IP Library Granted Patent US 8,895,313
Granted Patent B2
US 8,895,313 · App. 13/063,525 · Granted Nov 25, 2014

Ligands for aggregated tau molecules

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Quick Facts
Patent No.
US 8,895,313
App. No.
13/063,525
Granted
Nov 25, 2014
Kind
B2
Abstract

Provided are certain benzothiazole, imidazothiazole, imidazopyrimidine and imidazopyridine compounds, including, for example: formula (I) and pharmaceutically and physiologically acceptable salts, hydrates, and solvates thereof. Such compounds can be used as diagnostic ligands or labels of tau protein and PHF.

Claims (554)

1. A compound having the formula:

wherein

—R— is independently selected from:

wherein (T) indicates the point of attachment to -T;

and (Q) indicates the point of attachment to -Q-;

-Q- is independently selected from:

—N═N—;

—CH═CH—; —CR 1 ═CH—; —CH═CR 1 —; —CR 1 ═CR 1 —;

each —R 1 is independently unsubstituted saturated aliphatic C 1-4 -alkyl;

—P is independently selected from:

where the asterisk indicates the point of attachment;

-T is independently selected from:

where the asterisk indicates the point of attachment;

and X is independently CH;

—W 1 is independently —W A ;

—W 2 is independently —H or —W A ;

—W 3 is independently —H or —W A ;

—W 4 is independently —H or —W A ;

—W 5 is independently —H or —W A ;

—W 6 is independently —H or —W A ;

with the proviso that at least one of —W 4 , —W 5 and —W 6 is —W A ;

where —W A is independently selected from:

—F, —Cl, —Br, —I,

—OH, —W A1 , —O—W A1 ,

—NH 2 , —NHW A1 , and —N(W A1 ) 2 ;

and —W A1 is independently selected from:

unsubstituted saturated aliphatic C 1-4 -alkyl,

—CF 3 ,

—CH 2 CH 2 OH, and

—CH 2 CH 2 N(Me) 2 ;

-G 1 is independently —H or -G A ;

-G 2 is independently —H or -G A ;

where -G A is independently selected from:

—F, —Cl, —Br, —I,

—CF 3 , —OCF 3 ,

—OH, —OR 2 ;

—[O—CH 2 CH 2 ] n —R B2 , where n is 2 to 6;

-G 3 is independently —H or -G B ;

-G 4 is independently —H or -G B

where -G B is independently selected from:

—F, —Cl, —Br, —I,

—CF 3 , —OCF 3 ,

—OH, —OR 2 ;

—[O—CH 2 CH 2 ] n —R B2 , where n is 2 to 6;

wherein:

—P 1 is independently —H or —P A ;

—P 2 is independently —H or —P B ;

—P 3 is independently —H or —P C ;

—P 4 is independently —H or —P B ;

—P 5 is independently —H or —P A ;

and wherein:

each —P A , each —P B , and each —P C is independently:

—F, —Cl, —Br, —I,

—R 2 ,

—CF 3 , —OCF 3 ,

—OH, -L 1 -OH,

—OR 2 , -L 1 -OR 2 , —O-L 1 -OR 2 ,

—SH, —SR 2 ,

—CN,

—NO 2 ,

—NH 2 , —NHR 2 , —NR 2 2 , —NR 3 R 4 ,

—NHOH,

-L 1 -NH 2 , -L 1 -NHR 2 , -L 1 -NR 2 2 , -L 1 -NR 3 R 4 ,

—O-L 1 -NH 2 , —O-L 1 -NHR 2 , —O-L 1 -NR 2 2 , —O-L 1 -NR 3 R 4 ,

—C(═O)OH, —C(═O)OR 2 ,

—OC(═O)R 2 ,

—C(═O)NH 2 , —C(═O)NHR 2 , —C(═O)NR 2 2 , —C(═O)NR 3 R 4 ,

—NHC(═O)R 2 , —NR 2 C(═O)R 2 ,

—C(═O)NHOR 2 , —C(═O)NR 2 OR 2 ,

—NHC(═O)OR 2 , —NR 2 C(═O)OR 2 ,

—OC(═O)NH 2 , —OC(═O)NHR 2 , —OC(═O)NR 2 2 , —OC(═O)NR 3 R 4 ,

—C(═O)R 2 ,

—NHC(═O)NH 2 , —NHC(═O)NHR 2 ,

—NHC(═O)NR 2 2 , —NHC(═O)NR 3 R 4 ,

—NR 2 C(═O)NH 2 , —NR 2 C(═O)NHR 2 ,

—NR 2 C(═O)NR 2 2 , —NR 2 C(═O)NR 3 R 4 ,

—NHS(═O) 2 R 2 , —NR 2 S(═O) 2 R 2 ,

—S(═O) 2 NH 2 , —S(═O) 2 NHR 2 , —S(═O) 2 NR 2 2 , —S(═O) 2 NR 3 R 4 ,

—S(═O)R 2 , —S(═O) 2 R 2 , —OS(═O) 2 R 2 , or —S(═O) 2 OR 2

wherein:

each -L 1 - is independently saturated aliphatic C 1-5 alkylene;

in each group —NR 3 R 4 , —R 3 and —R 4 , taken together with the nitrogen atom to which they are attached, form a 4-, 5-, 6-, or 7-membered non-aromatic ring having exactly 1 ring heteroatom or exactly 2 ring heteroatoms, wherein one of said exactly 2 ring heteroatoms is N, and the other of said exactly 2 ring heteroatoms is independently N, O, or S;

each —R 2 is independently:

—R A1 , —R A2 , —R A3 , —R A4 , —R A5 , —R A6 , —R A7 , —R A8 ,

L A -R A4 , -L A -R A5 , -L A -R A6 , -L A -R A7 , or -L A -R A8 ;

wherein:

each —R A1 is independently saturated aliphatic C 1-6 alkyl;

each —R A2 is independently aliphatic C 2-6 alkenyl;

each —R A3 is independently aliphatic C 2-6 alkynyl;

each —R A4 is independently saturated C 3-6 cycloalkyl;

each —R A5 is independently C 3-6 cycloalkenyl;

each —R A6 is independently non-aromatic C 3-7 heterocyclyl;

each —R A7 is independently C 6-10 -carboaryl;

each —R A8 is independently C 5-10 heteroaryl;

each -L A - is independently saturated aliphatic C 1-3 alkylene;

and wherein:

each —R A4 , —R A5 , —R A6 , —R A7 , and —R A8 is optionally substituted, for example, with one or more substituents —R B1 and/or one or more substituents —R B2 , and

each —R A1 , —R A2 , —R A3 , and -L A - is optionally substituted, for example, with one or more substituents —R B2 ,

wherein:

each —R B1 is independently saturated aliphatic C 1-4 -alkyl, phenyl, or benzyl;

each —R B2 is independently:

—F, —Cl, —Br, —I,

—CF 3 , —OCF 3 ,

—OH, -L C -OH, —O-L C -OH,

—OR C1 , -L C -OR C1 , —O-L C -OR C1 ,

—SH, —SR C1 ,

—CN,

—NO 2 ,

—NH 2 , —NHR C1 , —NR C1 2 , —NR C2 R C3 ,

-L C -NH 2 , -L C -NHR C1 , -L C -NR C1 2 , or -L C -NR C2 R C3 ,

—O-L C -NH 2 , —O-L C -NHR C1 , —O-L C -NR C1 2 , —O-L C -NR C2 R C3 ,

—C(═O)OH, —C(═O)OR C1 ,

—OC(═O)R C1 ,

—C(═O)R C1 ,

—C(═O)NH 2 , —C(═O)NHR C1 , —C(═O)NR C1 2 , —C(═O)NR C2 R C3 ,

—NHC(═O)R C1 , —NR C1 C(═O)R C1 ,

—NHS(═O) 2 R C1 , —NR C1 S(═O) 2 R C1 ,

—S(═O) 2 NH 2 , —S(═O) 2 NHR C1 , —S(═O) 2 NR C1 2 , —S(═O) 2 NR C2 R C3 , or

—S(═O) 2 R C1 ;

wherein:

each —R C1 is independently unsubstituted saturated aliphatic C 1-4 -alkyl, phenyl, or benzyl;

each -L C - is independently unsubstituted saturated aliphatic C 1-5 alkylene; and

in each group —NR C2 R C3 , —R C2 and —R C3 , taken together with the nitrogen atom to which they are attached, form a 4-, 5-, 6-, or 7-membered non-aromatic ring having exactly 1 ring heteroatom or exactly 2 ring heteroatoms, wherein one of said exactly 2 ring heteroatoms is N, and the other of said exactly 2 ring heteroatoms is independently N, O, or S,

and pharmaceutically and physiologically acceptable salts thereof,

with the proviso that the compound is not a compound:

(a) P-002 through P-015; and

(b) where -T is:

—R— is:

and —P is:

and —W 4 is —H, -Q- is —CH═CH—, -G 1 , -G 2 , -G 3 , and -G 4 are all —H, and

(i) —P 1 , —P 2 , —P 4 and —P 5 are all —H, and —P 3 is —R A1 ; or

(ii) one of —P 1 , —P 2 , —P 3 , P 4 and —P 5 is —R A7 , and the others of —P 1 , —P 2 , —P 3 , P 4 and —P 5 are —H.

2. A compound of formula:

wherein

—R— is independently selected from:

wherein (T) indicates the point of attachment to -T;

and (Q) indicates the point of attachment to -Q-;

-Q- is independently selected from:

—NHC(O)—; —NR 1 C(O)—;

each —R 1 is independently unsubstituted saturated aliphatic C 1-4 -alkyl;

—P is independently selected from:

where the asterisk indicates the point of attachment;

-T is independently selected from:

where the asterisk indicates the point of attachment;

and X is independently CH;

—W 1 is independently —W A ;

—W 2 is independently —H or —W A ;

—W 3 is independently —H or —W A ;

where —W A is independently selected from:

—F, —Cl, —Br, —I,

—OH, —W A1 , —O—W A1 ,

—NH 2 , —NHW A1 , and —N(W A1 ) 2 ;

and —W A1 is independently selected from:

unsubstituted saturated aliphatic C 1-4 -alkyl,

—CF 3 ,

—CH 2 CH 2 OH, and

—CH 2 CH 2 N(Me) 2 ;

-G 1 is independently —H or -G A ;

-G 2 is independently —H or -G A ;

where -G A is independently selected from:

—F, —Cl, —Br, —I,

—CF 3 , —OCF 3 ,

—OH, —OR 2 ;

—[O—CH 2 CH 2 ] n —R B2 , where n is 2 to 6;

-G 3 is independently —H or -G B ;

-G 4 is independently —H or -G B

where -G B is independently selected from:

—F, —Cl, —Br, —I,

—CF 3 , —OCF 3 ,

—OH, —OR 2 ;

—[O—CH 2 CH 2 ] n —R B2 , where n is 2 to 6;

wherein:

—P 1 is independently —H or —P A ;

—P 2 is independently —H or —P B ;

—P 3 is independently —H or —P C ;

—P 4 is independently —H or —P B ;

—P 5 is independently —H or —P A ;

and wherein:

each —P A , each —P B , and each —P C is independently:

—F, —Cl, —Br, —I,

—R 2 ,

—CF 3 , —OCF 3 ,

—OH, -L 1 -OH,

—OR 2 , -L 1 -OR 2 , —O-L 1 -OR 2 ,

—SH, —SR 2 ,

—CN,

—NO 2 ,

—NH 2 , —NHR 2 , —NR 2 2 , —NR 3 R 4 ,

—NHOH,

-L 1 -NH 2 , -L 1 -NHR 2 , -L 1 -NR 2 2 , -L 1 -NR 3 R 4 ,

—O-L 1 -NH 2 , —O-L 1 -NHR 2 , —O-L 1 -NR 2 2 , —O-L 1 -NR 3 R 4 ,

—C(═O)OH, —C(═O)OR 2 ,

—OC(═O)R 2 ,

—C(═O)NH 2 , —C(═O)NHR 2 , —C(═O)NR 2 2 , —C(═O)NR 3 R 4 ,

—NHC(═O)R 2 , —NR 2 C(═O)R 2 ,

—C(═O)NHOR 2 , —C(═O)NR 2 OR 2 ,

—NHC(═O)OR 2 , —NR 2 C(═O)OR 2 ,

—OC(═O)NH 2 , —OC(═O)NHR 2 , —OC(═O)NR 2 2 , —OC(═O)NR 3 R 4 ,

—C(═O)R 2 ,

—NHC(═O)NH 2 , —NHC(═O)NHR 2 ,

—NHC(═O)NR 2 2 , —NHC(═O)NR 3 R 4 ,

—NR 2 C(═O)NH 2 , —NR 2 C(═O)NHR 2 ,

—NR 2 C(═O)NR 2 2 , —NR 2 C(═O)NR 3 R 4 ,

—NHS(═O) 2 R 2 , —NR 2 S(═O) 2 R 2 ,

—S(═O) 2 NH 2 , —S(═O) 2 NHR 2 , —S(═O) 2 NR 2 2 , —S(═O) 2 NR 3 R 4 ,

—S(═O)R 2 , —S(═O) 2 R 2 , —OS(═O) 2 R 2 , or —S(═O) 2 OR 2

wherein:

each -L 1 - is independently saturated aliphatic C 1-5 alkylene;

in each group —NR 3 R 4 , —R 3 and —R 4 , taken together with the nitrogen atom to which they are attached, form a 4-, 5-, 6-, or 7-membered non-aromatic ring having exactly 1 ring heteroatom or exactly 2 ring heteroatoms, wherein one of said exactly 2 ring heteroatoms is N, and the other of said exactly 2 ring heteroatoms is independently N, O, or S;

each —R 2 is independently:

—R A1 , —R A2 , —R A3 , —R A4 , —R A5 , —R A6 , —R A7 , —R A8 ,

-L A -R A4 , -L A -R A5 -L A -R A6 , L A -R A7 , or -L A -R A8 ;

wherein:

each —R A1 is independently saturated aliphatic C 1-6 alkyl;

each —R A2 is independently aliphatic C 2-6 alkenyl;

each —R A3 is independently aliphatic C 2-6 alkynyl;

each —R A4 is independently saturated C 3-6 cycloalkyl;

each —R A5 is independently C 3-6 cycloalkenyl;

each —R A6 is independently non-aromatic C 3-7 heterocyclyl;

each —R A7 is independently C 6-10 -carboaryl;

each —R A8 is independently C 5-10 heteroaryl;

each -L A - is independently saturated aliphatic C 1-3 alkylene;

and wherein:

each —R A4 , —R A5 , —R A6 , —R A7 , and —R A8 is optionally substituted, for example, with one or more substituents —R B1 and/or one or more substituents —R B2 , and

each —R A1 , —R A2 , —R A3 , and -L A - is optionally substituted, for example, with one or more substituents —R B2 ,

wherein:

each —R B1 is independently saturated aliphatic C 1-4 -alkyl, phenyl, or benzyl;

each —R B2 is independently:

—F, —Cl, —Br, —I,

—CF 3 , —OCF 3 ,

—OH, -L C -OH, —O-L C -OH,

—OR C1 , -L C -OR C1 , —O-L C -OR C1 ,

—SH, —SR C1 ,

—CN,

—NO 2 ,

—NH 2 , —NHR C1 , —NR C1 2 , —NR C2 R C3 ,

-L C -NH 2 , -L C -NHR C1 , -L C -NR C1 2 , or -L C -NR C2 R C3 ,

—O-L C -NH 2 , —O-L C -NHR C1 , —O-L C -NR C1 2 , —O-L C -NR C2 R C3 ,

—C(═O)OH, —C(═O)OR C1 ,

—OC(═O)R C1 ,

—C(═O)R C1 ,

—C(═O)NH 2 , —C(═O)NHR C1 , —C(═O)NR C1 2 , —C(═O)NR C2 R C3 ,

—NHC(═O)R C1 , —NR C1 C(═O)R C1 ,

—NHS(═O) 2 R C1 , —NR C1 S(═O) 2 R C1 ,

—S(═O) 2 NH 2 , —S(═O) 2 NHR C1 , —S(═O) 2 NR C1 2 , —S(═O) 2 NR C2 R C3 , or

—S(═O) 2 R C1 ;

wherein:

each —R C1 is independently unsubstituted saturated aliphatic C 1-4 -alkyl, phenyl, or benzyl;

each -L C - is independently unsubstituted saturated aliphatic C 1-5 alkylene; and

in each group —NR C2 R C3 , —R C2 and —R C3 , taken together with the nitrogen atom to which they are attached, form a 4-, 5-, 6-, or 7-membered non-aromatic ring having exactly 1 ring heteroatom or exactly 2 ring heteroatoms, wherein one of said exactly 2 ring heteroatoms is N, and the other of said exactly 2 ring heteroatoms is independently N, O, or S,

and pharmaceutically and physiologically acceptable salts thereof.

3. A compound of formula:

wherein

—R— is independently selected from:

wherein (T) indicates the point of attachment to -T;

and (Q) indicates the point of attachment to -Q-;

-Q- is independently selected from:

—NHC(O)—; —NR 1 C(O)—;

each —R 1 is independently unsubstituted saturated aliphatic C 1-4 -alkyl;

—P is independently selected from:

where the asterisk indicates the point of attachment;

-T is independently selected from:

where the asterisk indicates the point of attachment;

—W 4 is independently —H or —W A ;

—W 5 is independently —H or —W A ;

—W 6 is independently —H or —W A ;

with the proviso that at least one of —W 4 , —W 5 and —W 6 is —W A ;

where —W A is independently selected from:

—F, —Cl, —Br, —I,

—OH, —W A1 , —O—W A1 ,

—NH 2 , —NHW A1 , and —N(W A1 ) 2 ;

and —W A1 is independently selected from:

unsubstituted saturated aliphatic C 1-4 -alkyl,

—CF 3 ,

—CH 2 CH 2 OH, and

—CH 2 CH 2 N(Me) 2 ;

-G 1 is independently —H or -G A ;

-G 2 is independently —H or -G A ;

where -G A is independently selected from:

—F, —Cl, —Br, —I,

—CF 3 , —OCF 3 ,

—OH, —OR 2 ;

—[O—CH 2 CH 2 ] n —R B2 , where n is 2 to 6;

-G 3 is independently —H or -G B ;

-G 4 is independently —H or -G B

where -G B is independently selected from:

—F, —Cl, —Br, —I,

—CF 3 , —OCF 3 ,

—OH, —OR 2 ;

—[O—CH 2 CH 2 ] n —R B2 , where n is 2 to 6;

wherein:

—P 1 is independently —H or —P A ;

—P 2 is independently —H or —P B ;

—P 3 is independently —H or —P C ;

—P 4 is independently —H or —P B ;

—P 5 is independently —H or —P A ;

and wherein:

each —P A , each —P B , and each —P C is independently:

—F, —Cl, —Br, —I,

—R 2 ,

—CF 3 , —OCF 3 ,

—OH, -L 1 -OH,

—OR 2 , -L 1 -OR 2 , —O-L 1 -OR 2 ,

—SH, —SR 2 ,

—CN,

—NO 2 ,

—NH 2 , —NHR 2 , —NR 2 2 , —NR 3 R 4 ,

—NHOH,

-L 1 -NH 2 , -L 1 -NHR 2 , -L 1 -NR 2 2 , -L 1 -NR 3 R 4 ,

—O-L 1 -NH 2 , —O-L 1 -NHR 2 , —O-L 1 -NR 2 2 , —O-L 1 -NR 3 R 4 ,

—C(═O)OH, —C(═O)OR 2 ,

—OC(═O)R 2 ,

—C(═O)NH 2 , —C(═O)NHR 2 , —C(═O)NR 2 2 , —C(═O)NR 3 R 4 ,

—NHC(═O)R 2 , —NR 2 C(═O)R 2 ,

—C(═O)NHOR 2 , —C(═O)NR 2 OR 2 ,

—NHC(═O)OR 2 , —NR 2 C(═O)OR 2 ,

—OC(═O)NH 2 , —OC(═O)NHR 2 , —OC(═O)NR 2 2 , —OC(═O)NR 3 R 4 ,

—C(═O)R 2 ,

—NHC(═O)NH 2 , —NHC(═O)NHR 2 ,

—NHC(═O)NR 2 2 , —NHC(═O)NR 3 R 4 ,

—NR 2 C(═O)NH 2 , —NR 2 C(═O)NHR 2 ,

—NR 2 C(═O)NR 2 2 , —NR 2 C(═O)NR 3 R 4 ,

—NHS(═O) 2 R 2 , —NR 2 S(═O) 2 R 2 ,

—S(═O) 2 NH 2 , —S(═O) 2 NHR 2 , —S(═O) 2 NR 2 2 , —S(═O) 2 NR 3 R 4 ,

—S(═O)R 2 , —S(═O) 2 R 2 , —OS(═O) 2 R 2 , or —S(═O) 2 OR 2

wherein:

each -L 1 - is independently saturated aliphatic C 1-5 alkylene;

in each group —NR 3 R 4 , —R 3 and —R 4 , taken together with the nitrogen atom to which they are attached, form a 4-, 5-, 6-, or 7-membered non-aromatic ring having exactly 1 ring heteroatom or exactly 2 ring heteroatoms, wherein one of said exactly 2 ring heteroatoms is N, and the other of said exactly 2 ring heteroatoms is independently N, O, or S;

each —R 2 is independently:

—R A1 , —R A2 , —R A3 , —R A4 , —R A5 , —R A6 , —R A7 , —R A8 ,

-L A -R A4 , -L A -R A5 , -L A -R A6 , -L A -R A7 , or -L A -R A8 ;

wherein:

each —R A1 is independently saturated aliphatic C 1-6 alkyl;

each —R A2 is independently aliphatic C 2-6 alkenyl;

each —R A3 is independently aliphatic C 2-6 alkynyl;

each —R A4 is independently saturated C 3-6 cycloalkyl;

each —R A5 is independently C 3-6 cycloalkenyl;

each —R A6 is independently non-aromatic C 3-7 heterocyclyl;

each —R A7 is independently C 6-10 -carboaryl;

each —R A8 is independently C 5-10 heteroaryl;

each -L A - is independently saturated aliphatic C 1-3 alkylene;

and wherein:

each —R A4 , —R A5 , —R A6 , —R A7 , and —R A8 is optionally substituted, for example, with one or more substituents —R B1 and/or one or more substituents —R B2 , and

each —R A1 , —R A2 , —R A3 , and -L A - is optionally substituted, for example, with one or more substituents —R B2 ,

wherein:

each —R B1 is independently saturated aliphatic C 1-4 -alkyl, phenyl, or benzyl;

each —R B2 is independently:

—F, —Cl, —Br, —I,

—CF 3 , —OCF 3 ,

—OH, -L C -OH, —O-L C -OH,

—OR C1 , -L C -OR C1 , —O-L C -OR C1 ,

—SH, —SR C1 ,

—CN,

—NO 2 ,

—NH 2 , —NHR C1 , —NR C1 2 , —NR C2 R C3 ,

-L C -NH 2 , -L C -NHR C1 , -L C -NR C1 2 , or -L C -NR C2 R C3 ,

—O-L C -NH 2 , —O-L C -NHR C1 , —O-L C -NR C1 2 , —O-L C -NR C2 R C3 ,

—C(═O)OH, —C(═O)OR C1 ,

—OC(═O)R C1 ,

—C(═O)R C1 ,

—C(═O)NH 2 , —C(═O)NHR C1 , —C(═O)NR C1 2 , —C(═O)NR C2 R C3 ,

—NHC(═O)R C1 , —NR C1 C(═O)R C1 ,

—NHS(═O) 2 R C1 , —NR C1 S(═O) 2 R C1 ,

—S(═O) 2 NH 2 , —S(═O) 2 NHR C1 , —S(═O) 2 NR C1 2 , —S(═O) 2 NR C2 R C3 , or

—S(═O) 2 R C1 ;

wherein:

each —R C1 is independently unsubstituted saturated aliphatic C 1-4 -alkyl, phenyl, or benzyl;

each -L C - is independently unsubstituted saturated aliphatic C 1-5 alkylene; and

in each group —NR C2 R C3 , —R C2 and —R C3 , taken together with the nitrogen atom to which they are attached, form a 4-, 5-, 6-, or 7-membered non-aromatic ring having exactly 1 ring heteroatom or exactly 2 ring heteroatoms, wherein one of said exactly 2 ring heteroatoms is N, and the other of said exactly 2 ring heteroatoms is independently N, O, or S;

wherein the compound contains a —F group;

and pharmaceutically and physiologically acceptable salts thereof;

with the proviso that the compound is not compound P-001.

4. A compound of formula:

wherein

—R— is independently selected from:

wherein (T) indicates the point of attachment to -T;

and (Q) indicates the point of attachment to -Q-;

-Q- is independently selected from:

—NHC(O)—; —NR 1 C(O)—;

—N═N—;

—CH═CH—; —CR 1 ═CH—; —CH═CR 1 —; —CR 1 ═CR 1 —;

each —R 1 is independently unsubstituted saturated aliphatic C 1-4 -alkyl;

—P is independently selected from:

where the asterisk indicates the point of attachment;

-T is independently selected from:

where the asterisk indicates the point of attachment;

and X is independently N;

—W 1 is independently H or —W A ;

where —W A is independently selected from:

—F, —Cl, —Br, —I,

—OH, —W A1 , —O—W A1 ,

—NH 2 , —NHW A1 , and —N(W A1 ) 2 ;

and —W A1 is independently selected from:

unsubstituted saturated aliphatic C 1-4 -alkyl,

—CF 3 ,

—CH 2 CH 2 OH, and

—CH 2 CH 2 N(Me) 2 ;

-G 1 is independently —H or -G A ;

-G 2 is independently —H or -G A ;

where -G A is independently selected from:

—F, —Cl, —Br, —I,

—CF 3 , —OCF 3 ,

—OH, —OR 2 ;

—[O—CH 2 CH 2 ] n —R B2 , where n is 2 to 6;

-G 3 is independently —H or -G B ;

-G 4 is independently —H or -G B

where -G B is independently selected from:

—F, —Cl, —Br, —I,

—CF 3 , —OCF 3 ,

—OH, —OR 2 ;

—[O—CH 2 CH 2 ] n —R B2 , where n is 2 to 6;

wherein:

—P 1 is independently —H or —P A ;

—P 2 is independently —H or —P B ;

—P 3 is independently —H or —P C ;

—P 4 is independently —H or —P B ;

—P 5 is independently —H or —P A ;

and wherein:

each —P A , each —P B , and each —P C is independently:

—F, —Cl, —Br, —I,

—R 2 ,

—CF 3 , —OCF 3 ,

—OH, -L 1 -OH,

—OR 2 , -L 1 -OR 2 , —O-L 1 -OR 2 ,

—SH, —SR 2 ,

—CN,

—NO 2 ,

—NH 2 , —NHR 2 , —NR 2 2 , —NR 3 R 4 ,

—NHOH,

-L 1 -NH 2 , -L 1 -NHR 2 , -L 1 -NR 2 2 , -L 1 -NR 3 R 4 ,

—O-L 1 -NH 2 , —O-L 1 -NHR 2 , —O-L 1 -NR 2 2 , —O-L 1 -NR 3 R 4 ,

—C(═O)OH, —C(═O)OR 2 ,

—OC(═O)R 2 ,

—C(═O)NH 2 , —C(═O)NHR 2 , —C(═O)NR 2 2 , —C(═O)NR 3 R 4 ,

—NHC(═O)R 2 , —NR 2 C(═O)R 2 ,

—C(═O)NHOR 2 , —C(═O)NR 2 OR 2 ,

—NHC(═O)OR 2 , —NR 2 C(═O)OR 2 ,

—OC(═O)NH 2 , —OC(═O)NHR 2 , —OC(═O)NR 2 2 , —OC(═O)NR 3 R 4 ,

—C(═O)R 2 ,

—NHC(═O)NH 2 , —NHC(═O)NHR 2 ,

—NHC(═O)NR 2 2 , —NHC(═O)NR 3 R 4 ,

—NR 2 C(═O)NH 2 , —NR 2 C(═O)NHR 2 ,

—NR 2 C(═O)NR 2 2 , —NR 2 C(═O)NR 3 R 4 ,

—NHS(═O) 2 R 2 , —NR 2 S(═O) 2 R 2 ,

—S(═O) 2 NH 2 , —S(═O) 2 NHR 2 , —S(═O) 2 NR 2 2 , —S(═O) 2 NR 3 R 4 ,

—S(═O)R 2 , —S(═O) 2 R 2 , —OS(═O) 2 R 2 , or —S(═O) 2 OR 2

wherein:

each -L 1 - is independently saturated aliphatic C 1-5 alkylene;

in each group —NR 3 R 4 , —R 3 and —R 4 , taken together with the nitrogen atom to which they are attached, form a 4-, 5-, 6-, or 7-membered non-aromatic ring having exactly 1 ring heteroatom or exactly 2 ring heteroatoms, wherein one of said exactly 2 ring heteroatoms is N, and the other of said exactly 2 ring heteroatoms is independently N, O, or S;

each —R 2 is independently:

—R A1 , —R A2 , —R A3 , —R A4 , —R A5 , —R A6 , —R A7 , —R A8 ,

-L A -R A4 , -L A -R A5 , -L A -R A6 , -L A -R A7 , or -L A -R A8 ;

wherein:

each —R A1 is independently saturated aliphatic C 1-6 alkyl;

each —R A2 is independently aliphatic C 2-6 alkenyl;

each —R A3 is independently aliphatic C 2-6 alkynyl;

each —R A4 is independently saturated C 3-6 cycloalkyl;

each —R A5 is independently C 3-6 cycloalkenyl;

each —R A6 is independently non-aromatic C 3-7 heterocyclyl;

each —R A7 is independently C 6-10 -carboaryl;

each —R A8 is independently C 5-10 heteroaryl;

each -L A - is independently saturated aliphatic C 1-3 alkylene;

and wherein:

each —R A4 , —R A5 , —R A6 , —R A7 , and R A8 is optionally substituted, for example, with one or more substituents —R B1 and/or one or more substituents —R B2 , and

each —R A1 , —R A2 , —R A3 , and -L A - is optionally substituted, for example, with one or more substituents —R B2 ,

wherein:

each —R B1 is independently saturated aliphatic C 1-4 -alkyl, phenyl, or benzyl;

each —R B2 is independently:

—F, —Cl, —Br, —I,

—CF 3 , —OCF 3 ,

—OH, -L C -OH, —O-L C -OH,

—OR C1 , -L C -OR C1 , —O-L C -OR C1 ,

—SH, —SR C1 ,

—CN,

—NO 2 ,

—NH 2 , —NHR C1 , —NR C1 2 , —NR C2 R C3 ,

-L C -NH 2 , -L C -NHR C1 , -L C -NR C1 2 , or -L C -NR C2 R C3 ,

—O-L C -NH 2 , —O-L C -NHR C1 , —O-L C -NR C1 2 , —O-L C -NR C2 R C3 ,

—C(═O)OH, —C(═O)OR C1 ,

—OC(═O)R C1 ,

—C(═O)R C1 ,

—C(═O)NH 2 , —C(═O)NHR C1 , —C(═O)NR C1 2 , —C(═O)NR C2 R C3 ,

—NHC(═O)R C1 , —NR C1 C(═O)R C1 ,

—NHS(═O) 2 R C1 , —NR C1 S(═O) 2 R C1 ,

—S(═O) 2 NH 2 , —S(═O) 2 NHR C1 , —S(═O) 2 NR C1 2 , —S(═O) 2 NR C2 R C3 , or

—S(═O) 2 R C1 ;

wherein:

each —R C1 is independently unsubstituted saturated aliphatic C 1-4 -alkyl, phenyl, or benzyl; and

each -L C - is independently unsubstituted saturated aliphatic C 1-5 alkylene; and

in each group —NR C2 R C3 , —R C2 and —R C3 , taken together with the nitrogen atom to which they are attached, form a 4-, 5-, 6-, or 7-membered non-aromatic ring having exactly 1 ring heteroatom or exactly 2 ring heteroatoms, wherein one of said exactly 2 ring heteroatoms is N, and the other of said exactly 2 ring heteroatoms is independently N, O, or S,

and pharmaceutically and physiologically acceptable salts thereof.

5. A compound according to any one of claims 1 to 4 , wherein -G A is independently selected from:

—F,

—CF 3 , —OCF 3 ,

—OH, and —OR 2 .

6. A compound according to any one of claims 1 to 4 , wherein -G B is independently selected from:

—F,

—CF 3 , —OCF 3 ,

—OH, —OR 2 ; and

—[O—CH 2 CH 2 ] n —R B2 , where n is 2 to 6.

7. A compound according to any one of claims 1 to 4 , wherein -G B is independently —OCH 2 CH 2 N(Me) 2 or [O—CH 2 CH 2 ] n —R B2 , where n is 2 to 6.

8. A compound according to any one of claims 1 to 4 , wherein —P is independently:

9. A compound according to claim 8 , wherein —P 1 and —P 5 are independently —H or —P A .

10. A compound according to claim 8 , wherein —P 2 and —P 4 are independently —H or —P B .

11. A compound according to claim 8 , wherein —P 3 is independently —H or —P C .

12. A compound according to claim 9 , wherein —P A is independently selected from:

—F,

—CF 3 , —OCF 3 ,

—OH,

—OR 2 ,

—NO 2 ,

—NH 2 , —NHR 2 , —NR 2 2 , and —NR 3 R 4 .

13. A compound according to claim 10 , wherein —P B is independently selected from:

—F,

—CF 3 , —OCF 3 ,

—NO 2 ,

—NH 2 , —NHR 2 , —NR 2 2 , and —NR 3 R 4 .

14. A compound according to claim 11 , wherein —P C is independently selected from:

—F, —Cl, —Br, —I,

—CF 3 , —OCF 3 ,

—OH, —OR 2 ,

—NO 2 ,

—NH 2 , —NHR 2 , —NR 2 2 , —NR 3 R 4 ,

—NHOH,

—OC(═O)R 2 , and

—NHC(═O)R 2 .

15. A compound according to claim 8 , wherein at least one of —P 1 , —P 2 , —P 3 , P 4 , and —P 5 is not —H.

16. A compound according to any one of claims 1 to 4 wherein —P is independently selected from:

17. A compound according to claim 16 , wherein —P 2 , —P 3 , and —P 4 are each independently —H.

18. A compound according to claim 1 or claim 3 , wherein —W 5 is independently —H.

19. A compound according to claim 18 , wherein —W 6 is independently —H.

20. A compound according to claim 18 , wherein —W 4 is independently —H or —W A .

21. A compound according to claim 20 wherein —W A is independently selected from —OH, —W A1 , and —O—W A1 .

22. A compound according to claim 21 , wherein —W A1 is independently -Me.

23. A compound according to claim 1 , claim 2 or claim 4 wherein —W 1 is independently —H or —W A .

24. A compound according to claim 23 , wherein —W A is independently —W A1 .

25. A compound according to claim 24 , wherein —W A1 is independently -Me.

26. A compound according to claim 1 or claim 2 wherein —W 2 is independently —H or —W A .

27. A compound according to claim 26 , wherein —W A is independently -Me.

28. A compound according to claim 1 or claim 2 , wherein —W 3 is independently —H or —W A .

29. A compound according to claim 28 , wherein —W A is independently -Me.

30. A compound according to any one of claims 1 to 4 , wherein the compound has a molecular weight of 500 or less.

31. A compound according to any one of claims 1 to 4 , wherein the compound has a miLog P of from 2.0 to 5.0.

32. A compound according to any one of claims 1 to 4 , wherein the compound has a Log D of from 2.0 to 5.0.

33. A compound according to any one of claims 1 to 4 , wherein the compound has a topological polar surface area of 90 Å 2 or less.

34. A compound according to any one of claims 1 to 4 , wherein the compound has 3 or less hydrogen bond donors.

35. A method of detecting and/or visualizing paired helical filaments (PHFs), the method comprising

(a) contacting the PHFs with a compound which binds to said PHFs; and

(b) detecting the presence of said compound;

wherein the compound which binds to said PHFs is a compound as defined in any one of claims 1 to 4 .

36. A method of detecting and/or visualizing aggregated tau molecules, the method comprising

(a) contacting the aggregated tau molecules with a compound which binds to said aggregated tau molecules; and

(b) detecting the presence of said compound;

wherein the compound which binds to said aggregated tau molecules is a compound as defined in any one of claims 1 to 4 .

Assignments (5)
CHANGE OF ADDRESS Recorded Jan 20, 2015
From: WISTA LABORATORIES LTD.
To: WISTA LABORATORIES LTD.
Reel/Frame 034781/0897 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 8, 2011
From: HEINRICH, TOBIAS KERST
To: BAYER SCHERING PHARMA AG
Reel/Frame 027192/0117 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 8, 2011
From: BAYER SCHERING PHARMA AG
To: WISTA LABORATORIES LTD.
Reel/Frame 027192/0235 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 8, 2011
From: KEMP, STEVEN JOHN; STOREY, LYNDA JANE; STOREY, JOHN MERVYN DAVID; RICKARD, JANET; HARRINGTON, CHARLES ROBERT; WISCHIK, CLAUDE MICHEL; CLUNAS, SCOTT
To: THE UNIVERSITY COURT OF THE UNIVERSITY OF ABERDEEN
Reel/Frame 027192/0535 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 8, 2011
From: THE UNIVERSITY COURT OF THE UNIVERSITY OF ABERDEEN
To: WISTA LABORATORIES LTD.
Reel/Frame 027192/0736 →