IP Library Granted Patent US 8,518,335
Granted Patent B2
US 8,518,335 · App. 13/161,989 · Granted Aug 27, 2013

System for preparing silica aerogel powder

Inventors: Young Chul Joung (Suwon-si, KR); Myung Je Roe (Seoul, KR); Young Jong Yoo (Hwaseong-si, KR); Jong Chul Park (Hwaseong-si, KR); Hee Jung Choi (Seongnam-si, KR); Min Woo Kim (Daejeon-si, KR)
Assignee: Jios Aerogel Limited
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 8,518,335
App. No.
13/161,989
Granted
Aug 27, 2013
Kind
B2
Abstract

A system for preparing silica aerogel powders. The system includes a material supplier, a mixer, a drier and a recoverer. The material supplier transmitting de-ionized water, water glass, an organosilane compound, an inorganic acid and at least one organic solvent. Some of organic solvents are mixed and transmitted to the mixer and tramining organic solvent is transmitted to the mixer. The mixer mixes the materials transmitted from the material supplier so as to generate silica hydrogel. The drier dries the silica hydrogel so as to generate silica aerogel powders. The recoverer recovers some vaporized materials of the materials used in the mixer and the drier.

Claims (59)

1. A system for preparing silica aerogel powders, the system comprising:

a material supplier for transmitting de-ionized water, water glass, an organosilane compound, an inorganic acid and at least one organic solvent to the mixer;

a mixer for mixing the materials transmitted from the material supplier so as to generate silica hydrogel;

a drier for drying the silica hydrogel so as to generate silica aerogel powders; and

a recoverer for recovering some vaporized materials of the materials used in the mixer and the drier,

wherein some of organic solvents are mixed and then transmitted to the mixer and remaining organic solvent is transmitted to the mixer as it is.

2. The system of claim 1 , wherein the inorganic acid comprises HNO 3 , wherein the organic solvent is a nonpolar organic solvent, and wherein the organosilane compound comprises hexamethyldisilazane (HMDS).

3. The system of claim 1 , further comprising at least one of:

a therm oil boiler for transmitting therm oil to the mixer and the drier; and

a heater for transmitting heat to the mixer and the drier.

4. The system of claim 3 , wherein the material supplier comprises:

a first stirrer for generating a water glass solution by mixing de-ionized water and water glass at a predetermined ratio;

a second stirrer, when at least two organic solvents are input to the second stirrer, for mixing the at least two organic solvents;

a first storage tank comprising a first load cell for measuring an introduced amount of the organosilane compound; and

a second storage tank comprising a second load cell for measuring an introduced amount of the inorganic acid.

5. The system of claim 4 , wherein materials output from the first stirrer, the second stirrer, the first storage tank and the second storage tank are transmitted to the mixer according to a predetermined order.

6. The system of claim 3 , wherein the mixer comprises:

a first motor; and

a mixing tank, wherein the mixing tank comprises:

a stirrer rotated by the first motor and comprising a stirring shaft on which a plurality of impellers are installed; and

a temperature sensor for measuring an internal temperature of the mixing tank.

7. The system of claim 6 , wherein a predetermined space is formed between an internal wall and an external wall of the mixing tank, and

wherein the therm oil or the heat is supplied to the predetermined space so as to increase the internal temperature of the mixing tank.

8. The system of claim 3 , wherein the drier comprises:

a second motor; and

a drying tank, wherein the drying tank comprises:

a stirring shaft that is rotated by the second motor and on which a plurality of impellers are installed;

a temperature sensor for measuring an internal temperature of the drier; and

a filter for filtering some vaporized materials.

9. The system of claim 8 , wherein a predetermined space is formed between an internal wall and an external wall of the drying tank, and

wherein the therm oil or the heat is supplied to the predetermined space so as to increase the internal temperature of the mixing tank.

10. The system of claim 8 , wherein a portion of each impeller, which contacts the drying tank, is formed of Teflon.

11. The system of claim 1 , wherein the recoverer comprises:

a condenser for liquefying the vaporized material; and

a storage tank for storing a liquefied material.

12. The system of claim 11 , wherein the vaporized material comprises an organic solvent.

13. The system of claim 11 , wherein the recoverer further comprises:

a chiller for decreasing temperatures of the condenser and the storage tank; and

a vacuum pump for adjusting pressures of the condenser and the storage tank.

14. The system of claim 1 , wherein the de-ionized water, the water glass, the organosilane compound, the inorganic acid and the at least one organic solvent, which are stored in respective corresponding material containers, are transmitted to the material supplier through a diaphragm pump installed in each material container.

15. The system of claim 1 , further comprising a collector for collecting the silica aerogel generated in the drier.

16. The system of claim 15 , wherein at least one connection tube is installed between the material supplier and the mixer, between the mixer and the drier, between the drier and the recoverer, between the mixer and the recoverer and between the drier and the collector, and

wherein at least one connection tube is opened and closed by at least one valve.

17. The system of claim 3 , wherein at least one connection tube is connected between the mixer and the therm oil boiler and between the drier and the therm oil boiler, or between the mixer and the heater and between the drier and the heater, and

wherein at least one connection tube is opened and closed by at least one valve.

18. The system of claim 1 , wherein the mixer comprises:

a first motor; and

a mixing tank, wherein the mixing tank comprises:

a first heating coil installed outside the mixing tank;

a stirrer rotated by the first motor and comprising a stirring shaft on which a plurality of impellers are installed; and

a temperature sensor for measuring an internal temperature of the mixer.

19. The system of claim 1 , wherein the drier comprises:

a second motor; and

a drying tank, wherein the drying tank comprises:

a second heating coil installed outside the drying tank;

a stirrer rotated by the second motor and comprising a stirring shaft on which a plurality of impellers are installed;

a temperature sensor for measuring an internal temperature of the drier; and

a filter for filtering some vaporized materials.

20. The system of claim 19 , wherein a portion of the impeller, which contacts the drying tank, is formed of Teflon.

Assignments (5)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 9, 2023
From: JIOS AEROGEL LIMITED
To: AEROGEL R&D PTE. LTD.
Reel/Frame 062932/0331 →
RELEASE OF SECURITY INTEREST Recorded Jan 13, 2022
From: ARMACELL INTERNATIONAL GMBH
To: JIOS AEROGEL LIMITED
Reel/Frame 058645/0617 →
SECURITY INTEREST Recorded Apr 5, 2017
From: JIOS AEROGEL LIMITED
To: ARMACELL INTERNATIONAL GMBH
Reel/Frame 042162/0682 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 12, 2013
From: JIOS CO.,LTD.
To: JIOS AEROGEL LIMITED
Reel/Frame 030209/0279 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 17, 2011
From: JOUNG, YOUNG CHUL; ROE, MYUNG JE; YOO, YOUNG JONG; PARK, JONG CHUL; CHOI, HEE JUNG; KIM, MIN WOO
To: JIOS CO., LTD.
Reel/Frame 026453/0378 →
Priority Claims (1)
KR 10-2011-0025718 · Mar 23, 2011 · national
Continuity (1)
Related Publication 20120244040A1 · Sep 27, 2012