IP Library Granted Patent US 9,789,520
Granted Patent B2
US 9,789,520 · App. 13/160,220 · Granted Oct 17, 2017

Method for cleaning porous metallic filters using a steam-ultrasonic technique

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Quick Facts
Patent No.
US 9,789,520
App. No.
13/160,220
Granted
Oct 17, 2017
Kind
B2
Abstract

A method of cleaning plugged or dirty porous metallic filter elements to regain filter activity, comprising the steps of: steaming a filter element for a first period of time; submerging the filter element in a first solution; and exposing the first solution to ultrasound waves for a second period of time.

Claims (10)

1. A method for cleaning plugged or dirty porous sintered metal filter coupon to regain filter activity comprising the following steps in sequence:

i. arranging a filter coupon to be held at an angle between 10° to 40° from horizontal;

ii. steaming said filter coupon for a first period of time by blasting about 100 psig steam against the filter coupon in a back flushing orientation for about 10 to 20 minutes so as to dislodge fine particles from pores within the filter coupon;

iii. drying the filter coupon for about three hours with a device selected from the group consisting of: an oven, a dehumidifier, a heater or combinations thereof and where the filter coupon is heated to about 150° C.;

iv. submerging the filter coupon in a first solution at a depth of about 1 to 1.5 inches below the surface of the first solution wherein the first solution comprises at least water and citric acid;

v. exposing the filter coupon to ultrasound waves within the first solution for a second period of time of about 15 to 90 minutes wherein the ultrasound waves are applied to the filter coupon at a range of about 50 to 60 Hz; and

vi. soaking the filter coupon in a second solution for a third period of time being about one hour wherein the second solution is about 10 wt % citric acid in water.

2. The method of claim 1 , wherein the activity of the cleaned filter coupon regains about 90% of its original activity.

3. The method of claim 1 , wherein the activity of the cleaned filter coupon regains about 94% of its original activity.

4. The method of claim 1 , wherein the plugged or dirty porous metallic filter coupons occur from liquid or gaseous hydrocarbon streams.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 15, 2012
From: CONOCOPHILLIPS COMPANY
To: PHILLIPS 66 COMPANY
Reel/Frame 028213/0824 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 14, 2011
From: UPPILI, SUNDARARAJAN
To: CONOCOPHILLIPS COMPANY
Reel/Frame 026443/0751 →