IP Library Granted Patent US 8,367,117
Granted Patent B2
US 8,367,117 · App. 13/104,605 · Granted Feb 5, 2013

Nanocomposite hyaluronic acid-clay based hydrogels

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Quick Facts
Patent No.
US 8,367,117
App. No.
13/104,605
Granted
Feb 5, 2013
Kind
B2
Abstract

Hydrogels formed from hyaluronic acid, a nanoclay and gelatin-type A. The hyaluronic acid is preferably dissolved in a cell culture medium containing amino acids, salts, glucose, vitamins and an antibiotic to form a hyaluronic acid solution. The gelatin-type A has a weight/volume of from about 0.02% to 0.08%. The nanoclay is exfoliated in deionized water and preferably includes SiO 2 , MgO, Na 2 O and Li 2 O.

Claims (14)

1. A hydrogel comprising:

hyaluronic acid (“HA”);

a nanoclay; and

gelatin-type A

wherein the HA is dissolved in a cell culture medium containing amino acids, salts, glucose, vitamins and an antibiotic to form a HA solution;

wherein the hydrogel comprises 5-30 percent by weight HA, 5-30 percent by weight gelatin-type A, and about 40-90 percent by weight nanoclay; and

wherein the nonclay comprised about 55-65% SiO 2 , 20-35% MgO, 1-5%, Na 2 O and 0.2-2% LiO 2 O.

2. The hydrogel according to claim 1 , wherein the nanoclay is exfoliated in deionized water.

3. The hydrogel according to claim 1 , wherein the gelatin-type A has a weight/volume of from about 0.02% to 0.08%.

4. The hydrogel according to claim 3 , wherein the HA solution and gelatin-type A have a volume ratio of from about 8:5 to about 5:8.

5. The hydrogel according to claim 3 , wherein the HA solution and gelatin-type A have a volume ratio of about 1:1.

6. The hydrogel according to claim 3 , wherein the nanoclay has a weight/volume of from about 0.01% to about 0.08%.

7. The hydrogel according to claim 3 , wherein the volume ratio of HA/gelatin-type A mixture to clay is from about 1:5 to about 1:20.

8. The hydrogel according to claim 3 , wherein the hydrogel comprises 10-25 percent by weight HA, 10-25 percent by weight gelatin and about 50-80 percent by weight nanoclay.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 15, 2011
From: COWMAN, MARY K.
To: POLYTECHNIC INSTITUTE OF NEW YORK UNIVERSITY
Reel/Frame 026457/0351 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 15, 2011
From: RAFAILOVICH, MIRIAM; BHATNAGAR, DIVYA
To: THE RESEARCH FOUNDATION OF STATE UNIVERSITY OF NEW YORK
Reel/Frame 026459/0296 →
CONFIRMATORY LICENSE Recorded Jun 13, 2011
From: STATE UNIVERSITY NEW YORK STONY BROOK
To: NATIONAL SCIENCE FOUNDATION
Reel/Frame 026444/0871 →