IP Library Granted Patent US 9,066,867
Granted Patent B2
US 9,066,867 · App. 12/807,707 · Granted Jun 30, 2015

Amphoteric liposomes

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Quick Facts
Patent No.
US 9,066,867
App. No.
12/807,707
Granted
Jun 30, 2015
Kind
B2
Abstract

A serum-stable mixture of lipids capable of encapsulating an active agent to form a liposome, said mixture comprising phosphatidylcholine and phosphatidylethanolamine in a ratio in the range of about 0.5 to about 8. The mixture may also include pH sensitive anionic and cationic amphiphiles, such that the mixture is amphoteric, being negatively charged or neutral at pH 7.4 and positively charged at pH 4. Amphoteric liposomes comprising such a mixture may be used for encapsulating nucleic acid therapeutics, such as oligonucleotides and DNA plasmids. The drug/lipid ratio may be adjusted to target the liposomes to particular organs or other sites in the body.

Claims (16)

1. An amphoteric liposome comprising POPC, MoChol, CHEMS, and DOPE, wherein the amphoteric liposome retains at least 60% of an encapsulated active agent after 4 hours exposure to human serum, wherein MoChol and CHEMS combined comprise 50 to 80 mol % of the amphoteric liposome, wherein POPC and DOPE combined comprise 20 to 50 mol % of the amphoteric liposome, wherein POPC, MoChol, CHEMS, and DOPE combined comprise substantially 100 mol % of the amphoteric liposome, wherein the ratio of DOPE to POPC is from 2 to 4, and wherein the ratio of CHEMS to MoChol is from 0.3 to 0.75.

2. The amphoteric liposome of claim 1 , wherein the liposome consists of a formulation selected from:

POPC/DOPE/MoChol/CHEMS 6:24:47:23 (mol. %)

POPC/DOPE/MoChol/CHEMS 10:30:30:30 (mol. %).

3. The amphoteric liposome of claim 1 , wherein the liposome has a size of from 50 to 500 nm.

4. The amphoteric liposome of claim 1 , wherein the liposome encapsulates at least one active agent.

5. The amphoteric liposome of claim 4 , wherein the active agent comprises a nucleic acid.

6. The amphoteric liposome of claim 4 , wherein the active agent is a circular DNA plasmid, a linear DNA construct, an antisense oligonucleotide, a decoy oligonucleotide, an agent influencing transcription, an agent influencing splicing, a ribozyme, a DNAzyme, or an aptamer.

7. The amphoteric liposome of claim 4 , wherein the active agent is an RNA, an siRNA, an mRNA, an shRNA, or an miRNA.

8. The amphoteric liposome of claim 4 , wherein the active agent comprises one or more modified nucleosides selected from locked nucleic acids (LNA), peptide nucleic acids (PNA), 2′O-methyl RNA (2′Ome), or 2′O-methoxyethyl RNA (2′MOE) in their phosphate or phosphothioate forms.

9. The amphoteric liposome of claim 4 , wherein the active agent modulates expression of CD40 in mammalian cells.

10. A pharmaceutical composition comprising an effective amount of the active agent-loaded amphoteric liposome of claim 4 .

11. A method for treating an inflammatory, immune, or autoimmune disorder in a human in need thereof, the method comprising administering to the human a pharmaceutical composition according to claim 10 .

12. The method of claim 11 , wherein the inflammatory, immune, or autoimmune disorder is graft rejection, graft-versus-host disease, diabetes type I, multiple sclerosis, systemic lupus erythematosous, rheumatoid arthritis, asthma, inflammatory bowel disease, Crohn's disease, ulcerative colitis, psoriasis, thyroiditis, infection, or a solid tumor.

13. The method of claim 11 , wherein the pharmaceutical composition is administered systemically.

14. The method of claim 11 , wherein the pharmaceutical composition is administered locally.

Assignments (10)
RELEASE OF SECURITY INTEREST Recorded Jul 9, 2020
From: MONSANTO COMPANY
To: MARINA BIOTECH, INC.; CEQUENT PHARMACEUTICALS, INC.; MDRNA RESEARCH, INC.
Reel/Frame 053171/0508 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 16, 2020
From: ADHERA THERAPEUTICS, INC.
To: NOVOSOM VERWALTUNGS GMBH
Reel/Frame 052955/0256 →
CHANGE OF NAME Recorded Jun 16, 2020
From: MARINA BIOTECH, INC.
To: ADHERA THERAPEUTICS, INC.
Reel/Frame 052957/0901 →
CHANGE OF NAME Recorded Jun 16, 2020
From: BIONTECH PROTEIN THERAPEUTICS GMBH
To: BIONTECH DELIVERY TECHNOLOGIES GMBH
Reel/Frame 052957/0904 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 16, 2020
From: NOVOSOM VERWALTUNGS GMBH
To: BIONTECH PROTEIN THERAPEUTICS GMBH
Reel/Frame 052958/0867 →
RELEASE OF SECURITY INTEREST Recorded Apr 14, 2014
From: GENESIS CAPITAL MANAGEMENT, LLC, AS AGENT
To: MARINA BIOTECH, INC.; CEQUENT PHARMACEUTICALS, INC.; MDRNA RESEARCH, INC.
Reel/Frame 032685/0158 →
SECURITY AGREEMENT Recorded May 13, 2013
From: MARINA BIOTECH, INC.; CEQUENT PHARMACEUTICALS, INC.; MDRNA RESEARCH, INC.
To: MONSANTO COMPANY
Reel/Frame 030401/0461 →
SECURITY AGREEMENT Recorded Feb 15, 2012
From: MARINA BIOTECH, INC; CEQUENT PHARMACEUTICALS, INC.; MDRNA RESEARCH, INC.
To: GENESIS CAPITAL MANAGEMENT, LLC, AS AGENT
Reel/Frame 027712/0200 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 13, 2011
From: NOVOSOM AG
To: MARINA BIOTECH, INC.
Reel/Frame 025634/0517 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 23, 2010
From: PANZNER, STEFFEN; KERWITZ, YVONNE; RAUCHHAUS, UNA; LUTZ, SILKE; ENDERT, GEROLD
To: NOVOSOM AG
Reel/Frame 025521/0762 →