IP Library Granted Patent US 8,883,308
Granted Patent B2
US 8,883,308 · App. 13/038,789 · Granted Nov 11, 2014

High surface area fibrous silica nanoparticles

Inventors: Vivek Polshettiwar (Thuwal, SA); Jean-Marie Basset (Thuwal, SA)
Assignee: King Abdullah University of Science and Technology
C09C1/3054C01P2006/17Y02E60/50B01J23/28C01B33/18C01P2004/32B01J23/22B01J23/70H01M4/921B01J21/066C01P2006/37C01P2006/12B82Y40/00B01J35/006H01M4/925B01J35/023B01J23/38B01J35/06B01J23/10C01P2004/50B01J23/14B01J23/06B01J21/063C01B33/14C01P2004/61C01P2004/62B01J37/0201B01J23/02B82Y30/00C01P2004/10
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Quick Facts
Patent No.
US 8,883,308
App. No.
13/038,789
Granted
Nov 11, 2014
Kind
B2
Abstract

Disclosed are high surface area nanoparticles that have a fibrous morphology. The nanoparticles have a plurality of fibers, wherein each fiber is in contact with one other fiber and each fiber has a length of between about 1 nm and about 5000 nm. Also disclosed are applications of the nanoparticles of the present invention, and methods of fabrication of the nanoparticles of the present invention.

Claims (36)

1. A spherical nanoparticle comprising a plurality of silica fibers that are radially oriented in the nanoparticle and that are covalently linked with each other through siloxane linkages, wherein

the nanoparticle has a diameter of between about 1 nm and about 5000 nm.

2. The nanoparticle of claim 1 , wherein the nanoparticle is in the form of a dendrimer.

3. The nanoparticle of claim 1 , wherein each fiber has a length of between about 1 nm and about 2500 nm.

4. The nanoparticle of claim 1 , wherein each fiber has a thickness of between about 1 nm and about 25 nm.

5. The nanoparticle of claim 4 , wherein each fiber has a thickness of between about 1 nm to about 10 nm.

6. The nanoparticle of claim 5 , wherein each fiber has a length of between about 1 nm and about 2500 nm and a thickness of between about 1 nm and about 10 nm.

7. The nanoparticle of claim 1 , wherein the fibers are of varying thickness and varying lengths.

8. The nanoparticle of claim 1 , wherein the fibers are of a uniform thickness and a uniform length.

9. The nanoparticle of claim 1 , wherein the nanoparticle is comprised of about 10 3 fibers to 10 6 fibers.

10. The nanoparticle of claim 9 , wherein the nanoparticle is comprised of at least about 10 4 fibers.

11. The nanoparticle of claim 10 , wherein the nanoparticle is comprised of at least about 10 5 fibers.

12. The nanoparticle of claim 1 , wherein the nanoparticle is further defined as a nanosphere comprised of a plurality of fibers that are substantially radially oriented within the nanosphere.

13. The nanoparticle of claim 1 , further comprising one or more ligands attached to one or more fibers.

14. The nanoparticle of claim 13 , wherein a ligand is attached to the one or more fibers via a linker.

15. The nanoparticle of claim 14 , wherein the linker is an alkyl, a hydride, a carbene, a carbyne, a cyclopentadienyl, an alkoxide, an amido, or an imido group.

16. The nanoparticle of claim 13 , wherein the ligand is a catalyst, a drug, or an organic molecule.

17. The nanoparticle of claim 16 , wherein the ligand is a catalyst.

18. The nanoparticle of claim 17 , wherein the catalyst is a metal catalytic molecule.

19. The nanoparticle of claim 18 , wherein the metal catalytic molecule is a metal or a metal oxide.

20. The nanoparticle of claim 19 , wherein the metal catalytic molecule is a metal selected from the group consisting of Au, Pt, Pd, Ag, Ni, Ru, Rh, Ir, Os, Co, Fe and Cu.

21. The nanoparticle of claim 19 , wherein the metal catalytic molecule is a metal oxide selected from the group consisting of Al 2 O 3 , TiO 2 , Fe 2 O 3 , CeO 2 , CuO, ZnO, SiO 2 , V2O 5 , MgO, La2O 3 , ZrO 2 , SnO 2 , MnO 2 , MoO 3 , Mo 2 O 5 and zeolites.

22. The nanoparticle of claim 1 , wherein the nanoparticle has a maximum diameter of between about 100 nm and about 750 nm.

23. The nanoparticle of claim 22 , wherein the nanoparticle has a maximum diameter of between about 250 nm and about 500 nm.

24. The nanoparticle of claim 1 , wherein each fiber has a length of between about 1 nm and about 500 nm.

25. A composition comprising nanoparticles as set forth in claim 1 .

26. A composite comprising nanoparticles as set forth in claim 1 .

27. A catalyst composition comprising a nanoparticle as set forth in claim 17 .

28. A kit comprising nanoparticles as set forth in claim 1 in one or more sealed containers.

29. The kit of claim 28 , wherein the nanoparticles are comprised in a chromatography column.

30. A chromatography column comprising a stationary phase comprising nanoparticles as set forth in claim 1 .

31. A drug delivery device comprising nanoparticles as set forth in claim 1 .

32. A packaging material comprising nanoparticles as set forth in claim 1 .

33. The nanoparticle of claim 1 , wherein each fiber is in contact with at least one other fiber.

34. The nanoparticle of claim 1 , wherein each fiber has a length of between about 1 nm and about 5000 nm.

35. The nanoparticle of claim 1 , wherein each fiber has a thickness of between about 1 nm to about 50 nm.

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 19, 2011
From: POLSHETTIWAR, VIVEK; BASSET, JEAN-MARIE
To: KING ABDULLAH UNIVERSITY OF SCIENCE AND TECHNOLOGY
Reel/Frame 026149/0278 →
Continuity (3)
Continuation PCTIB2010002421 · Sep 7, 2010
Provisional Application 61309721 · Mar 2, 2010
Related Publication 20110253643A1 · Oct 20, 2011