Magnetic in-line purification of fluid
View Patent ↗Methods for in-line purification of surfactant from a first fluid, such as a microemulsion are disclosed. Magnetic particles coated with surfactant molecules may be used to bind surfactants from a fluid. A magnetic field may be used to separate the bound materials from the fluid.
1. A method for in-line purification, the method comprising:
providing a first fluid having a plurality of first surfactant molecules;
providing a second fluid comprising magnetic particles coated with a plurality of second surfactant molecules selected to associate with the first surfactant molecules;
contacting the first fluid and the second fluid to form a mixture containing bound surfactant particles; and
passing the mixture through a magnetic channel to separate the bound surfactant particles from the mixture;
wherein the first fluid is a latex formed by a microemulsion polymerization reaction.
2. A method for in-line purification, the method comprising:
providing a first fluid having a plurality of first surfactant molecules;
providing a second fluid comprising magnetic particles coated with a plurality of second surfactant molecules selected to associate with the first surfactant molecules;
contacting the first fluid and the second fluid to form a mixture containing bound surfactant particles; and
passing the mixture through a magnetic channel to separate the bound surfactant particles from the mixture;
wherein the magnetic channel section is a section of a microchannel of a microreactor.
3. The method of claim 2 , wherein the magnetic channel section comprises one or more magnets exterior to the microchannel.
4. The method of claim 2 , wherein the magnetic channel section comprises one or more wire coils coupled to a selectable voltage source, and wherein the method further comprises selecting a voltage with the selectable voltage source.
5. A system for in-line purification, the system comprising:
a microreactor having a plurality of pumps; and
a control device operatively coupled to the microreactor and configured to selectively activate individual ones of the plurality of pumps to operate the microreactor to:
flow a first fluid through a first channel of the microreactor, wherein the first fluid includes a plurality of first surfactant molecules;
combine the first fluid with a second fluid including a plurality of second surfactant molecules selected to bind with the first surfactant molecules from a second channel of the microreactor to form a mixture containing the first surfactant molecules bound with the second surfactant molecules in a mixing area of the microreactor, wherein the mixing area is situated at an intersection of the first channel and the second channel, wherein the second fluid comprises magnetic particles coated with the plurality of second surfactant molecules; and
pass the mixture through a third channel coupled to the mixing area to separate the first surfactant molecules bound with the second surfactant molecules from the mixture, wherein the third channel comprises a magnetic channel section.
6. The system of claim 5 , wherein the microreactor further comprises an agitator situated along the third channel between the mixing area and the magnetic channel section, and wherein the control device is further configured to selectively activate the agitator.
7. The system of claim 5 , further comprising one or more wire coils situated along the magnetic channel section, and wherein the control device is further configured to selectively activate the one or more wire coils to generate a magnetic field.
8. The system of claim 5 , further comprising one or more magnets exterior to the magnetic channel section.
9. A computer-readable medium having instructions stored thereon that, in response to execution by a computing device coupled to a microreactor having a plurality of pumps, cause the computing device to generate signals to operate the microreactor to:
flow a first fluid through a first channel of the microreactor, wherein the first fluid includes a plurality of first surfactant molecules;
combine the first fluid with a second fluid including a plurality of second surfactant molecules selected to bind with the first surfactant molecules from a second channel of the microreactor to form a mixture containing the first surfactant molecules bound with the second surfactant molecules in a mixing area of the microreactor, wherein the mixing area is situated at an intersection of the first channel and the second channel, wherein the second fluid comprises magnetic particles coated with the plurality of second surfactant molecules; and
pass the mixture through a third channel coupled to the mixing area to separate the first surfactant molecules bound with the second surfactant molecules from the mixture, wherein the third channel comprises a magnetic channel section.
10. The computer-readable medium of claim 9 , wherein the instructions, in response to execution by the computing device, cause the computing device to generate signals to selectively activate an agitator of the microreactor.
11. The computer-readable medium of claim 9 , wherein the instructions, in response to execution by the computing device, cause the computing device to generate signals to selectively activate one or more wire coils situated proximally to the magnetic channel section to generate a magnetic field.