Formable sealant barrier
View Patent ↗In one embodiment of the present invention, an assembly for HPHT processing comprises a can with an opening. A powder mixture is disposed within the opening. A substrate is disposed within the opening adjacent the powder mixture. Paint is coated on a surface within the opening and opposite the powder mixture with respect to the substrate. A meltable sealant is disposed within the opening and opposite the substrate with respect to the surface and a cap is covering the opening. In another embodiment of the present invention, an assembly for HPHT processing comprises a can with an opening, a powder mixture is disposed within the opening, a substrate disposed within the opening adjacent and above the powder mixture, a formable sealant barrier is disposed within the opening above the substrate, a meltable sealant is disposed within the opening above the formable sealant barrier, and a cap covers the opening.
1. A method of preparing an assembly for HPHT processing, comprising:
providing an assembly comprising a can with an opening and a powder mixture disposed within the opening, a substrate being adjacent the powder mixture, a formable sealant barrier positioned opposite the powder mixture from the substrate; a meltable sealant disposed intermediate the sealant barrier and a cap covering the opening;
heating the assembly to a cleansing temperature for a first period of time;
further heating the assembly to a sealing temperature for a second period of time;
bringing the assembly to a pressure higher than atmospheric pressure; and
bringing the assembly back to atmospheric pressure at a temperature sufficient to melt the sealant.
2. The method of claim 1 , wherein the heating is performed in a vacuum.
3. The method of claim 1 , wherein the further heating is performed in an inert gas.
4. The method of claim 1 , wherein the cleansing temperature is between 800° C. and 1050° C.
5. The method of claim 1 , wherein the sealing temperature is between 1000° C. and 1200° C.
6. The method of claim 1 , wherein the first period of time is between 15 minutes and 60 minutes.
7. The method of claim 1 , wherein the second period of time is between 2 minutes and 25 minutes.