Method and apparatus for forming nano-particles
View Patent ↗Nano-scale particles of materials can be produced by vaporizing material and allowing the material to flow in a non-violently turbulent manner into thermal communication with a cooling fluid, thereby forming small particles of the material that can be in the nano-scale size range. A raw material feeder can be configured to feed raw material toward a heater which vaporizes the raw material. The feeder can include a metering device for controlling the flow of raw material toward the heater. A gas source can also be used to cause gas to flow through a portion of the raw material feeder along with the raw material.
1. A nano-scale particle generator comprising:
a first heating device configured to vaporize raw material;
a raw material feeder configured to feed a raw material into contact with the first heating device and to feed a gas along with the raw material through the raw material feeder, wherein the raw material feeder device comprises a conduit configured to guide the raw material and the gas toward the first heating device; and
a heat shield disposed at an end of the conduit proximate the first heater.
2. A nano-scale particle generator comprising:
a first heating device configured to vaporize raw material;
a raw material feeder configured to feed a raw material into contact with the first heating device and to feed a gas along with the raw material through the raw material feeder, wherein the raw material feeder device comprises a conduit configured to guide the raw material and the gas toward the first heating device; and
a member disposed at an end of the conduit proximate the first heater, the member configured to define a gap between a portion of an outer surface of the conduit and an inner surface of the member.
3. The generator according to claim 2 , wherein the conduit comprises an aperture opening into the gap.
4. The generator according to claim 3 , wherein the aperture is sized to allow the gas to flow through the aperture and into the gap and to prevent the raw material from flowing into the gap.
5. A nano-scale particle generator comprising:
a first heating device configured to vaporize raw material; and
a raw material feeder configured to feed a raw material into contact with the first heating device, the raw material feeder comprising a moveable receptacle defining a cavity.
6. The generator according to claim 5 , wherein the cavity is configured to have an adjustable volume and is configured to be movable between an upright orientation and an inverted orientation.
7. The generator according to claim 6 , wherein the cavity is in fluidic communication with a reservoir of raw material when the cavity is in the upright orientation and wherein the cavity is in fluidic communication with the heating device when it is in the inverted orientation.
8. The generator according to claim 7 , wherein the raw material feeder comprises a conduit extending from the cavity toward the first heating device.
9. The generator according to claim 8 , additionally comprising a gas source connected to the conduit downstream from the cavity, the gas source being configured to feed a gas into the conduit such that the gas can flow through the conduit along with the raw material in parallel.
10. A nano-scale particle generator comprising:
a heater device configured to vaporize a raw material;
a controller configured to maintain the heater device at a first temperature to and lower the temperature of the heater device to a second temperature that is lower than the first temperature; and
a raw material feeder device configured to feed a raw material toward the heater device;
wherein the controller is configured to maintain the temperature of the heater device at the first temperature which is sufficiently high so as to vaporize the raw material, to lower the temperature of the heater device to a temperature at or less than the second temperature before the raw material feeder device feeds additional raw material toward the heater device, and to raise the temperature of the heater device after the feeder device has fed the raw material toward the heater device.
11. The generator according to claim 10 , wherein the controller is configured to allow at least some of the additional raw material to melt before raising the temperature of the heater device to the first temperature.
12. The generator according to claim 10 , wherein the first temperature is about 1900° F. and the second temperature being about 1700° F., and wherein the raw material is granular manganese.
13. A nano-scale particle generator comprising:
a first heating device configured to vaporize raw material; and
means for feeding raw material and a gas together toward the first heating device, wherein the means for feeding includes an outlet end, the generator further comprising means for shielding the outlet end from heat from the first heater.