IP Library Granted Patent US 8,859,035
Granted Patent B1
US 8,859,035 · App. 12/962,463 · Granted Oct 14, 2014

Powder treatment for enhanced flowability

Inventor: David Leamon (Gilbert, AZ)
Assignee: SDCmaterials, Inc.
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Quick Facts
Patent No.
US 8,859,035
App. No.
12/962,463
Granted
Oct 14, 2014
Kind
B1
Abstract

A method of enhancing the flowability of a powder. The powder is defined by a plurality of particles having an initial level of inter-particle forces between each particle. The method comprises: treating the powder, wherein the level of inter-particle forces between each particle is substantially decreased from the initial level; fluidizing the treated powder; flowing the treated powder into a plasma arc chamber; the plasma arc chamber generating a plasma arc; and the plasma arc chamber operating on the treated powder using the generated plasma arc. Preferably, the inter-particle forces are decreased by coating the particles with an organic surfactant.

Claims (45)

1. A method of enhancing the flowability of a powder to produce nanoparticles, the powder defined by a plurality of particles having an initial level of inter-particle forces between each particle, the method comprising:

coating the powder with an organic material, wherein the level of inter-particle forces between each particle is substantially decreased from the initial level;

fluidizing the coated powder;

flowing the coated powder into a plasma arc chamber;

the plasma arc chamber generating a plasma arc;

the generated plasma arc vaporizing the coated powder

in order to nano-size the powder to produce nanoparticles.

2. The method of claim 1 , wherein the organic material is a surfactant.

3. The method of claim 2 , wherein the surfactant is sorbitan monooleate.

4. The method of claim 3 , wherein each particle in the plurality of particles is a non-oxide.

5. The method of claim 1 , wherein each particle in the plurality of particles is an oxide and the organic material is a material selected from the group consisting of trialkoxysilane, alkyltrialkoxysilane, trialkylalkoxysilane, trialkyldimethylaminosilane, trialkylchlorosilane, and octyltriethoxysilane.

6. The method of claim 1 , wherein coating the powder comprises:

disposing the powder in a solvent within a container, wherein the solvent comprises the organic material;

agitating the combination of the powder and the solvent in the container;

coating the plurality of particles with the organic material; and

separating substantially all of the remaining solvent from the coated powder.

7. The method of claim 6 , wherein the organic material is a surfactant.

8. The method of claim 7 , wherein the surfactant is sorbitan monooleate.

9. The method of claim 8 , wherein each particle in the plurality of particles is a non-oxide.

10. The method of claim 8 , wherein the solvent further comprises a hydrocarbon.

11. The method of claim 10 , wherein the hydrocarbon is toluene.

12. The method of claim 10 , wherein the hydrocarbon is cyclohexane.

13. The method of claim 6 , wherein each particle in the plurality of particles is an oxide and the organic material is a material selected from the group consisting of trialkoxysilane, alkyltrialkoxysilane, trialkylalkoxysilane, trialkyldimethylaminosilane, trialkylchlorosilane, and octyltriethoxysilane.

14. The method of claim 6 , wherein separating substantially all of the solvent from the coated powder comprises decanting substantially all of the remaining solvent from the container.

15. The method of claim 14 , further comprising the step of drying the coated powder.

16. The method of claim 15 , wherein the step of drying comprises applying heat and vacuum pressure to the coated powder.

17. A method of enhancing the flowability of a powder to produce nanoparticles, the powder defined by a plurality of particles having an initial level of inter-particle forces between each particle, the method comprising:

disposing the powder in a solvent within a container, wherein the solvent comprises an organic material;

coating the plurality of particles with the organic material;

separating substantially all of the remaining solvent from the coated powder, wherein the level of inter-particle forces between each particle is substantially decreased from the initial level;

fluidizing the coated powder;

flowing the coated powder into a plasma arc chamber;

the plasma arc chamber generating a plasma arc;

the generated plasma arc vaporizing the coated powder; and

in order to nano-size the powder to produce nanoparticles.

18. The method of claim 17 , wherein the organic material is a surfactant.

19. The method of claim 18 , wherein the surfactant is sorbitan monooleate.

20. The method of claim 19 , wherein the solvent further comprises a hydrocarbon.

21. The method of claim 20 , wherein the hydrocarbon is toluene.

22. The method of claim 20 , wherein the hydrocarbon is cyclohexane.

23. The method of claim 19 , wherein each particle in the plurality of particles is a non-oxide.

24. The method of claim 17 , wherein each particle in the plurality of particles is an oxide and the organic material is a material selected from the group consisting of trialkoxysilane, alkyltrialkoxysilane, trialkylalkoxysilane, trialkyldimethylaminosilane, trialkylchlorosilane, and octyltriethoxysilane.

25. The method of claim 17 , wherein separating substantially all of the remaining solvent from the coated powder comprises decanting substantially all of the solvent from the container.

26. The method of claim 25 , further comprising the step of drying the coated powder.

27. The method of claim 26 , wherein the step of drying comprises applying heat and vacuum pressure to the coated powder.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 16, 2018
From: SM (ASSIGNMENT FOR THE BENEFIT OF CREDITORS), LLC
To: UMICORE AG & CO. KG
Reel/Frame 045350/0280 →
CORRECTION OF REVEIVING PARTY NAME PREVIOUSLY RECORDED ON REEL 026058 FRAME 0792. Recorded May 18, 2011
From: LEAMON, DAVID
To: SDCMATERIALS, INC.
Reel/Frame 026296/0792 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 31, 2011
From: LEAMON, DAVID
To: SDCMATERIALS, INCC
Reel/Frame 026058/0792 →
Continuity (1)
Provisional Application 61284329 · Dec 15, 2009