IP Library Granted Patent US 8,603,353
Granted Patent B2
US 8,603,353 · App. 13/148,679 · Granted Dec 10, 2013

Thermal insulation material comprising precipitated silica

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Quick Facts
Patent No.
US 8,603,353
App. No.
13/148,679
Granted
Dec 10, 2013
Kind
B2
Abstract

A thermal insulation material comprising a precipitated silica having a modified tapped density of less than or equal to 70 g/l.

Claims (33)

1. A thermal insulation material, comprising:

from 30 to 95% by weight of a comminuted and classified precipitated silica having a modified tapped density of 10 to 50 g/l; and

from 5 to 70% by weight of opacifier material.

2. The material of claim 1 , wherein

a) a d 50 -value of the precipitated silica is from 150 to 2000 nm,

b) a d 90 -value of the precipitated silica is from 500 to 7000 nm, and

c) a silanol group density of the precipitated silica is from 2.5 to 8 OH/nm 2 .

3. The material of claim 1 , wherein a BET-surface area of the precipitated silica is from 100 to 350 m 2 /g.

4. The material of claim 1 , wherein the precipitated silica has at least one property selected from the group consisting of

a loss on drying is from 1.5 to 8% by weight, and

a loss on ignition is from 1.5 to 9% by weight.

5. The material of claim 1 , wherein a pH-value of the precipitated silica is from 4 to 9.

6. The material of claim 1 , wherein a content of the precipitated silica is from 40 to 80 wt.-% based on a weight of the thermal insulation material.

7. The material of claim 1 , further comprising:

a particulate insulating filler material.

8. The material of claim 7 , wherein an amount of the particulate insulating filler material is from greater than 0 to 70 wt.-%, based on a weight of the thermal insulation material.

9. The material of claim 1 , further comprising

a binder material.

10. The material of claim 9 , wherein an amount of the binder material is from greater than 0 to 70 wt.-%, based on a weight of the thermal insulation material.

11. The material of claim 1 , wherein a thermal conductivity at a mean temperature of 300K of the precipitated silica is less than 0.05 W/mK at a reduced gas pressure.

12. A loose filled thermal insulation, a sheet, a block, or a vacuum isolation system, comprising the material of claim 1 .

13. The material of claim 2 , wherein a BET-surface area of the precipitated silica is from 100 to 350 m 2 /g.

14. The material of claim 2 , wherein

the precipitated silica has at least one property selected from the group consisting of

a loss on drying is from 1.5 to 8% by weight, and

a loss on ignition is from 1.5 to 9% by weight.

15. The material of claim 3 , wherein

the precipitated silica has at least one property selected from the group consisting of

a loss on drying is from 1.5 to 8% by weight, and

a loss on ignition is from 1.5 to 9% by weight.

16. The material of claim 2 , wherein the pH-value of the precipitated silica is from 4 to 9.

17. The material of claim 3 , wherein the pH-value of the precipitated silica is from 4 to 9.

18. The material of claim 4 , wherein the pH-value of the precipitated silica is from 4 to 9.

Assignments (1)
CHANGE OF NAME Recorded Jan 31, 2020
From: EVONIK DEGUSSA GMBH
To: EVONIK OPERATIONS GMBH
Reel/Frame 051765/0166 →