IP Library Granted Patent US 8,216,383
Granted Patent B2
US 8,216,383 · App. 12/830,854 · Granted Jul 10, 2012

Methods and composition for cleaning a heat transfer system having an aluminum component

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Quick Facts
Patent No.
US 8,216,383
App. No.
12/830,854
Granted
Jul 10, 2012
Kind
B2
Abstract

Disclosed herein is a method and treatment system for rapid cleaning and protecting of automotive cooling systems containing controlled atmosphere brazed aluminum heat exchangers. The method and treatment system can optionally include a conditioning (passivating) step. The treatment system can comprise three different parts: (1) cleaner or cleaning solution; (2) conditioner or conditioning solution; and (3) compatible CAB aluminum protective heat transfer fluid.

Claims (23)

1. A treatment system for a heat transfer system comprising: a cleaner comprising an azole compound and an organic acid having a pKa of less than or equal to 5.0 at 25° C.; and a conditioner separate from the cleaner wherein the conditioner comprises a pyrophosphate, an azole, and an alkaline metal phosphate.

2. The treatment system of claim 1 , wherein the organic acid comprises oxalic acid.

3. The treatment system of claim 1 , further comprising an organic phosphate ester.

4. The treatment system of claim 1 , wherein the cleaner is combined with water to form a cleaning solution.

5. The treatment system of claim 1 further comprising a refill heat transfer fluid.

6. The treatment system of claim 1 wherein the cleaner is a solid.

7. The treatment system of claim 4 , wherein the cleaning solution has a pH less than or equal to 2.0.

8. The treatment system of claim 5 , wherein the refill heat transfer fluid is free of silicate.

9. A treatment system for a heat transfer system comprising:

a cleaner comprising an azole compound and an organic acid having a pKa of less than or equal to 5.0 at 25° C.;

a conditioner separate from the cleaner comprising a pyrophosphate, an azole, and an alkaline metal phosphate;

wherein the cleaner, when diluted with water, has a pH less than or equal to 2.0 at room temperature and the conditioner, when diluted with water, has a pH greater than or equal to 7.5 at room temperature.

10. A method of cleaning a heat transfer system comprising:

draining a heat transfer fluid from the heat transfer system;

filling the heat transfer system with a cleaning solution wherein the cleaning solution comprises an azole compound and an organic acid having a pKa of less than or equal to 5.0 at 25° C.;

circulating the cleaning solution through the heat transfer system;

draining the cleaning solution from the heat transfer system;

filling the heat transfer system with a conditioning solution comprising a pyrophosphate, an azole, and an alkaline metal phosphate; and

circulating the conditioning solution through the heat transfer system,

wherein the heat transfer system comprises a controlled atmosphere brazed component.

11. The method of claim 10 , wherein the cleaning solution has a pH less than or equal to 2.0.

12. The method of claim 10 , wherein the conditioning solution has a pH greater than or equal to 7.5 at room temperature.

13. The method of claim 10 , further comprising draining the conditioning solution and filling the heat transfer system with a heat transfer fluid free of silicate.

Assignments (17)
RELEASE/TERMINATION OF INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Jul 8, 2024
From: WILMINGTON TRUST, NATIONAL ASSOCIATION
To: BIO-LAB, INC.; KIK CUSTOM PRODUCTS INC.; NC BRANDS, L.P.; PRESTONE PRODUCTS CORPORATION
Reel/Frame 068220/0306 →
PARTIAL RELEASE OF SECURITY INTEREST IN INTELLECTUAL PROPERTY Recorded Jun 18, 2024
From: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS NOTES COLLATERAL AGENT
To: PRESTONE PRODUCTS CORPORATION
Reel/Frame 067777/0649 →
RELEASE OF SECURITY INTEREST IN INTELLECTUAL PROPERTY Recorded Jun 18, 2024
From: BARCLAYS BANK PLC, AS COLLATERAL AGENT
To: PRESTONE PRODUCTS CORPORATION
Reel/Frame 067777/0671 →
RELEASE OF SECURITY INTEREST IN INTELLECTUAL PROPERTY Recorded Jun 18, 2024
From: BARCLAYS BANK PLC, AS COLLATERAL AGENT
To: PRESTONE PRODUCTS CORPORATION
Reel/Frame 067777/0751 →
RELEASE OF INTELLECTUAL PROPERTY SECURITY INTEREST Recorded Jul 29, 2021
From: BARCLAYS BANK PLC, AS COLLATERAL AGENT
To: BIO-LAB, INC.; HI-LEX LLC; HOMECARE LABS, INC.; JAMES AUSTIN COMPANY; KIK INTERNATIONAL LLC; NC BRANDS L.P.; PRESTONE PRODUCTS CORPORATION; SOLSKYN PERSONAL CARE LLC; SUNBELT POOL PRODUCTS, LLC
Reel/Frame 057650/0125 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT (NOTES) Recorded Dec 22, 2020
From: BIO-LAB, INC.; KIK CUSTOM PRODUCTS INC.; KIK INTERNATIONAL LLC; PRESTONE PRODUCTS CORPORATION; SOLSKYN PERSONAL CARE LLC; JAMES AUSTIN COMPANY; CYGNUS CORPORATION; NC BRANDS L.P.; AQUA CLEAR INDUSTRIES, LLC; ASEPSIS, INC.; HI-LEX LLC; HOMECARE LABS, INC.; SUNBELT POOL PRODUCTS, LLC
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS NOTES COLLATERAL AGENT
Reel/Frame 055327/0754 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT (2019) Recorded Jan 28, 2019
From: APG, INC.; AQUA CLEAR INDUSTRIES, LLC; ASEPSIS, INC.; BIO-LAB, INC.; HI-LEX LLC; HOMECARE LABS, INC.; KIK CUSTOM PRODUCTS INC.; KIK CUSTOM PRODUCTS, INC; KIK INTERNATIONAL LLC; MARIETTA CORPORATION; PRESTONE PRODUCTS CORPORATION; SOLSKYN PERSONAL CARE LLC; SUNBELT POOL PRODUCTS, LLC; JAMES AUSTIN COMPANY; CBI LABORATORIES, INC.; CYGNUS CORPORATION; NC BRANDS L.P.
To: BARCLAYS BANK PLC, AS AGENT
Reel/Frame 048180/0101 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT (ABL) Recorded Jan 23, 2019
From: PRESTONE PRODUCTS CORPORATION
To: BARCLAYS BANK PLC
Reel/Frame 049518/0001 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT (TERM LOAN) Recorded Jan 23, 2019
From: PRESTONE PRODUCTS CORPORATION
To: BARCLAYS BANK PLC
Reel/Frame 049517/0967 →
RELEASE OF SECURITY INTEREST Recorded Sep 14, 2016
From: BARCLAYS BANK PLC
To: APG, INC.; AQUA CLEAR INDUSTRIES, LLC; ASEPSIS, INC.; BIO-LAB, INC.; CYGNUS CORPORATION; HI-LEX LLC; HOMECARE LABS, INC.; KIK CUSTOM PRODUCTS INC.; KIK CUSTOM PRODUCTS, INC; KIK INTERNATIONAL LLC; MARIETTA CORPORATION; SOLSKYN PERSONAL CARE LLC; KIK NEW JERSEY, LLC; PRESTONE PRODUCTS CORPORATION
Reel/Frame 040031/0793 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Apr 5, 2016
From: APG, INC.; AQUA CLEAR INDUSTRIES, LLC; ASEPSIS, INC.; BIO-LAB, INC.; CYGNUS CORPORATION; HI-LEX LLC; HOMECARE LABS, INC.; KIK CUSTOM PRODUCTS, INC. (TEXAS); KIK CUSTOM PRODUCTS INC. (DELAWARE); KIK INTERNATIONAL LLC; MARIETTA CORPORATION; PRESTONE PRODUCTS CORPORATION; SOLSKYN PERSONAL CARE LLC; KIK NEW JERSEY, LLC
To: BARCLAYS BANK PLC, AS COLLATERAL AGENT
Reel/Frame 038354/0938 →
TERM AND REL OF SEC INT IN PATS-1ST LIEN Recorded Apr 4, 2016
From: CREDIT SUISSE AG, AS COLLATERAL AGENT; PRESTONE PRODUCTS CORPORATION
To: FRAM GROUP IP LLC
Reel/Frame 038337/0741 →
TERM AND REL OF SEC INT IN PATS-2ND LIEN Recorded Apr 4, 2016
From: CREDIT SUISSE AG, AS COLLATERAL AGENT; PRESTONE PRODUCTS CORPORATION
To: FRAM GROUP IP LLC
Reel/Frame 038337/0762 →
SECURITY AGREEMENT Recorded Aug 12, 2011
From: FRAM GROUP IP LLC; PRESTONE PRODUCTS CORPORATION
To: CREDIT SUISSE AG, AS SECOND LIEN COLLATERAL AGENT
Reel/Frame 026740/0089 →
SECURITY AGREEMENT Recorded Aug 11, 2011
From: FRAM GROUP IP LLC; PRESTONE PRODUCTS CORPORATION
To: CREDIT SUISSE AG, AS FIRST LIEN COLLATERAL AGENT
Reel/Frame 026732/0670 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 29, 2011
From: HONEYWELL INTERNATIONAL INC.
To: PRESTONE PRODUCTS CORPORATION
Reel/Frame 026671/0823 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 17, 2010
From: YANG, BO; GERSHUN, ALEKSEI V.; WOYCIESJES, PETER M.
To: HONEYWELL INTERNATIONAL INC.
Reel/Frame 025002/0451 →