IP Library Granted Patent US 8,466,257
Granted Patent B2
US 8,466,257 · App. 12/918,262 · Granted Jun 18, 2013

Process and apparatus for purifying solid salt compositions

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Quick Facts
Patent No.
US 8,466,257
App. No.
12/918,262
Granted
Jun 18, 2013
Kind
B2
Abstract

Methods and apparatus for the recovery and purification of solid salt compositions from an organic liquid containing epoxy resin and at least one of epihalohydrin and solvent to obtain purified salt and/or brine compositions that may be useful in industrial processes.

Claims (15)

1. A method for purifying a solid salt composition, the method comprising:

separating the solid salt from an organic liquid containing epoxy resin and at least one of epihalohydrin and solvent to obtain a separated solid salt;

washing the separated solid salt with at least one solvent to reduce an amount of epoxy resin retained in the solid salt;

drying the washed salt at a temperature to reduce an amount of volatile components in the solid salt to obtain a solid salt having a reduced content of volatile components;

dissolving the solid salt having a reduced content of volatile components in water forming brine; and

removing insoluble material from the brine by filtration or dissolved air flotation and then removing soluble organic contaminants by carbon adsorption to form a purified brine wherein the insoluble material is a polymer byproduct or epoxy resin.

2. The method of claim 1 , wherein a filter aid is used to improve removal of insoluble material by filtration.

3. The method of claim 2 , wherein the filter aid is selected from diatomaceous earth, perlite and calcined rice hull.

4. The method of claim 1 , wherein the purified brine has a Total Organic Content of 10 ppm or less.

5. A method for purifying a solid salt composition comprising:

separating the solid salt from an organic liquid containing epoxy resin and at least one of epihalohydrin and solvent to obtain a separated solid salt;

washing the separated solid salt with at least one solvent to reduce an amount of epoxy resin retained in the solid salt;

dissolving the solid salt comprising reduced volatile components in water forming brine;

distilling the brine to remove the volatile organic components; and

removing at least one of insoluble material and then removing soluble organic contaminants from the brine to form a purified brine wherein the insoluble material is a polymer byproduct or epoxy resin.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 11, 2015
From: DOW GLOBAL TECHNOLOGIES LLC
To: BLUE CUBE IP LLC
Reel/Frame 035887/0193 →