IP Library Granted Patent US 8,802,304
Granted Patent B2
US 8,802,304 · App. 12/854,131 · Granted Aug 12, 2014

Bifunctional (rechargeable) air electrodes comprising a corrosion-resistant outer layer and conductive inner layer

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Quick Facts
Patent No.
US 8,802,304
App. No.
12/854,131
Granted
Aug 12, 2014
Kind
B2
Abstract

Performance, properties and stability of bifunctional air electrodes may be improved by using modified current collectors, and improving water wettability of air electrode structures. This invention provides information on creating non-corroding, electrically rechargeable, bifunctional air electrodes. In some embodiments, this bifunctional air electrode includes a corrosion-resistant outer layer and an electrically conductive inner layer. In some embodiments, this bifunctional air electrode includes titanium suboxides formed by reducing titanium dioxide. Titanium suboxides may be corrosion-resistant and electrically conductive.

Claims (35)

1. A bifunctional air electrode for a metal-air battery or cell, said air electrode comprising:

at least one current collector having:

a corrosion-resistant outer layer comprising TiC; and

a conductive inner layer comprising Ti; and

an air permeable, hydrophobic catalytic membrane,

wherein the corrosion-resistant outer layer has a greater corrosion resistance than the conductive inner layer and the conductive inner layer has a higher level of electrical conductivity than the corrosion-resistant outer layer.

2. The bifunctional air electrode of claim 1 , wherein the conductive inner layer is sandwiched within or coated by the corrosion-resistant outer layer.

3. The bifunctional air electrode of claim 1 , wherein the conductive inner layer further comprises at least one of the following: LiVTiO 4 , LiVTiO 3 , or LaTiO 3 .

4. The bifunctional air electrode of claim 1 , wherein fullerenes are electrochemically deposited from either an aqueous or non-aqueous solvent on the current collector.

5. The bifunctional air electrode of claim 1 , wherein carbon nanotubes (CNT) are deposited on the current collector.

6. The bifunctional air electrode of claim 1 , wherein the current collector further comprises glassy carbon that is coated on a substrate with a resin and pyrolysed in an inert atmosphere.

7. The bifunctional air electrode of claim 1 , wherein the corrosion-resistant outer layer comprises a powder coating that coats the conductive inner layer.

8. The bifunctional air electrode of claim 1 , further comprising a porous carbon-based coating on the current collector.

9. The bifunctional air electrode of claim 1 , further comprising a catalytic membrane that includes a catalyst selected from the group consisting of: metals, salts, or compounds containing one or more of the following: Mn, Co, Pt, Mo, Pd, or mixtures thereof.

10. The bifunctional air electrode of claim 1 , wherein the catalytic membrane acts as a catalyst to affect the reduction of oxygen or the generation of oxygen from water.

11. The bifunctional air electrode of claim 10 , wherein the catalytic membrane further comprises an air permeable, silicone rubber.

12. The bifunctional air electrode of claim 10 , wherein the catalytic membrane comprises an air permeable and hydrophobic material comprising at least one of the following: dimethyl silicone, fluorosilicone, nitrile silicone, natural rubber, ethyl cellulose, or low density polyethylene.

13. A bifunctional air electrode for a metal-air battery or cell comprising:

a current collector comprising:

a corrosion-resistant outer layer comprising TiC; and

a conductive inner layer comprising Ti; and

a catalytic membrane that is attached to a surface of the current collector,

wherein the catalytic membrane is air permeable and hydrophobic.

14. The bifunctional air electrode of claim 13 , wherein at least a portion of the conductive inner layer is sandwiched within or coated by the corrosion-resistant outer layer.

15. The bifunctional air electrode of claim 14 , wherein the current collector further comprises a perforated material, an expanded screen, or a woven structure.

16. The bifunctional air electrode of claim 14 , wherein the conductive inner layer further comprises LiVTiO 4 , LiVTiO 3 , LaTiO 3 , or any combination thereof.

17. The bifunctional air electrode of claim 14 , wherein the corrosion-resistant outer layer further comprises a powder coating.

18. The bifunctional air electrode of claim 14 , wherein the catalytic membrane comprises a porous carbon-based coating.

19. The bifunctional air electrode of claim 14 , wherein the catalytic membrane comprises glassy carbon.

20. The bifunctional air electrode of claim 14 , wherein the current collector further comprises fullerenes.

21. The bifunctional air electrode of claim 14 , wherein the current collector further comprises carbon nanotubes.

22. The bifunctional air electrode of claim 14 , wherein the catalytic membrane further comprises a catalyst comprising Mn, Co, Pt, Mo, Pd, any salt thereof, or any mixture thereof.

23. The bifunctional air electrode of claim 14 , wherein the catalytic membrane affects the reduction of oxygen or the generation of oxygen from water.

24. The bifunctional air electrode of claim 14 , wherein the catalytic membrane further comprises an air permeable silicone rubber.

25. The bifunctional air electrode of claim 14 , wherein the catalytic membrane further comprises an air permeable and hydrophobic material comprising dimethyl silicone, fluorosilicone, nitrile silicone, natural rubber, ethyl cellulose, low density polyethylene, or any combination thereof.

Assignments (12)
SECURITY INTEREST Recorded Nov 27, 2024
From: EOS ENERGY TECHNOLOGY HOLDINGS, LLC; EOS ENERGY STORAGE LLC
To: CITIBANK, N.A., AS COLLATERAL AGENT
Reel/Frame 069458/0388 →
TERMINATION AND RELEASE OF PATENT SECURITY AGREEMENT Recorded Jun 24, 2024
From: ACP POST OAK CREDIT I LLC
To: EOS ENERGY STORAGE LLC; EOS ENERGY TECHNOLOGY HOLDINGS, LLC
Reel/Frame 067823/0035 →
SECURITY INTEREST Recorded Jun 24, 2024
From: EOS ENERGY TECHNOLOGY HOLDINGS, LLC; EOS ENERGY STORAGE LLC
To: CCM DENALI DEBT HOLDINGS, LP, AS COLLATERAL AGENT
Reel/Frame 067823/0430 →
CORRECTIVE ASSIGNMENT TO CORRECT THE COVER SHEET US PATENT NO. 7369440 SHOULD HAVE BEEN 7396440 PREVIOUSLY RECORDED ON REEL 048752 FRAME 0864. ASSIGNOR(S) HEREBY CONFIRMS THE SECURITY INTEREST. Recorded Jun 15, 2023
From: EOS ENERGY STORAGE, LLC
To: ALTENERGY STORAGE BRIDGE, LLC
Reel/Frame 064021/0102 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 12, 2022
From: EOS ENERGY STORAGE LLC
To: EOS ENERGY TECHNOLOGY HOLDINGS, LLC
Reel/Frame 061161/0750 →
SECURITY INTEREST Recorded Aug 3, 2022
From: EOS ENERGY STORAGE LLC; EOS ENERGY TECHNOLOGY HOLDINGS LLC
To: ACP POST OAK CREDIT I LLC
Reel/Frame 061056/0282 →
RELEASE OF SECURITY INTEREST Recorded May 25, 2022
From: ALTENERGY STORAGE BRIDGE LLC
To: EOS ENERGY STORAGE LLC
Reel/Frame 060178/0097 →
SECURITY INTEREST Recorded Apr 1, 2019
From: EOS ENERGY STORAGE, LLC
To: ALTENERGY STORAGE BRIDGE, LLC
Reel/Frame 048752/0864 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 16, 2011
From: GRID STORAGE TECHNOLOGIES PARTNERS, LLC
To: EOS ENERGY STORAGE LLC
Reel/Frame 027238/0754 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 16, 2011
From: AMENDOLA, STEVEN; BINDER, MICHAEL; BLACK, PHILIP J.; SHARP-GOLDMAN, STEPHANIE; JOHNSON, LOIS; KUNZ, MICHAEL; OSTER, MICHAEL; CHCIUK, TESIA; JOHNSON, REGAN
To: GRID STORAGE TECHNOLOGIES PARTNERS, LLC
Reel/Frame 027238/0053 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 7, 2011
From: GRID STORAGE TECHNOLOGIES PARTNERS, LLC
To: EOS ENERGY STORAGE LLC
Reel/Frame 026868/0907 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 11, 2010
From: AMENDOLA, STEVEN; BINDER, MICHAEL; BLACK, PHILLIP J.; SHARP-GOLDMAN, STEFANIE; JOHNSON, LOIS; KUNZ, MICHAEL; OSTER, MICHAEL; CHCIUK, TESIA; JOHNSON, REGAN
To: GRID STORAGE TECHNOLOGIES PARTNERS, LLC
Reel/Frame 025354/0102 →