IP Library Granted Patent US 8,178,623
Granted Patent B2
US 8,178,623 · App. 12/797,717 · Granted May 15, 2012

High stiffness high impact propylene impact copolymers field of the invention

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Quick Facts
Patent No.
US 8,178,623
App. No.
12/797,717
Granted
May 15, 2012
Kind
B2
Abstract

The present invention relates to polypropylene impact copolymer compositions which exhibit improved stiffness without degrading the impact resistance performance. The polypropylene impact copolymer comprises a matrix and a dispersed phase. The matrix comprises a polypropylene homopolymer or a propylene/alpha-olefin random copolymer which comprises more than 50 wt. % of units derived from propylene monomer. The matrix should have a relatively high crystallinity, preferably 50% or greater. The polypropylene homopolymer or a propylene/alpha-olefin random copolymer preferably has a MWD between 4 and 8, such as typically obtained using Ziegler-Natta catalysts. The dispersed phase in the impact copolymer comprises an ethylene-propylene copolymer which comprises from 45 to 70 wt. % of units derived from an ethylene monomer. Preferably the dispersed phase comprises from 20 to 50 percent by weight of the polypropylene impact copolymer.

Claims (14)

1. A polypropylene impact copolymer comprising:

(a) a matrix comprising a polypropylene homopolymer or a propylene/alpha-olefin random copolymer which comprises more than 50 wt. % of units derived from propylene monomer, the polypropylene homopolymer or a propylene/alpha-olefin random copolymer having an MWD between 4 and 8; wherein said matrix has a crystallinity of at least 50%;

(b) a dispersed phase comprising an ethylene-propylene copolymer which comprises from 45 to 65 wt. % of units derived from an ethylene monomer;

wherein the dispersed phase comprises from 30 to 50 percent by weight of the polypropylene impact copolymer.

2. The propylene impact copolymer of claim 1 wherein the dispersed phase comprises from 30 to 40 percent by weight of the polypropylene impact copolymer.

3. The propylene impact copolymer of claim 1 wherein the matrix comprises a polypropylene homopolymer.

4. The propylene impact copolymer of claim 1 wherein the matrix has an MWD between 4 and 6.

5. The propylene impact copolymer of claim 1 wherein the matrix is a propylene/alpha-olefin random copolymer which comprises more than 90 wt. % of units derived from propylene monomer.

6. The propylene impact copolymer of claim 1 wherein the matrix is a propylene/alpha-olefin random copolymer in which the alpha olefin is ethylene.

7. The propylene impact copolymer of claim 1 wherein the matrix has a crystallinity greater than 60%.

8. The propylene impact copolymer of claim 1 wherein the dispersed polymer comprises at least 50 wt. % of ethylene.

9. The propylene impact copolymer of claim 1 having a melt flow rate of from 1 to 50 g/10 min (230° C./2.16 kg).

10. The propylene impact copolymer of claim 1 which has been vis-broken and the vis-breaking ratio is greater than or equal to 2.

11. The propylene impact copolymer of claim 10 in which the vis-breaking ratio is greater than or equal to 4.

Assignments (13)
NOTES SECURITY INTEREST Recorded Jan 29, 2026
From: W. R. GRACE & CO.-CONN.; ADVANCED REFINING TECHNOLOGIES LLC
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS NOTES COLLATERAL AGENT
Reel/Frame 074532/0229 →
SECURITY AGREEMENT (NOTES) Recorded Aug 19, 2025
From: W. R. GRACE & CO.-CONN.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS NOTES COLLATERAL AGENT
Reel/Frame 072520/0653 →
SECURITY INTEREST Recorded Feb 17, 2023
From: W.R. GRACE & CO.-CONN.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION
Reel/Frame 062792/0510 →
NOTES SECURITY AGREEMENT Recorded Sep 23, 2021
From: W. R. GRACE & CO.-CONN.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION
Reel/Frame 057594/0156 →
RELEASE OF SECURITY INTEREST Recorded Sep 23, 2021
From: GOLDMAN SACHS BANK USA
To: W. R. GRACE & CO.-CONN.
Reel/Frame 057594/0026 →
TERM LOAN SECURITY AGREEMENT Recorded Sep 23, 2021
From: W. R. GRACE & CO.-CONN.
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 057594/0104 →
SECURITY INTEREST Recorded Apr 3, 2018
From: W. R. GRACE & CO.-CONN.
To: GOLDMAN SACHS BANK USA, AS COLLATERAL AGENT
Reel/Frame 045828/0683 →
RELEASE OF SECURITY AGREEMENT RECORDED AT REEL/FRAME NO.: 032159/0384 Recorded Apr 3, 2018
From: GOLDMAN SACHS BANK USA, AS THE COLLATERAL AGENT
To: W.R. GRACE & CO.-CONN.
Reel/Frame 045832/0887 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNEE NAME TO "W. R. GRACE & CO. - CONN." PREVIOUSLY RECORDED ON REEL 032554 FRAME 0730. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNEE NAME WAS PREVIOUSLY INCORRECTLY LISTED IN THE RECORDATION COVER SHEET DATED 3/28/2014 AS "W. R. GRACE & CO. CONN.". Recorded Apr 2, 2014
From: DOW GLOBAL TECHNOLOGIES LLC; UNION CARBIDE CHEMICALS & PLASTICS TECHNOLOGY LLC
To: W. R. GRACE & CO. - CONN.
Reel/Frame 032589/0554 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 28, 2014
From: DOW GLOBAL TECHNOLOGIES LLC; UNION CARBIDE CHEMICALS & PLASTICS TECHNOLOGY LLC
To: W. R. GRACE & CO. CONN.
Reel/Frame 032554/0730 →
SECURITY AGREEMENT Recorded Feb 4, 2014
From: W.R. GRACE & CO.-CONN.
To: GOLDMAN SACHS BANK USA, AS THE COLLATERAL AGENT
Reel/Frame 032159/0384 →
CORRECTIVE ASSIGNMENT TO CORRECT THE INCOMPLETE NAME CONVERSION PAPERWORK WAS UPLOADED. PREVIOUSLY RECORDED ON REEL 026406 FRAME 0192. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Jun 14, 2011
From: CHOU, CHAI-JING
To: DOW GLOBAL TECHNOLOGIES LLC
Reel/Frame 026437/0914 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 8, 2011
From: CHOU, CHAI-JING
To: DOW GLOBAL TECHNOLOGIES LLC
Reel/Frame 026406/0192 →