IP Library Granted Patent US 9,173,880
Granted Patent B2
US 9,173,880 · App. 12/986,223 · Granted Nov 3, 2015

Stabilized formulations containing anti-interleukin-6 receptor (IL-6R) antibodies

Inventors: Daniel B. Dix (LaGrangeville, NY); Kenneth S. Graham (Pleasant Valley, NY); Douglas Kamen (Poughquag, NY); Scott M. Walsh (Tarrytown, NY)
Assignee: Regeneron Pharmaceuticals, Inc.
A61K31/485A61K9/0019C07K16/248A61K47/183A61K47/26C07K2317/515
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 9,173,880
App. No.
12/986,223
Granted
Nov 3, 2015
Kind
B2
Abstract

The present invention provides pharmaceutical formulations comprising a human antibody that specifically binds to human interleukin-6 receptor (hIL-6R). The formulations may contain, in addition to an anti-hIL-6R antibody, at least one amino acid, at least one sugar, and/or at least one non-ionic surfactant. The pharmaceutical formulations of the present invention exhibit a substantial degree of antibody stability after storage for several months.

Claims (17)

1. A stable pharmaceutical formulation comprising: (i) 5 mg/mL to 200 mg/mL of a human antibody that specifically binds to human interleukin-6 receptor (hIL-6R), wherein the antibody comprises a heavy chain variable region having the amino acid sequence of SEQ ID NO:18 and a light chain variable region having the amino acid sequence of SEQ ID NO:26; (ii) histidine at a concentration of from 25 mM to 100 mM; (iii) arginine at a concentration of from 25 mM to 50 mM; (iv) sucrose in an amount of from 3% to 10% w/v; and (v) polysorbate 20 in an amount of from 0.1% to 0.2%, wherein the formulation has a pH of about 5.8, about 6.0, or about 6.2, and at least 90% of the native form of the antibody is recovered after 1 month of storage at 45° C., as determined by size exclusion chromatography.

2. The pharmaceutical formulation of claim 1 , comprising: (i) about 150 mg/mL of the antibody; (ii) about 25 mM histidine; (iii) about 5% sucrose; (iv) about 0.2% polysorbate 20; and (v) about 25 mM arginine.

3. The pharmaceutical formulation of claim 1 , comprising: (i) about 175 mg/mL of the antibody; (ii) about 25 mM histidine; (iii) about 5% sucrose; (iv) about 0.2% polysorbate 20; and (v) about 50 mM arginine.

4. The pharmaceutical formulation of claim 3 contained in a glass vial.

5. The pharmaceutical formulation of claim 3 contained in a syringe.

6. The pharmaceutical formulation of claim 3 contained in a microinfusor.

7. The pharmaceutical formulation of claim 5 , wherein said syringe comprises a fluorocarbon-coated plunger.

8. The pharmaceutical formulation of claim 5 , wherein said syringe is a low tungsten syringe.

9. The pharmaceutical formulation of claim 8 , wherein said syringe comprises a fluorocarbon-coated plunger.

10. The pharmaceutical formulation of claim 3 , wherein at least 90% of native form of said antibody is recovered after nine months of storage at 5° C., as determined by size exclusion-high performance liquid chromatography (SE-HPLC).

11. The pharmaceutical formulation of claim 10 , wherein at least 95% of native form of said antibody is recovered after nine months of storage at 5° C., as determined by size exclusion-high performance liquid chromatography (SE-HPLC).

12. The pharmaceutical formulation of claim 11 , wherein at least 96% of native form of said antibody is recovered after nine months of storage at 5° C., as determined by size exclusion-high performance liquid chromatography (SE-HPLC).

13. The pharmaceutical formulation of claim 3 , wherein the formulation exhibits a viscosity of less than about 15 cPoise.

14. The pharmaceutical formulation of claim 13 , wherein the formulation exhibits a viscosity of less than about 12 cPoise.

15. The pharmaceutical formulation of claim 14 , wherein the formulation exhibits a viscosity of less than about 9 cPoise.

16. A stable pharmaceutical formulation comprising: (i) about 175 mg/mL of a human antibody that specifically binds to human interleukin-6 receptor (hIL-6R), wherein said antibody comprises a heavy chain and light chain variable region (HCVR/LCVR) amino acid sequence pair of SEQ ID NOs:18/26; (ii) about 25 mM histidine; (iii) about 5% sucrose; (iv) about 0.2% polysorbate 20; and (v) about 50 mM arginine, wherein the formulation has a pH of about 6.0 and at least 90% of the native form of the antibody is recovered after 1 month of storage at 45° C., as determined by size exclusion chromatography.

17. A stable pharmaceutical formulation comprising: (i) 25 mg/mL to 200 mg/mL of a human antibody that specifically binds to human interleukin-6 receptor (hIL-6R), wherein the antibody comprises a heavy chain variable region having the amino acid sequence of SEQ ID NO:18 and a light chain variable region having the amino acid sequence of SEQ ID NO:26; (ii) about 25 mM histidine; (iii) about 25 mM or about 50 mM arginine; (iv) about 5% w/v sucrose; and (v) about 0.2% w/v polysorbate 20, wherein the formulation has a pH of about 6, and at least 90% of the native form of the antibody is recovered after 1 month of storage at 45° C., as determined by size exclusion chromatography.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 10, 2011
From: DIX, DANIEL B.; GRAHAM, KENNETH S.; KAMEN, DOUGLAS; WALSH, SCOTT M.
To: REGENERON PHARMACEUTICALS, INC.
Reel/Frame 025933/0422 →
Continuity (2)
Provisional Application 61293227 · Jan 8, 2010
Related Publication 20110171241A1 · Jul 14, 2011