IP Library Granted Patent US 8,785,044
Granted Patent B2
US 8,785,044 · App. 12/869,244 · Granted Jul 22, 2014

Lithium-iron disulfide cathode formulation having pyrite content and low conductive additives

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Quick Facts
Patent No.
US 8,785,044
App. No.
12/869,244
Granted
Jul 22, 2014
Kind
B2
Abstract

The invention relates to primary electrochemical cells having a jellyroll electrode assembly that includes a lithium-based negative electrode, a positive electrode with a coating comprising iron disulfide deposited on a current collector and a polymeric separator. More particularly, the invention relates to a cell designs and cathode formulations incorporating specific types of conductors to improve cell performance.

Claims (26)

1. An electrochemical cell comprising:

a cylindrical housing;

a nonaqueous electrolyte including an organic solvent and a spiral wound electrode assembly disposed within the housing;

wherein the spiral wound electrode assembly includes an anode consisting essentially of lithium or a lithium alloy and a cathode mix coated onto a foil current collector at a final solids packing percentage of at least 58% and no more than 63%;

wherein the cathode mix comprises at least 95 wt. % of pyrite, less than 2 wt. % of a binder and less than or equal to 2 wt. % of conductors; and

wherein the conductors include graphite and at least 50 wt. % of acetylene black.

2. The electrochemical cell according to claim 1 , wherein the graphite is mechanically expanded graphite.

3. The electrochemical cell according to claim 1 , wherein the cathode mix consists essentially of 95-98 wt. % pyrite, 1-2 wt. % conductors and less than 2 wt. % of a binder and, optionally, processing aids.

4. The electrochemical cell according to claim 1 , wherein the cathode mix comprises at least 96 wt. % of pyrite.

5. The electrochemical cell according to claim 1 , wherein the solids packing percentage is at least 58% and no more than 60%.

6. The electrochemical cell according to claim 1 , wherein the conductor includes lactonic or phenolic functional groups.

7. The electrochemical cell according to claim 1 , wherein the conductor includes functional groups at a concentration of less than about 50 μg of functional group/g of conductor.

8. The electrochemical cell according to claim 1 , wherein the conductors include at least 55 wt. % of acetylene black.

9. An electrochemical cell comprising:

a cylindrical housing;

a nonaqueous electrolyte including an organic solvent and a spiral wound electrode assembly disposed within the housing;

wherein the spiral wound electrode assembly includes an anode consisting essentially of lithium or a lithium alloy and a cathode mix coated onto a foil current collector at a final solids packing percentage of at least 58% and no more than 63%;

wherein the cathode mix comprises at least 95 wt. % of pyrite, less than 2 wt. % of a binder and less than or equal to 2 wt. % of conductors; and

wherein the conductors include graphitized carbon and graphite.

10. The electrochemical cell according to claim 9 , wherein the graphitized carbon comprises at least 50 wt. % of the conductors.

11. The electrochemical cell according to claim 9 , wherein the graphite is mechanically expanded graphite.

12. The electrochemical cell according to claim 9 , wherein the cathode mix is coated to a solids packing percentage between at least 58% and no more than 60%.

13. The electrochemical cell according to claim 9 , wherein the cathode mix comprises at least 96 wt. % of pyrite.

14. The electrochemical cell according to claim 9 , wherein the conductor includes lactonic or phenolic functional groups.

15. The electrochemical cell according to claim 9 , the conductor includes functional groups at a concentration of less than about 50 μg of functional group/g of conductor.

16. The electrochemical cell according to claim 9 , wherein the cathode mix consists essentially of 95-98 wt. % pyrite, 1-2 wt. % conductors and less than 2 wt. % of a binder and, optionally, processing aids.

Assignments (8)
AMENDED AND RESTATED INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Mar 19, 2025
From: ENERGIZER BRANDS, LLC; ENERGIZER AUTO, INC.,; ENERGIZER AUTO SALES, INC.
To: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
Reel/Frame 070565/0282 →
PATENT SECURITY AGREEMENT Recorded Dec 30, 2020
From: ENERGIZER BRANDS, LLC; ENERGIZER AUTO, INC.
To: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 054875/0651 →
PATENT SECURITY AGREEMENT Recorded Jan 8, 2019
From: ENERGIZER HOLDINGS, INC.; AMERICAN COVERS, LLC; ASSOCIATED PRODUCTS, LLC; CALIFORNIA SCENTS, LLC; ENERGIZER BRANDS, LLC; ENERGIZER MANUFACTURING, INC.
To: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 048029/0246 →
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENT RIGHTS Recorded Jan 8, 2019
From: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
To: ENERGIZER BRANDS, LLC
Reel/Frame 048888/0300 →
CORRECTIVE ASSIGNMENT TO CORRECT THE APPLICATION NUMBER 29/499,135 PREVIOUSLY RECORDED AT REEL: 036019 FRAME: 814. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Sep 16, 2016
From: EVEREADY BATTERY COMPANY
To: ENERGIZER BRANDS, LLC
Reel/Frame 040054/0660 →
SECURITY AGREEMENT Recorded Jul 15, 2015
From: ENERGIZER BRANDS, LLC
To: JPMORGAN CHASE BANK, N.A., AS AGENT
Reel/Frame 036106/0392 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 26, 2015
From: EVEREADY BATTERY COMPANY, INC.
To: ENERGIZER BRANDS, LLC
Reel/Frame 036019/0814 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 27, 2010
From: MARPLE, JACK W; HUANG, WEIWEI; WEMPLE, MICHAEL W.
To: EVEREADY BATTERY COMPANY, INC.
Reel/Frame 025045/0548 →