IP Library Granted Patent US 8,435,345
Granted Patent B2
US 8,435,345 · App. 12/892,239 · Granted May 7, 2013

Internally curing cement based materials

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Quick Facts
Patent No.
US 8,435,345
App. No.
12/892,239
Granted
May 7, 2013
Kind
B2
Abstract

A method of curing cementitious material comprising added a carboxylated bleached wood pulp fiber to the material during mixing. The fiber has a carboxyl content of from 10 to 70 meq/100 g cellulose fiber. The fibers are 0.1 to 5% by weight of the dry weight of the cementitious material. The structure produced by the method. The autogenous shrinkage of the cementitious material is reduced.

Claims (23)

1. A method of curing cement to reduce autogenous shrinkage comprising:

providing a mixture comprising cementitious material, water and carboxylated bleached wood pulp fiber;

allowing the mixture to cure;

the cementitious material comprises cement;

the carboxylated fibers have a carboxyl content of 10 to 70 meq/100 g of cellulose fiber;

the carboxylated fibers are 0.1 to 5% by weight of the dry weight of the cementitious material;

the carboxylated fibers are made by the oxidation process and stabilized to convert aldehyde groups to carboxyl groups; and,

the water to cement material ratio is a high performance concrete ratio.

2. The method of claim 1 , wherein the fibers have a carboxyl content of 20 to 60 meq/100 g of cellulose fiber.

3. The method of claim 1 , wherein the fibers have a carboxyl content of 30 to 50 meq/100 g of cellulose fiber.

4. The method of claim 1 , wherein the fibers are 025 to 0.75% by weight of the dry weight of the cementitious material.

5. The method of claim 1 , wherein the cementitious material further comprises aggregate material.

6. The method of claim 5 , wherein the fibers have a carboxyl content of 20 to 60 meq/100 g of cellulose fiber.

7. The cementitious structure of claim 5 wherein the fibers have, a carboxyl content of 30 to 50 meq/100 g of cellulose fiber.

8. The cementitious structure of claim 5 , wherein the fibers have a carboxyl content of 35 to 45 meq/100 g of cellulose fiber.

9. The method of claim 5 , wherein the fibers are 0.25 to 0.75 by weight of the dry weight of the cementitious material.

10. A method of reducing the autogenous shrinkage of cement or concrete comprising:

providing a mixture comprising cementitious material, water and carboxylated bleached wood pulp fiber;

allowing the mixture to cure;

the carboxylated fibers have a carboxyl content of 10 to 70 meq/100 g of cellulose fiber;

the carboxylated fibers are 0.1 to 5% by weight of the dry weight of the cementitious material;

the carboxylated fibers are made by the oxidation process and stabilized to convert aldehyde groups to carboxyl groups; and

the water to cement material ratio is a high performance concrete ratio.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 5, 2019
From: WEYERHAEUSER NR COMPANY
To: INTERNATIONAL PAPER COMPANY
Reel/Frame 049964/0838 →