Method for producing parts made of a thermostructural composite material
View Patent ↗A method of fabricating a thermostructural composite material part includes making a fiber preform formed of yarns or tows and impregnated by a consolidating composition containing a carbon- or ceramic-precursor, transforming the carbon- or ceramic-precursor by pyrolysis, and then densifying the preform by chemical vapor infiltration. A consolidating composition is used that additionally contains refractory solid fillers in the powder form presenting mean grain size less than 200 nanometers and leaving, after pyrolysis, a consolidated solid phase in which the carbon or the ceramic derived from the precursor occupies a volume representing 3% to 10% of the apparent volume of the preform, and the solid fillers occupy a volume representing 0.5% to 5% of the apparent volume of the preform.
1. A method of fabricating a thermostructural composite material part, the method comprising:
providing a fiber texture formed of yarns or tows,
impregnating the yarns or tows with a consolidating composition in liquid form containing a carbon- or ceramic-precursor and refractory solid fillers in the form of a powder of mean grain size less than 200 nanometers,
forming a fiber preform with said impregnated fiber texture and holding the fiber preform in a desired shape,
pyrolyzing the carbon- or ceramic-precursor to obtain a fiber preform consolidated by a consolidating solid phase comprising the carbon or ceramic derived from the precursor and the refractory solid fillers, the impregnating being carried out such that the carbon or ceramic derived from the precursor occupies a volume representing 3% to 10% of the apparent volume of the preform and the refractory solid fillers occupy a volume representing 0.5% to 5% of the apparent volume of the preform, and
densifying the consolidated fiber preform with a matrix by chemical vapor infiltration.
2. A method according to claim 1 , wherein the volume percentage in the preform of the carbon or ceramic of the consolidating phase derived from the precursor lies in the range 3% to 6%.
3. A method according to claim 1 , wherein the volume percentage in the preform of the solid fillers of the consolidating phase lies in the range 0.5% to 3%.
4. A method according to claim 1 , wherein the solid fillers used present mean grain size of less than 100 nanometers.
5. A method according to claim 1 , wherein the fiber preform is made by conforming the fiber texture formed of yarns or tows and impregnated by the consolidating composition.
6. A method according to claim 5 , wherein the carbon- or ceramic-precursor in the consolidating composition is a resin, and the fiber preform is conformed after pre-curing the resin.
7. A method according to claim 1 , for fabricating a part out of a ceramic matrix composite material, wherein the solid fillers comprise a powder of at least one compound selected from SiC, TiC, B 4 C, and BN.
8. A method according to claim 1 , wherein an interphase layer is formed by chemical vapor infiltration on the fibers of the yarns or tows prior to impregnation with the consolidating composition.
9. A method according to claim 1 , wherein a first interphase layer is formed by chemical vapor infiltration on the fibers of the yarns or tows prior to impregnation by the consolidating composition, and a second interphase layer is formed after consolidation of the fiber preform and prior to densification of the consolidated fiber preform.