element is at least partially leached of the metallic material.

15. The method of claim 1 wherein the polycrystalline diamond element is unleached.

16. The method of claim 1 wherein the polycrystalline diamond element was formed on a cemented carbide substrate.

17. The method of claim 1 wherein the polycrystalline diamond element can form part of a polycrystalline diamond compact in which the polycrystalline diamond element is bonded to a cemented carbide substrate.

18. A method, comprising:

providing a polycrystalline diamond element that can form part of a polycrystalline diamond compact in which the polycrystalline diamond element is bonded to a cemented carbide substrate; and

measuring at least one magnetic characteristic of the polycrystalline diamond element; and

determining at least one physical characteristic of the polycrystalline diamond element at least partially based on the at least one magnetic characteristic.

19. The method of claim 18 wherein measuring at least one magnetic characteristic of the polycrystalline diamond element comprises measuring a magnetic saturation of the polycrystalline diamond element.

20. A method of characterizing a polycrystalline diamond element, the method comprising:

providing the polycrystalline diamond element; and

measuring at least one magnetic characteristic of the polycrystalline diamond element.

Assignments (5)
SECURITY INTEREST Recorded Jul 18, 2025
From: US SYNTHETIC CORPORATION
To: KEYBANK NATIONAL ASSOCIATION
Reel/Frame 074973/0089 →
RELEASE OF SECURITY INTEREST IN PATENTS Recorded Jul 17, 2025
From: JPMORGAN CHASE BANK, N.A.
To: CHAMPIONX LLC; APERGY ESP SYSTEMS, LLC; APERGY BMCS ACQUISITION CORP; HARBISON-FISCHER, INC.; NORRIS RODS, INC.,; NORRIS RODS, INC.,; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; US SYNTHETIC CORPORATION
Reel/Frame 072004/0019 →
RELEASE OF SECURITY INTEREST Recorded Jun 7, 2022
From: BANK OF AMERICA, N.A.
To: ACE DOWNHOLE, LLC; HARBISON-FISCHER, INC.; NORRIS RODS, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; THETA OILFIELD SERVICES, INC.; APERGY BMCS ACQUISITION CORP.; NORRISEAL-WELLMARK, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
Reel/Frame 060305/0001 →
SECURITY INTEREST Recorded Jun 5, 2020
From: ACE DOWNHOLE, LLC; APERGY BMCS ACQUISITION CORP.; HARBISON-FISCHER, INC.; NORRIS RODS, INC.; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; THETA OILFIELD SERVICES, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
To: BANK OF AMERICA, N.A.
Reel/Frame 053790/0001 →
SECURITY AGREEMENT Recorded May 9, 2018
From: APERGY (DELAWARE) FORMATION, INC.; APERGY BMCS ACQUISITION CORP.; APERGY ENERGY AUTOMATION, LLC; HARBISON-FISCHER, INC.; NORRISEAL-WELLMARK, INC.; PCS FERGUSON, INC.; QUARTZDYNE, INC.; SPIRIT GLOBAL ENERGY SOLUTIONS, INC.; US SYNTHETIC CORPORATION; WINDROCK, INC.
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 046117/0015 →