IP Library Granted Patent US 8,431,061
Granted Patent B2
US 8,431,061 · App. 13/022,097 · Granted Apr 30, 2013

Method for manufacturing a ceramic composite article

View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 8,431,061
App. No.
13/022,097
Granted
Apr 30, 2013
Kind
B2
Abstract

A method for use in manufacturing a ceramic matrix composite article includes assembling a ceramic fiber sheet between a tool and a die, where the tool is conformable to the shape of the die and the melting point of the die is greater than the melting point of the tool. The assembly is then heated to soften the tool. At least one of the tool, the die or a separate inflatable member is then pressurized to conform the tool and the ceramic fiber sheet to the die. Next, the assembly is cooled and the pressure is vented before removal of the tool and ceramic fiber sheet from the die. A preceramic resin with a catalyst is then applied to the ceramic fiber sheet and cured at a curing temperature that is below the melting point of the tool, to form a preform. The tool is then removed from the preform.

Claims (30)

1. A method for use in manufacturing a ceramic matrix composite article, the method comprising:

assembling a ceramic fiber sheet between a tool and a die, where the tool is conformable to the shape of the die and the melting point of the die is greater than the melting point of the tool;

heating the assembly of the tool, the ceramic fiber sheet and the die to soften the tool;

pressurizing at least one of the tool, the die or a separate inflatable member to conform the tool and the ceramic fiber sheet to the die;

cooling the assembly of the tool, the ceramic fiber sheet and the die such that the tool hardens;

venting the pressure;

removing the tool and ceramic fiber sheet from the die;

applying a preceramic resin with a catalyst to the ceramic fiber sheet;

curing the preceramic resin with catalyst at a curing temperature that is below the melting point of the tool, to form a preform; and

removing the tool from the preform.

2. The method as recited in claim 1 , further comprising converting the preceramic resin to a ceramic matrix.

3. The method as recited in claim 1 , wherein the tool is formed of a thermoset polymer material.

4. The method as recited in claim 1 , wherein the tool is formed of a material that includes tin.

5. The method as recited in claim 1 , wherein the tool is formed of a thermoplastic material.

6. The method as recited in claim 1 , wherein the tool is formed of a polyolefin.

7. The method as recited in claim 1 , wherein the removing of the tool is by melting the tool.

8. The method as recited in claim 1 , wherein the removing of the tool is by chemical etching of the tool.

9. A method for use in manufacturing a ceramic matrix composite article, the method comprising:

softening a die member to a pliable state;

moving the softened die member against an opposed contoured die surface, with a fiber structure between the die member and the contoured die surface, to conform the die member and the fiber structure to the contoured die surface; and

hardening the die member to a rigid state such that the die member and the fiber structure maintain the contour of the contoured die surface.

10. The method as recited in claim 9 , wherein the softening of the die member includes heating the die member and the hardening of the die member includes cooling the die member.

11. The method as recited in claim 9 , wherein the moving of the softened die member against the opposed contoured die surface includes inflating an inflatable member against the softened die member.

12. The method as recited in claim 11 , wherein the fiber structure is a tubular fiber structure and the inflatable member is located within the tubular structure.

13. The method as recited in claim 9 , further comprising impregnating the fiber structure, while the fiber structure is maintained in the contour of the contoured die surface, with a resin material, and curing the resin material.

14. The method as recited in claim 13 , wherein the curing includes heating the die member, the fiber structure and the resin material to a curing temperature.

15. The method as recited in claim 14 , wherein the curing temperature is lower than the softening temperature of the die member.

16. The method as recited in claim 14 , wherein the resin material is a preceramic resin.

17. The method as recited in claim 16 , further comprising converting the preceramic resin to a ceramic matrix.

18. The method as recited in claim 13 , further comprising removing the die member from the fiber structure after the curing.

Assignments (7)
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENTS Recorded Jul 28, 2023
From: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT (AS SUCCESSOR AGENT TO WELLS FARGO BANK, NATIONAL ASSOCIATION (AS SUCCESSOR-IN-INTEREST TO WACHOVIA BANK, N.A.), AS ADMINISTRATIVE AGENT
To: AEROJET ROCKETDYNE OF DE, INC. (F/K/A PRATT & WHITNEY ROCKETDYNE, INC.)
Reel/Frame 064424/0050 →
RELEASE OF SECURITY INTEREST Recorded Aug 5, 2016
From: U.S. BANK NATIONAL ASSOCIATION
To: AEROJET ROCKETDYNE OF DE, INC. (F/K/A PRATT & WHITNEY ROCKETDYNE, INC.)
Reel/Frame 039597/0890 →
NOTICE OF SUCCESSION OF AGENCY (INTELLECTUAL PROPERTY) Recorded Jun 20, 2016
From: WELLS FARGO BANK, NATIONAL ASSOCIATION, AS THE RESIGNING AGENT
To: BANK OF AMERICA, N.A., AS THE SUCCESSOR AGENT
Reel/Frame 039079/0857 →
CHANGE OF NAME Recorded Jul 30, 2013
From: PRATT & WHITNEY ROCKETDYNE, INC.
To: AEROJET ROCKETDYNE OF DE, INC.
Reel/Frame 030902/0313 →
SECURITY AGREEMENT Recorded Jun 21, 2013
From: PRATT & WHITNEY ROCKETDYNE, INC.
To: U.S. BANK NATIONAL ASSOCIATION
Reel/Frame 030656/0615 →
SECURITY AGREEMENT Recorded Jun 17, 2013
From: PRATT & WHITNEY ROCKETDYNE, INC.
To: WELLS FARGO BANK, NATIONAL ASSOCIATION
Reel/Frame 030628/0408 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 18, 2011
From: STOUT, JEFFREY B.; FITZSIMMONS, MARK ANDREW; SCHEPEL, CHAD
To: PRATT & WHITNEY ROCKETDYNE, INC.
Reel/Frame 025981/0326 →