IP Library Granted Patent US 8,791,101
Granted Patent B2
US 8,791,101 · App. 12/917,066 · Granted Jul 29, 2014

Aryl- and heteroaryl-substituted tetrahydrobenzazepines and use thereof to block reuptake of norepinephrine, dopamine, and serotonin

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Quick Facts
Patent No.
US 8,791,101
App. No.
12/917,066
Granted
Jul 29, 2014
Kind
B2
Abstract

The compounds of the present invention are represented by the following aryl- and heteroaryl-substituted tetrahydrobenzazepine and dihydrobenzazapine derivatives having formulae I(A-E) and formula (II): where the carbon atom designated * is in the R or S configuration, and the substituents X and R 1 -R 9 are as defined herein.

Claims (51)

1. A compound of formulae I(A-E) having the following structure:

wherein:

the carbon atom designated * is in the R or S configuration; and

X is phenyl, optionally substituted from 1 to 4 times with substituents as defined below in R 14 ;

R 1 is H or C 1 -C 6 alkyl;

R 2 is H;

R 3 is H;

R 4 is pyridazinyl, optionally substituted from 1 to 4 times with substituents as defined below in R 14 ;

R 5 is H;

R 6 is H;

R 7 is H;

R 8 is H;

R 9 is H; and

R 14 is independently selected at each occurrence from a substituent in the group consisting of halogen and C 1 -C 6 alkyl, wherein C 1 -C 6 alkyl is optionally substituted from 1 to 3 times with halogen,

or an oxide thereof, or a pharmaceutically acceptable salt thereof.

2. The compound according to claim 1 , wherein R 1 is H.

3. The compound according to claim 1 , wherein R 1 is methyl.

4. The compound according to claim 1 , wherein R 4 pyridazin-3-yl, 6-methylpyridazin-3-yl, or 6-(trifluoromethyl)pyridazin-3-yl.

5. The compound according to claim 4 , wherein R 4 is 6-(trifluoromethyl)pyridazin-3-yl.

6. The compound according to claim 1 , wherein R 14 is fluorine or chlorine.

7. The compound according to claim 1 , wherein X is disubstituted with R 14 and wherein R 14 at each occurrence is a halogen.

8. The compound according to claim 1 , wherein the carbon atom designated * is in the R configuration.

9. The compound according to claim 1 , wherein the carbon atom designated * is in the S configuration.

10. The compound according to claim 1 , wherein the compound is a (+) stereoisomer.

11. The compound according to claim 1 , wherein the compound is a (−) stereoisomer.

12. A pharmaceutical composition comprising a pharmaceutically acceptable carrier and a therapeutically effective amount of the compound according to claim 1 .

13. A method of treating a disorder which is created by or is dependent upon decreased availability of norepinephrine, dopamine, or serotonin, said method comprising:

administering to a patient in need of such treatment a therapeutically effective amount of a compound according to claim 1 or a pharmaceutically acceptable salt thereof, wherein the disorder is selected from the group consisting of: lower back pain, attention deficit hyperactivity disorder (ADHD), cognition impairment, anxiety disorders, generalized anxiety disorder (GAD), panic disorder, bipolar disorder or manic depression or manic-depressive disorder, obsessive compulsive disorder (OCD), posttraumatic stress disorder (PTSD), acute stress disorder, social phobia, simple phobias, pre-menstrual dysphoric disorder (PMDD), social anxiety disorder (SAD), major depressive disorder (MDD), postnatal depression, dysthymia, depression associated with Alzheimer's disease, Parkinson's disease, or psychosis, supranuclear palsy, eating disorders, obesity, anorexia nervosa, bulimia nervosa, binge eating disorder, analgesia, nicotine addiction, cocaine addiction, alcohol and amphetamine addiction, Lesch-Nyhan syndrome, Parkinson's disease, late luteal phase syndrome or narcolepsy, psychiatric symptoms, anger, rejection sensitivity, movement disorders, extrapyramidal syndrome, Tic disorders, restless leg syndrome (RLS), tardive dyskinesia, supranuclear palsy, sleep related eating disorder (SRED), night eating syndrome (NES), stress urinary incontinence (SUI), migraine, neuropathic pain, diabetic neuropathy, fibromyalgia syndrome (FS), chronic fatigue syndrome (CFS), sexual dysfunction, premature ejaculation, male impotence, and thermoregulatory disorders.

14. The method according to claim 13 , further comprising:

administering a therapeutically effective amount of WAY 100135 or spiperone.

15. The method according to claim 13 , further comprising:

administering a therapeutically effective amount of L-tyrosine or L-phenylalanine.

16. The method according to claim 13 , wherein the disorder is lower back pain.

17. The method according to claim 13 , wherein the disorder is attention deficit hyperactivity disorder.

18. The method according to claim 13 , wherein the disorder is anxiety disorder.

19. The method according to claim 13 , wherein the disorder is bipolar disorder or manic depressive disorder.

20. The method according to claim 13 , wherein the disorder is major depressive disorder.

21. The method according to claim 13 , wherein the disorder is postnatal depression.

22. The method according to claim 13 , wherein the disorder is dysthymia.

23. The method according to claim 13 , wherein the disorder is depression associated with Alzheimer's disease, Parkinson's disease, or psychosis.

24. The method according to claim 13 , wherein the disorder is eating disorder.

25. The method according to claim 13 , wherein the disorder is obesity.

26. The method according to claim 13 , wherein the disorder is Parkinson's disease.

27. The method according to claim 13 , wherein the disorder is neuropathic pain.

28. The method according to claim 13 , wherein the disorder is diabetic neuropathy.

29. The method according to claim 13 , wherein the disorder is fibromyalgia syndrome.

30. The method according to claim 13 , wherein the disorder is sexual dysfunction.

31. The method according to claim 13 , wherein the disorder is premature ejaculation.

32. The method according to claim 13 , wherein the disorder is stress urinary incontinence.

33. The method according to claim 13 , wherein the disorder is thermoregulatory disorder.

34. The method according to claim 33 , wherein the thermoregulatory disorder is hot flashes.

Assignments (13)
ASSIGNMENT OF SECURITY INTEREST IN INTELLECTUAL PROPERTY, RECORDED ON SEPTEMBER 1, 2017, AT REEL/FRAME 043746/0621 Recorded Mar 17, 2025
From: BARCLAYS BANK PLC, AS EXISTING AGENT
To: APOLLO ADMINISTRATIVE AGENCY LLC, AS SUCCESSOR AGENT
Reel/Frame 070531/0279 →
SECURITY INTEREST Recorded Sep 6, 2021
From: CURIA GLOBAL, INC. (FKA ALBANY MOLECULAR RESEARCH, INC.); CURIA MASSACHUSETTS, INC. (FKA AMRI BURLINGTON, INC.); CURIA WISCONSIN, INC. (FKA CEDARBURG PHARMACEUTICALS, INC.); CURIA INDIANA, LLC (FKA AMRI SSCI, LLC); CURIA NEW MEXICO, LLC (FKA OSO BIOPHARMACEUTICALS MANUFACTURING, LLC); CURIA IP HOLDINGS, LLC
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 057423/0665 →
RELEASE OF SECURITY INTEREST Recorded Oct 29, 2020
From: MORGAN STANLEY SENIOR FUNDING, INC., AS COLLATERAL AGENT
To: ALBANY MOLECULAR RESEARCH, INC.; AMRI BURLINGTON, INC.; CEDARBURG PHARMACEUTICALS, INC.; EUTICALS INC.; OSO BIOPHARMACEUTICALS MANUFACTURING, LLC
Reel/Frame 054252/0687 →
CORRECTIVE ASSIGNMENT TO CORRECT THE INCORRECT PATENT NO. 7541537 PREVIOUSLY RECORDED AT REEL: 034045 FRAME: 0951. ASSIGNOR(S) HEREBY CONFIRMS THE SECURITY INTEREST. Recorded Aug 14, 2018
From: ALBANY MOLECULAR RESEARCH, INC.; ALO ACQUISITION LLC; AMRI BURLINGTON, INC.; AMRI RENSSELAER, INC.; CEDARBURG PHARMACEUTICALS, INC.; OSO BIOPHARMACEUTICALS MANUFACTURING, LLC
To: BARCLAYS BANK PLC, AS THE COLLATERAL AGENT
Reel/Frame 046796/0352 →
SECOND LIEN SECURITY AGREEMENT Recorded Sep 1, 2017
From: ALBANY MOLECULAR RESEARCH, INC.; AMRI BURLINGTON, INC.; CEDARBURG PHARMACEUTICALS, INC.; EUTICALS INC.; OSO BIOPHARMACEUTICALS MANUFACTURING LLC-BY ITS SOLE MEMBER:ALO ACQUISITION LLC
To: MORGAN STANLEY SENIOR FUNDING, INC.
Reel/Frame 043746/0657 →
FIRST LIEN SECURITY AGREEMENT Recorded Sep 1, 2017
From: ALBANY MOLECULAR RESEARCH, INC.; AMRI BURLINGTON, INC.; CEDARBURG PHARMACEUTICALS, INC.; EUTICALS INC.; OSO BIOPHARMACEUTICALS MANUFACTURING, LLC-BY ITS SOLE MEMBER: ALO ACQUISITION LLC
To: BARCLAYS BANK, PLC AS COLLATERAL AGENT
Reel/Frame 043746/0621 →
RELEASE OF SECURITY INTEREST Recorded Aug 31, 2017
From: BARCLAYS BANK PLC, AS COLLATERAL AGENT
To: ALBANY MOLECULAR RESEARCH, INC.; ALO ACQUISITION LLC; AMRI BURLINGTON, INC.; AMRI RENSSELAER, INC.; CEDARBURG PHARMACEUTICALS, INC.; OSO BIOPHARMACEUTICALS MANUFACTURING, LLC; AMRI SSCI, LLC; EUTICALS INC.
Reel/Frame 043742/0085 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 22, 2016
From: BRISTOL-MYERS SQUIBB COMPANY
To: ALBANY MOLECULAR RESEARCH, INC.
Reel/Frame 039116/0827 →
SECURITY INTEREST Recorded Oct 24, 2014
From: ALBANY MOLECULAR RESEARCH, INC.; ALO ACQUISITION LLC; AMRI BURLINGTON, INC.; AMRI RENSSELAER, INC.; CEDARBURG PHARMACEUTICALS, INC.; OSO BIOPHARMACEUTICALS MANUFACTURING, LLC
To: BARCLAYS BANK PLC, AS THE COLLATERAL AGENT
Reel/Frame 034045/0951 →
RELEASE OF SECURITY INTEREST Recorded Jul 9, 2014
From: WELLS FARGO
To: ALBANY MOLECULAR RESEARCH, INC.
Reel/Frame 033283/0357 →
SECURITY AGREEMENT Recorded Apr 20, 2012
From: ALBANY MOLECULAR RESEARCH, INC.; AMRI BURLINGTON, INC.; AMRI BOTHELL RESEARCH CENTER, INC.; AMRI RENESSELAER, INC.
To: WELLS FARGO BANK, NATIONAL ASSOCIATION
Reel/Frame 028078/0227 →
TERMINATION Recorded Apr 19, 2012
From: BANK OF AMERICA, N.A.
To: ALBANY MOLECULAR RESEARCH, INC.; AMRI BOTHELL RESEARCH CENTER, INC.; AMRI BURLINGTON, INC.; AMRI RENESSELAER, INC.
Reel/Frame 028072/0335 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Jun 6, 2011
From: ALBANY MOLECULAR RESEARCH, INC.; AMRI RENSSELAER, INC.; AMRI BOTHELL RESEARCH CENTER, INC.; AMRI BURLINGTON, INC.
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