IP Library Granted Patent US 9,683,299
Granted Patent B2
US 9,683,299 · App. 12/857,461 · Granted Jun 20, 2017

Internally reinforced structural composites and associated methods of manufacturing

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Quick Facts
Patent No.
US 9,683,299
App. No.
12/857,461
Granted
Jun 20, 2017
Kind
B2
Abstract

Internally reinforced structural composites, suitable uses for such composites, and associated methods of manufacturing are disclosed herein. In one embodiment, a method of making a reinforced structural component includes forming a precursor having a crystal structure with a plurality of lattice layers and exfoliating the precursor. As a result, a distance between adjacent pairs of the plurality of lattice layers is expanded. The method also includes wrapping the exfoliated precursor with a surface support material around at least a portion of a circumference of the individual lattice layers in the exfoliated precursor.

Claims (27)

1. A method of making a reinforced structural component, comprising:

forming a precursor having a crystal structure with a plurality of lattice layers, wherein forming the precursor further includes forming a graphite crystal having a plurality of layers of carbon atoms, the layers being arranged along a longitudinal axis and separated from one another by a distance;

implanting an interstitial exfoliation agent between at least some of the plurality of lattice layers;

exfoliating the precursor with the implanted interstitial exfoliation agent at an exfoliating temperature;

forming a surface support material around at least a portion of a circumference of the plurality of lattice layers in the exfoliated precursor wherein forming the surface support material includes attaching one or more layers of an adhesively coated graphite film to the plurality of lattice layers;

coating the one or more graphite film with diamond-like carbon; and

reordering the diamond-like carbon to graphite.

2. The method of claim 1 wherein:

forming a surface support material includes attaching glass fibers to at least a portion of the circumference of the plurality of lattice layers with an adhesive.

3. The method of claim 1 wherein:

forming a surface support material includes attaching one or more layers of a pyrolytic graphite film to at least a portion of the circumference of the plurality of lattice layers.

4. The method of claim 1 wherein:

the adhesively coated graphite film includes an adhesively coated pyrolytic graphite film; and

forming the surface support material includes attaching one or more layers of the adhesively coated pyrolytic graphite film to at least a portion of the circumference of the plurality of lattice layers.

5. The method of claim 1 wherein:

the method further includes coating the one or more graphite film with at least one of a braze metal material and a braze metal alloy, the braze metal material and the braze metal alloy including one or more of copper, nickel, cobalt, and aluminum.

6. The method of claim 1 wherein: forming a surface support material includes diffusion bonding the coated graphite films to the exfoliated precursor.

7. The method of claim 1 wherein:

forming a surface support material includes attaching one or more layers of an adhesively coated pyrolytic graphite film to at least a portion of the circumference of the plurality of lattice layers;

coating the one or more graphite film with diamond-like carbon via chemical vapor deposition using a precursor gas; and

adjusting chemistry of the precursor gas and doping the diamond-like carbon with at least one of oxygen, fluorine, hydrogen, phosphorous, and silicon.

8. A method of making a reinforced structural component, comprising:

forming a precursor having a crystal structure with a plurality of lattice layers, wherein each lattice layer of the plurality of lattice layers is arranged parallel to and at a distance from another lattice layer of the plurality of lattice layers;

exfoliating the precursor using an interstitial exfoliation agent between at least some of the plurality of lattice layers, thereby expanding the distance between adjacent pairs of the plurality of lattice layers such that the adjacent pairs of the plurality of lattice layers are spaced apart by the expanded distance;

wrapping the exfoliated precursor with a surface support material around at least a portion of an outer perimeter of the plurality of lattice layers in the exfoliated precursor for stabilizing the spaced apart lattice layers, wherein forming the surface support material includes attaching one or more layers of a graphite film to the plurality of lattice layers;

coating the one or more graphite film with diamond-like carbon; and

reordering the diamond-like carbon to graphite.

Assignments (6)
SECURITY INTEREST Recorded Jul 24, 2019
From: MCALISTER TECHNOLOGIES, LLC
To: PERKINS COIE LLP
Reel/Frame 049846/0329 →
SECURITY INTEREST Recorded Jan 28, 2019
From: MCALISTER TECHNOLOGIES, LLC
To: PERKINS COIE LLP
Reel/Frame 049509/0721 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 29, 2018
From: MCALISTER, ROY EDWARD
To: MCALISTER TECHNOLOGIES, LLC
Reel/Frame 045763/0233 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 9, 2015
From: ADVANCED GREEN TECHNOLOGIES, LLC.
To: ADVANCED GREEN INNOVATIONS, LLC
Reel/Frame 036827/0530 →
TERMINATION OF LICENSE AGREEMENT Recorded Jul 23, 2015
From: MCALISTER, ROY EDWARD
To: MCALISTER TECHNOLOGIES, LLC
Reel/Frame 036176/0079 →
AGREEMENT Recorded Jul 14, 2015
From: MCALISTER, ROY E., MR; MCALISTER TECHNOLOGIES, LLC
To: ADVANCED GREEN TECHNOLOGIES, LLC
Reel/Frame 036103/0923 →