IP Library Granted Patent US 8,450,629
Granted Patent B2
US 8,450,629 · App. 13/104,698 · Granted May 28, 2013

Method of producing molybdenum-99

View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 8,450,629
App. No.
13/104,698
Granted
May 28, 2013
Kind
B2
Abstract

Method of producing molybdenum-99, comprising accelerating ions by means of an accelerator; directing the ions onto a metal target so as to generate neutrons having an energy of greater than 10 MeV; directing the neutrons through a converter material comprising techentium-99 to produce a mixture comprising molybdenum-99; and, chemically extracting the molybdenum-99 from the mixture.

Claims (11)

1. A method of producing molybdenum-99, comprising:

a) accelerating ions by means of an accelerator;

b) directing the ions onto a metal target so as to generate neutrons having an energy of greater than 10 MeV;

c) directing the neutrons through a converter material comprising technetium-99 to produce a mixture comprising molybdenum-99; and,

d) chemically extracting the molybdenum-99 from the mixture by dissolving the mixture in a basic solution of sodium hydroxide or ammonium hydroxide having a pH of from about 10 to about 11, and passing the resulting solution through an strong-base anion exchange resin wherein molybdate anion, MoO 4 2− is captured selectively and pertechnetate anion, TcO 4 − passes through the resin, thereby producing molybdenum-99.

2. The method of claim 1 , wherein the metal target comprises metallic beryllium, lithium, or combinations thereof.

3. The method of claim 1 , wherein the technetium-99 is in the form of solid technetium metal, pertechnetate, a pertechnetate salt, or combinations thereof.

4. The method of claim 1 , wherein the accelerator is a cyclotron or a linear accelerator.

5. The method of claim 1 , wherein the accelerated ions are deuterons.

6. The method of claim 1 , wherein the technetium-99 is derived from spent nuclear fuel.

7. The method of claim 1 , wherein the molybdenum-99 is substantially isotopically pure, wherein substantially means greater than about 90% isotopically pure.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 7, 2018
From: LOS ALAMOS NATIONAL SECURITY, LLC
To: TRIAD NATIONAL SECURITY, LLC
Reel/Frame 047447/0201 →
CONFIRMATORY LICENSE Recorded Apr 23, 2012
From: LOS ALAMOS NATIONAL SECURITY
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 028086/0597 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 7, 2011
From: PITCHER, ERIC JOHN
To: LOS ALAMOS NATIONAL SECURITY, LLC
Reel/Frame 026403/0490 →