IP Library Granted Patent US 8,849,584
Granted Patent B2
US 8,849,584 · App. 12/981,074 · Granted Sep 30, 2014

Systems and methods for particle size determination and control in a fluidized bed reactor for use with thermally decomposable silicon-containing gas

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Quick Facts
Patent No.
US 8,849,584
App. No.
12/981,074
Granted
Sep 30, 2014
Kind
B2
Abstract

Systems and methods are provided for determining the size of particles within a fluidized bed reactor for use with thermally decomposable silicon-containing gas. The pressure of gas adjacent a gas inlet and adjacent a gas outlet of the reactor are measured with pressure sensors. An algorithm is applied to at least one of the pressure measurements to determine the size of particles within the reactor. The determined size of the particles can be used to control the operation of the reactor.

Claims (34)

1. A method for determining a size of at least one of a plurality of polysilicon particles in a fluidized bed reactor for use with thermally decomposable silicon-containing gas, the fluidized bed reactor having a liner comprising a non-reactive material, the method comprising:

measuring a gas pressure in an inlet of the reactor with an inlet pressure sensor;

communicating the measured gas pressure in the inlet of the reactor to a processor;

determining, using the processor, the size of at least one of the plurality of polysilicon particles in the fluidized bed reactor based at least in part on an algorithm applied to the gas pressure in the inlet of the reactor measured by the inlet pressure sensor; and

controlling the operation of the fluidized bed reactor based at least in part on the determined size of at least one of the plurality of polysilicon particles in the fluidized bed reactor, wherein controlling operation of the fluidized bed reactor includes increasing the flow rate of gas within the fluidized bed reactor when the determined size of at least one of the plurality of polysilicon particles exceeds a threshold level.

2. A method for determining a size of at least one of a plurality of polysilicon particles in a fluidized bed reactor for use with thermally decomposable silicon-containing gas, the fluidized bed reactor having a liner comprising a non-reactive material, the method comprising:

measuring a gas pressure in an inlet of the reactor with an inlet pressure sensor;

communicating the measured gas pressure in the inlet of the reactor to a processor;

determining, using the processor, the size of at least one of the plurality of polysilicon particles in the fluidized bed reactor based at least in part on an algorithm applied to the gas pressure in the inlet of the reactor measured by the inlet pressure sensor; and

controlling the operation of the fluidized bed reactor based at least in part on the determined size of at least one of the plurality of polysilicon particles in the fluidized bed reactor, wherein controlling operation of the fluidized bed reactor includes decreasing the flow rate of gas within the fluidized bed reactor when the determined size of at least one of the plurality of polysilicon particles falls under a threshold level.

3. A method for determining a size of at least one of a plurality of polysilicon particles in a fluidized bed reactor for use with thermally decomposable silicon-containing gas, the fluidized bed reactor having a liner comprising a non-reactive material, the method comprising:

measuring a gas pressure in an inlet of the reactor with an inlet pressure sensor;

communicating the measured gas pressure in the inlet of the reactor to a processor;

determining, using the processor, the size of at least one of the plurality of polysilicon particles in the fluidized bed reactor based at least in part on an algorithm applied to the gas pressure in the inlet of the reactor measured by the inlet pressure sensor; and

determining, with the processor, the rate at which the gas is consumed based on the determined size of at least one of the polysilicon particles.

4. The method of claim 1 wherein determining, using the processor, the size of at least one of the plurality of polysilicon particles in the fluidized bed reactor includes determining a diameter of at least one of the plurality of polysilicon particles in the fluidized bed reactor.

5. The method of claim 1 further comprising measuring a gas pressure in an outlet of the reactor with an outlet pressure sensor.

6. The method of claim 5 wherein determining the size of at least one of the plurality of polysilicon particles in the fluidized bed reactor includes applying the algorithm to the gas pressure measured by the outlet pressure sensor.

7. The method of claim 6 wherein determining the size of at least one of the plurality of polysilicon particles in the fluidized bed reactor includes determining, using the processor, a diameter of at least one of the plurality of polysilicon particles in the fluidized bed reactor.

8. The method of claim 1 wherein controlling the operation of the fluidized bed reactor includes one of increasing rate of addition of particles to the fluidized bed reactor and increasing rate of removal of particles from the fluidized bed reactor.

9. The method of claim 1 wherein controlling the operation of the fluidized bed reactor includes one of decreasing rate of addition of particles to the fluidized bed reactor and decreasing rate of removal of particles from the fluidized bed reactor.

10. The method of claim 2 wherein determining the size of at least one of the plurality of polysilicon particles in the fluidized bed reactor includes determining a diameter of at least one of the plurality of polysilicon particles in the fluidized bed reactor.

11. The method of claim 2 further comprising measuring a gas pressure in an outlet of the reactor with an outlet pressure sensor.

12. The method of claim 11 wherein determining the size of at least one of the plurality of polysilicon particles in the fluidized bed reactor includes applying the algorithm to the gas pressure measured by the outlet pressure sensor.

13. The method of claim 12 wherein determining the size of at least one of the plurality of polysilicon particles in the fluidized bed reactor includes determining, using the processor, a diameter of at least one of the plurality of polysilicon particles in the fluidized bed reactor.

14. The method of claim 2 wherein controlling the operation of the fluidized bed reactor includes one of increasing rate of addition of particles to the fluidized bed reactor and increasing rate of removal of particles from the fluidized bed reactor.

15. The method of claim 2 wherein controlling the operation of the fluidized bed reactor includes one of decreasing the rate of addition of particles to the fluidized bed reactor and decreasing rate of removal of particles from the fluidized bed reactor.

16. The method of claim 3 wherein determining the size of at least one of the plurality of polysilicon particles in the fluidized bed reactor includes determining a diameter of at least one of the plurality of polysilicon particles in the fluidized bed reactor.

17. The method of claim 3 further comprising measuring a gas pressure in an outlet of the reactor with an outlet pressure sensor.

18. The method of claim 17 wherein determining the size of at least one of the plurality of polysilicon particles in the fluidized bed reactor includes applying the algorithm to the gas pressure measured by the outlet pressure sensor.

19. The method of claim 18 wherein determining the size of at least one of the plurality of polysilicon particles in the fluidized bed reactor includes determining, using the processor, a diameter of at least one of the plurality of polysilicon particles in the fluidized bed reactor.

20. The method of claim 3 further comprising controlling the operation of the fluidized bed reactor based at least in part on the determined size of at least one of the plurality of polysilicon particles in the fluidized bed reactor.

21. The method of claim 20 wherein controlling the operation of the fluidized bed reactor includes one of increasing rate of addition of particles to the fluidized bed reactor and increasing rate of removal of particles from the fluidized bed reactor.

22. The method of claim 20 wherein controlling the operation of the fluidized bed reactor includes one of decreasing rate of addition of particles to the fluidized bed reactor and decreasing rate of removal of particles from the fluidized bed reactor.

Assignments (12)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 27, 2017
From: SUNEDISON, INC.; SUNEDISON PRODUCTS SINGAPORE PTE. LTD.; MEMC PASADENA, INC.; SOLAICX
To: CORNER STAR LIMITED
Reel/Frame 042351/0659 →
PATENT SECURITY AGREEMENT Recorded Apr 28, 2016
From: SUNEDISON, INC.
To: DEUTSCHE BANK AG NEW YORK BRANCH, AS ADMINISTRATIVE AGENT
Reel/Frame 038557/0472 →
SECURITY INTEREST Recorded Jan 13, 2016
From: SUNEDISON, INC.; SUN EDISON LLC; SOLAICX; NVT, LLC
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, SOLELY IN ITS CAPACITY AS COLLATERAL TRUSTEE
Reel/Frame 037508/0606 →
RELEASE OF SECURITY INTEREST Recorded Jan 13, 2016
From: GOLDMAN SACHS BANK USA, AS ADMINISTRATIVE AGENT
To: SUNEDISON, INC.; SUN EDISON LLC; SOLAICX; NVT, LLC
Reel/Frame 037508/0884 →
SECURITY INTEREST Recorded Aug 11, 2015
From: SUNEDISON, INC.; SUN EDISON LLC; SOLAICX; NVT, LLC
To: GOLDMAN SACHS BANK USA, AS ADMINISTRATIVE AGENT
Reel/Frame 036329/0470 →
CHANGE OF NAME Recorded Aug 25, 2014
From: MEMC ELECTRONIC MATERIALS, INC.
To: SUNEDISON, INC
Reel/Frame 033605/0553 →
RELEASE OF SECURITY INTEREST Recorded Mar 3, 2014
From: DEUTSCHE BANK AG NEW YORK BRANCH
To: NVT, LLC; SUN EDISON LLC; SOLAICX; SUNEDISON, INC.
Reel/Frame 032382/0724 →
SECURITY AGREEMENT Recorded Feb 28, 2014
From: SUNEDISON, INC.; SUN EDISON LLC; SOLAICX; NVT, LLC; ENFLEX CORPORATION
To: WELLS FARGO BANK, NATIONAL ASSOCIATION, AS ADMINISTRATIVE AGENT
Reel/Frame 032372/0610 →
SECURITY AGREEMENT Recorded Jan 30, 2014
From: SUNEDISON, INC.; SOLAICX; SUN EDISON, LLC; NVT, LLC
To: DEUTSCHE BANK AG NEW YORK BRANCH
Reel/Frame 032177/0359 →
RELEASE OF SECURITY INTEREST Recorded Dec 26, 2013
From: GOLDMAN SACHS BANK USA
To: NVT, LLC; SUN EDISON LLC; SOLAICX; SUNEDISON, INC. (F/K/A MEMC ELECTRONIC MATERIALS, INC.)
Reel/Frame 031870/0092 →
SECURITY AGREEMENT Recorded Oct 1, 2012
From: NVT, LLC; SUN EDISON LLC; SOLAICX, INC.; MEMC ELECTRONIC MATERIALS, INC.
To: GOLDMAN SACHS BANK USA
Reel/Frame 029057/0810 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 17, 2011
From: BHUSARAPU, SATISH; NAWAZ, ARIF; GUPTA, PUNEET; BALAKRISHNAN, KARTHIK
To: MEMC ELECTRONIC MATERIALS, INC.
Reel/Frame 025822/0097 →