IP Library Granted Patent US 8,716,318
Granted Patent B2
US 8,716,318 · App. 13/009,052 · Granted May 6, 2014

Pyridone sulfonamides and pyridone sulfamides as MEK inhibitors

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Quick Facts
Patent No.
US 8,716,318
App. No.
13/009,052
Granted
May 6, 2014
Kind
B2
Abstract

This invention concerns N-(ortho phenylamino dihydropyridyl)sulfonamides and N-(ortho phenylamino dihydropyridyl), N′-alkyl sulfamides which are inhibitors of MEK and are useful in the treatment of cancer and other hyperproliferative diseases.

Claims (31)

1. A compound of formula II or a pharmaceutically acceptable salt, or tautomer thereof:

wherein

B is H, C 1 -C 6 alkyl or C 2 -C 6 alkenyl;

wherein said C 1 -C 6 alkyl is optionally substituted with one or two groups selected independently from the group consisting of hydroxy, alkoxy, and oxy;

A and A′ are each independently H, C 1 -C 6 alkyl, or C 2 -C 6 alkenyl;

wherein each C 1 -C 6 alkyl is optionally substituted with one or two groups selected independently from the group consisting of hydroxy, alkoxy, and oxy; or

A and A′ together with the carbon atom to which they are attached, form a cyclopropyl, cyclobutyl, or cyclopentyl group,

wherein each cyclopropyl, cyclobutyl, or cyclopentyl group is optionally substituted with one or two groups selected independently from the group consisting of methyl, hydroxy, and halogen;

X and Y are each independently halogen, methyl, SCH 3 or trifluoromethyl;

R 1 is H, C 1 -C 6 alkyl, C 3 -C 6 cycloalkyl, C 2 -C 6 alkenyl, C 5 -C 6 cycloalkenyl or C 2 -C 6 alkynyl;

wherein each of said alkyl, cycloalkyl, alkenyl, cycloalkenyl and alkynyl groups are optionally substituted with 1-3 substituents selected independently from the group consisting of halogen, hydroxy, C 1 -C 4 alky, C 1 -C 4 alkoxy, cyano, cyanomethyl, nitro, azido, trifluoromethyl difluoromethoxy and phenyl;

R 2 is H, halogen, hydroxy, azido, cyano, cyanomethyl, C 1 -C 6 alkyl, C 3 -C 6 cycloalkyl, C 2 -C 6 alkenyl, C 5 -C 6 cycloalkenyl or C 2 -C 6 alkynyl, wherein each of said alkyl, cycloalkyl, alkenyl cycloalkenyl and alkynyl groups are optionally substituted with 1-3 substituents selected independently from the group consisting of halogen, hydroxy, C 1 -C 4 alkoxy, cyano, cyanomethyl, nitro, azido, trifluoromethyl and phenyl; and

D is H or C 1 -C 4 alkyl.

2. The compound of claim 1 , where D is H or methyl.

3. The compound of claim 1 , where D is ethyl, n-propyl, or isopropyl.

4. The compound of claim 1 , where C(A)(A′)B is methyl or ethyl and D is methyl or ethyl.

5. The compound of claim 1 , where A and A′ together with the carbon atom to which they are attached, form a cyclopropyl, cyclobutyl, or cyclopentyl group, wherein each cyclopropyl, cyclobutyl, or cyclopentyl group is optionally substituted with one or two groups selected independently from the group consisting of methyl, hydroxy, and halogen.

6. A compound which is

7. A pharmaceutical composition comprising a compound of claim 1 and a pharmaceutically acceptable carrier.

8. A pharmaceutical composition comprising a compound of claim 6 and a pharmaceutically acceptable carrier.

9. A pharmaceutically acceptable salt of a compound of claim 1 .

10. A compound of claim 1 , or a pharmaceutically acceptable salt or tautomer thereof.

11. A compound which is

or a pharmaceutically acceptable salt thereof.

12. A pharmaceutical composition comprising a compound of claim 11 and a pharmaceutically acceptable carrier.

13. A pharmaceutical composition comprising a compound of claim 2 and a pharmaceutically acceptable carrier.

14. A pharmaceutical composition comprising a compound of claim 3 and a pharmaceutically acceptable carrier.

15. A pharmaceutical composition comprising a compound of claim 4 and a pharmaceutically acceptable carrier.

16. A pharmaceutical composition comprising a compound of claim 5 and a pharmaceutically acceptable carrier.

17. A pharmaceutical composition comprising a compound of claim 9 and a pharmaceutically acceptable carrier.

18. A pharmaceutical composition comprising a compound of claim 10 and a pharmaceutically acceptable carrier.

Assignments (3)
RELEASE OF SECURITY INTEREST Recorded Apr 8, 2025
From: BARCLAYS BANK PLC, AS COLLATERAL AGENT
To: SOLTA MEDICAL, INC.; PRECISION DERMATOLOGY, INC.; BAUSCH HEALTH IRELAND LIMITED (F/K/A/ VALEANT PHARMACEUTICALS IRELAND LIMITED); SALIX PHARMACEUTICALS, INC.; SALIX PHARMACEUTICALS, LTD; SANTARUS, INC.; MEDICIS PHARMACEUTICAL CORPORATION; HUMAX PHARMACEUTICAL S.A.; SOLTA MEDICAL IRELAND LIMITED; BAUSCH & LOMB MEXICO, S.A. DE C.V.; BAUSCH+LOMB OPS B.V.; BAUSCH HEALTH AMERICAS, INC.; BAUSCH HEALTH COMPANIES INC.; BAUSCH HEALTH HOLDCO LIMITED; BAUSCH HEALTH MAGYARORSZAG KFT (A/K/A BAUSCH HEALTH HUNGARY LLC); BAUSCH HEALTH POLAND SPOLKA Z OGRANICZONA ODPOWIEDZIALNOSCIA (F/K/A VALEANT PHARMA POLAND SPOLKA Z OGRANICZONA ODPOWIEDZIALNOSCIA); BAUSCH HEALTH US, LLC; BAUSCH HEALTH, CANADA INC. / SANTE BAUSCH, CANADA INC.; ICN POLFA RZESZOW SPOLKA AKCYJNA (A/K/A ICN POLFA RZESZOW S.A.); ORAPHARMA, INC.; PRZEDSIEBIORSTWO FARMACEUTYCZNE JELFA SPOLKA AKCYJNA (A/K/A PRZEDSIEBIORSTWO FARMACEUTYCZNE JELFA S.A.); SOLTA MEDICAL DUTCH HOLDINGS B.V.; V-BAC HOLDING CORP.; VRX HOLDCO LLC; 1261229 B.C. LTD.; 1530065 B.C. LTD.
Reel/Frame 070778/0199 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNEE ADDRESS PREVIOUSLY RECORDED AT REEL: 026527 FRAME: 0843. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Sep 28, 2015
From: YAN, SHUNQI; VERNIER, JEAN MICHEL; HONG, ZHI; CHOW, SUETYING; KOH, YUNG-HYO
To: ARDEA BIOSCIENCES, INC.
Reel/Frame 036701/0652 →
NOTICE OF SUCCESSION OF AGENCY Recorded Jan 9, 2015
From: GOLDMAN SACHS LENDING PARTNERS, LLC
To: BARCLAYS BANK PLC, AS SUCCESSOR AGENT
Reel/Frame 034749/0689 →